KS M ISO 1408-2012 Rubber-Determination of carbon black content-Pyrolytic and chemical degradation methods《橡胶 炭黑含量的测定 热解和化学降解法》.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 1408 KS M ISO 1408: 2012 2012 3 19 http:/www.kats.go.krKS M ISO 1408:2012 : ( ) ( ) () ( ) : (http:/www.standard.go.kr) : :2012 3 19 2012-0114 : : ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS M ISO 1408:2012 i ii 1 1 2 2 3 2 3.1 A 2 3.2 B 2 3.

2、3 C 2 4 A .3 4.1 .3 4.2 .3 4.3 5 4.4 .5 4.5 6 5 B .6 5.1 .7 5.2 .7 5.3 .7 5.4 9 6 C .9 6.1 .9 6.2 .10 6.3 .10 6.4 11 7 .12 KS M ISO 1408:2012 ii 1995 3 ISO 1408, Rubber Determination of carbon black contentPyrolytic and chemical degradation methods , . KS M ISO 1408:2012 Rubber Determination of carb

3、on black content Pyrolytic and chemical degradation methods 1 1.1 (A) (B C) . 1.2 A A , (graphitic carbon), , (bitumen) , . , - - - - 30 %(m/m) , , . 30 %(m/m) - . 1.3 B B - KS M ISO 1408:2012 2 , A . 1.4 C C A B , A B - - . 2 . . ( ) . KS L ISO 383, KS M ISO 1407, 3 3.1 A , . 850 . . (furnace) . .

4、. 3.2 B . . , 850 . ( ) (850 ) . . . 3.3 C p- , (tert-butyl hydroperoxide) . 850 . ( ) (850 ) . . . KS M ISO 1408:2012 3 4 A . (fume cupboard)( ) . 4.1 , , ( ) . 4.1.1 “ ” (purification) . 4.1.2 4.1.3 (Xylene) 4.1.4 4.1.5 (Dichloromethane) 4.1.6 - (ETA) 7 (absolute) 3 . , 7 3 ( ) 4 . 1 (fraction) .

5、4.2 . 4.2.1 , (50 60) mm 4.2.2 (tube furnace) 1 , . KS M ISO 1408:2012 4 1 4.2.2.1 (porcelain) , (4.2.1) . . (4.2.2.2) 30 cm . , . 4.2.2.2 (furnace) (4.2.2.1) . , (85025) . . 4.2.2.3 (4.2.2.1) (4.2.2.4) , . 4.2.2.4 (Inlet tube) (side tube) (4.2.2.3) (joint) (4.2.2.1) . PVC . 4.2.2.5 , (4.2.2.1) (4.1

6、.3) 2 , . 29/32 29/32 850 25 KS M ISO 1408:2012 5 4.2.3 KS M ISO 1407 4.2.4 4.2.5 (85025) 4.3 1.5 g , 1 . 4.4 4.4.1 0.5 mm 6 . (0.1 0.5) g . , 1 mm . 4.4.2 0.1 mg ( m0). . , (4.1.4) 4 . , (4.1.5) 4 . (4.1.5) . ETA (4.1.6) . . . , . 4.4.3 , (1003) . 4.4.4 (4.2.1) , (4.2.2.1) . 4.4.5 (fitting) (4.1.1)

7、 . (850 25) (4.2.2.2) , . (4.2.2.5) . 4.4.6 5 200 cm3/ . KS M ISO 1408:2012 6 4.4.7 100 cm3/ , 5 . 4.4.8 5 . 4.4.9 , 10 . 4.4.10 (4.2.4) 0.1 mg ( m1). . 4.4.11 . (4.1.2) 100 cm3/ . . 4.4.12 4.4.11 , (4.2.5) (85025) . 4.4.13 . 4.4.14 0.1 mg ( m2). . 4.4.15 . 4.5 . 100021mmm m0 : (: g) (4.4.2 ) m1 : (

8、: g) (4.4.10 ) m2 : (: g) (4.4.14 ) 1 . , m0 . 2 ( ) 850 . . , . 5 B , . , (digestions), (washing) . KS M ISO 1408:2012 7 5.1 4.1 5.1.1 ( 1.42 Mg/m3) 5.1.2 2 ( 1.18 Mg/m3) 98 . 5.1.3 5.1.4 - 1+1 (V/V) 5.1.5 250 g/dm3 5.1.6 150 g/dm3 5.2 4.2 5.2.1 (Gooch) , . . , . , . , . , 5.3.5 5.3.16 2 (85025) .

