1、 KSKSKSKS KS M 8411SKSKSKS KSKSKS SKSKS KSKS SKS KS ()KS M 8411: 2006 2006 5 8 M 8411: 2006 ( ) ( ) SK R&D center ( ) ( ) ( ) ( ) : : 1996 12 30 : 2006 5 8 2006 0191 : : ( ) ( 02 509 7302 5) . 7 5 , . ICS 71.040.30 KS ( ) M 8411: 2006Propylene glycol CH3CH(OH)CH2OH FW: 76.10 1. (1)( .) . (1) 1,2 . 2
2、. . . KS M 0004 KS M 0005 KS M 0009 KS M 0010 KS M 0024 KS M 8001 3. 3.1 . , . 189 . 3.2 KS M 0024 3 390 cm 1, 2 970 cm 1, 1 460 cm 1, 1 380 cm 1, 1 140 cm 1, 1 050 cm 1 990 cm 1 . KS M 0024 7.3 a) . . M 8411: 2006 (%) (cm 1) 4. 5. , . (GC) (20 ) n 20D ( ) (CH3COOH ) (Cl) (SO4) (Pb) 99.0 % 1 034 1 0
3、38 kg/m31.429 1.434 0.2 % 0.005 % 0.006 % 0.001 % 0.002 % 5 ppm 5. 5.1 (GC) KS M 8001 6.32 . a) b) 1) 150 250 m , 20 % . 2 M 8411: 2006 W, W, 545 , 20 M . 2) 2 4 mm, 2 3 m 3) 150 190 220 270 220 270 4) , 30 50 mL/min 5) 0.6 L 5.2 10 mL 20 mL , 30 . 5.3 (20) KS M 0004 3.2 a) . 5.4 n KS M 0005 . 20D5.
4、5 KS M 0010 4.3( ) . 1.0 g . 5.6 ( ) KS M 0009 5.4.4 d) . 20 g, 0.5 mL 1 mg . 5.7 (CH3COOH ) 10 mL 200 mL/min 2 (100 mL) , 50 mL 3 , 0.02 mol/L 0.02 mol/L (2) (3) 10 g . ( ) , 0.05 mol/L 0.20 mL ( ) . (2) 0.01 mL . (3) KS M 8001 6.28 pH 6.8 70 mL (100 mL) 3 0.05 mol/L 1 mL 0.003 002 6 g CH3COOH . 5.
5、8 ( Cl) a) 2 g 20 mL , (1: 2) 5 mL 25 mL . b) (0.01 mg Cl/mL) 2.0 mL (1: 2) 5 mL 25 mL . c) KS M 8001 6.7 a) . 5.9 ( SO4) a) 2.0 g 20 mL (2: 1) 0.3 mL 25 mL . b) (0.01 mg SO4/mL) 4.0 mL (2: 1) 0.3 mL 25 mL . c) KS M 8001 6.15 a) . 5.10 ( Pb) a) 5.0 g 20 mL (1: 2) 0.3 mL . b) (0.01 mg Pb/mL) 2.5 mL 2
6、0 mL , (1: 2) 0.3 mL . c) KS M 8001 6.24 a) . 5.11 KS M 8001 6.26 c) 1) . 3 M 8411: 2006 5 mL 6 mL C . 6. . 7. . 8. . a) “ ” “ ” b) c) d) ( ) e) f) g) h) 4 ( ) 2006 6 2 135 513 701 7 (02)6009 4567 (02)6009 4887 8 http:/ 607 822 1 11( 10 ) (051)557 1239 Fax. (051)557 0430 702 845 2 1741( 3 ) (053)384
7、 1562 4 Fax. (053)384 1565 790 380 627( 3 ) (054)278 9661 Fax. (054)278 9662 406 829 7 50( 16 ) (032)260 0260 7 Fax. (032)260 0268 443 766 906 5( 9 ) (031)259 7000 9 Fax. (031)259 7010 200 041 1 9( 304 ) (033)252 9423, 254 9423 Fax. (033)256 9423 361 802 1508 1( 6 ) (043)236 2451 3 Fax. (043)236 245
8、4 305 343 23 14( 5 ) (042)864 2301 3 Fax. (042)864 2304 330 816 43 5( 1204 ) (041)589 0500 3 Fax. (041)589 0504 561 736 1 337 2( 7 ) (063)214 2235 7 Fax. (063)214 2238 506 301 621 15( 4 ) (062)953 1435 7 Fax. (062)953 1438 641 966 298 7( 6 ) (055)212 1212 Fax. (055)212 1213 683 804 758 2( 2 ) (052)2
9、89 6601 3 Fax. (052)289 6604 425 020 541 3( 4 ) (031)487 6191 4 Fax. (031)487 6195 730 350 92 30( 8 ) (054)473 6954 Fax. (054)473 6955 480 848 2 487 6( 3 ) (031)829 8182 4 Fax. (031)829 8185 KS M 8411: 2006 KOREAN STANDARDS ASSOCIATION KSKSKSSKSKS KSKS SKS KSKS SKSKS KSKSKSPropylene glycol ICS 71.040.30