9、(4.2.2) . 5.3 5.3.1 (0.3 0.5) g 0.1 mg ( m0). . 4.4.2 4.4.3 . 5.3.2 10 cm3 (5.1.1) 100 cm3 . . 5.3.3 . , . KS M ISO 1408:2012 8 . 5.3.4 (5.1.1) 50 cm3 , 2 . . 5.3.3 5.3.4 . . , (KS M ISO 5478 ) . . 5.3.5 (Gooch) (5.2.1) . 5.3.6 10 cm3 (5.1.1) 3 3 , . 5.3.7 , . . 5.3.8 10 cm3 (4.1.1) 3 3 , . 5.3.9 10

10、 cm3 - (5.1.4) 3 3 , . 5.3.10 10 cm3 (5.1.3) 3 , . , . , 5.3.11 . 5.3.11 250 g/dm3 (5.1.5) 25 cm3 , 30 . 5.3.12 35 cm3 , , . 5.3.13 150 g/dm3 (5.1.6) 10 cm3 3 . 5.3.14 (5.1.2) . 5.3.15 10 cm3 (4.1.4) . KS M ISO 1408:2012 9 5.3.16 (85025) (4.2.2) . (4.2.4) , 0.1 mg ( m1). . 5.3.17 , (4.1.2) . (85025)

11、 . 0.1 mg ( m2). . 5.3.18 . 5.3.19 . 5.4 . 100021mmm m0 : (: g) (5.3.1 ) m1: 850 (: g) (5.3.16 ) m2: 850 (: g) (5.3.17 ) ( ) 850 . . , . 6 C , . , (digestions), (washing) . 6.1 4.1 5.1 . 6.1.1 1,4- (p- ) 1,2- (o- ) (1,4-Dichlorobenzene (p-dichlorobenzene) or 1,2-dichlorobenzene (o-dichlorobenzene) 6

12、.1.2 (tert-Butyl hydroperoxide Solution) 60 % . 40 % - - (tert-butanol). . KS M ISO 1408:2012 10 6.1.3 6.2 4.2 5.2 6.2.1 150 cm3, 34/35 (female) (joint) KS L ISO 383 . 6.2.2 - 34/35 KS L ISO 383 . 6.2.3 250 mm, - 34/35 (male) KS L ISO 383 . 6.2.4 ( ) 200 6.2.5 5.2 , 6.3.7 6.3.15 2 (85025) 6.3 6.3.1

13、(0.3 0.5) g 0.1 mg ( m0). . 20 g (6.1.1) . 6.3.2 ( ) ( ) 30 60 (6.2.2) . , , . PTFE . 6.3.3 6.3.2 (80 90) , (6.2.3) , 5 cm3 (6.1.2) . 6.3.4 30 60 ( ) (50 60) . 6.3.5 (100 150) cm3 (6.1.3) . 6.3.6 1 2 . , , . 2 KS M ISO 1408:2012 11 , 6.3.2 6.3.4 . 6.3.7 (6.2.5) , 10 cm3 (6.1.3) 3 3 . , , 6.3.5 6.3.7

14、 (6.1.3) (4.1.4) . 6.3.8 10 cm3 (4.1.4) 3 3 . 6.3.9 . . 6.3.10 10 cm3 (5.1.1) 3 3 . 6.3.11 (5.1.2) . 6.3.12 . 6.3.13 10 cm3 (4.1.4) . 6.3.14 (85025) (4.2.2) . (4.2.4) , 0.1 mg ( m1). . 6.3.15 , (4.1.2) . (85025) . 0.1 mg ( m2). 6.3.16 . 6.3.17 . 6.4 . 100021mmm m0 : (: g) (6.3.1 ) m1 : 850 (: g) (6.

15、3.14 ) m2 : 850 (: g) (6.3.15 ) ( ) 850 KS M ISO 1408:2012 12 . . , . 7 . a) b) c) ( A, B, C) d) e) f) g) 153787 1 92 3(13) (02)26240114 (02)262401489 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M ISO 1408:2012 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS RubberDetermination of

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