1、 Comments, suggestions, or questions on this document should be addressed to: Commander, Naval Sea Systems Command, ATTN: SEA 05S, 1333 Isaac Hull Avenue, SE, Stop 5160, Washington Navy Yard, DC 20376-5160 or emailed to CommandStandardsnavy.mil, with the subject line “Document Comment”. Since contac
2、t information can change, you may want to verify the currency of this address information using the ASSIST Online database at https:/assist.daps.dla.mil. AMSC N/A FSC 9150 METRIC MIL-PRF-009000K(SH) 27 April 2011 USED IN LIEU OF MIL-PRF-9000J(SH) 07 January 2010 PERFORMANCE SPECIFICATION LUBRICATING
3、 OIL, SHIPBOARD INTERNAL COMBUSTION ENGINE, HIGH-OUTPUT DIESEL This specification is approved for interim use by the Naval Sea Systems Command, Department of the Navy. Other activities in the Department of Defense may use this interim revision or may continue using MIL-PRF-9000J. 1. SCOPE 1.1 Scope.
4、 This specification covers one grade (SAE 40) of lubricating oil for use in advanced design high-output shipboard main propulsion and auxiliary diesel engines using fuel conforming to MIL-DTL-16884 and MIL-DTL-5624. This lubricating oil is identified as Military Symbol 9250 and NATO Code 0-278. 2. A
5、PPLICABLE DOCUMENTS 2.1 General. The documents listed in this section are specified in sections 3, 4, or 5 of this specification. This section does not include documents cited in other sections of this specification or recommended for additional information or as examples. While every effort has bee
6、n made to ensure the completeness of this list, document users are cautioned that they must meet all specified requirements of documents cited in sections 3, 4, or 5 of this specification, whether or not they are listed. 2.2 Government documents. 2.2.1 Other Government documents, drawings, and publi
7、cations. The following other Government documents, drawings, and publications form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. BUREAU OF MEDICINE AND SURGERY (BUMED) BUMED INST 6270
8、.8 - Procedures for Obtaining Health Hazard Assessments Pertaining to Operational Use of a Hazardous Material (Copies of this document are available from the Bureau of Medicine and Surgery, Department of the Navy, 2300 E Street, NW, Washington, DC 20372-5300 or online at http:/navymedicine.med.navy.
9、mil.) NAVAL SEA SYSTEMS COMMAND (NAVSEA) S9510-AB-ATM-010 - Nuclear Powered Submarine Atmosphere Control Manual (Copies of this document are available from the Naval Logistics Library, 5450 Carlisle Pike, Mechanicsburg, PA 17055 or online at http:/nll.ahf.nmci.navy.mil.) Provided by IHSNot for Resal
10、eNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-009000K(SH) 2 2.3 Non-Government publications. The following documents form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitat
11、ion or contract. AMERICAN NATIONAL STANDARDS INSTITUE (ANSI) ANSI/ASQC Z1.4 - Sampling Procedures and Tables for Inspection by Attributes (DoD adopted) (Copies of this document are available from the American National Standards Institute, 25 W. 43rd St, 4th Floor, New York, NY 10036 or online at htt
12、p:/webstore.ansi.org/.) AMERICAN PETROLEUM INSTITUTE (API) API 1509 - API Base Oil Interchangeability Guidelines for Passenger Car Motor Oils and Diesel Engine Oils (Copies of this document are available from API Publications, Global Engineering Documents, 15 Inverness Way East, M/S C303B, Englewood
13、, CO 80112-5776 or online at http:/.) ASTM INTERNATIONAL ASTM D92 - Standard Test Method for Flash and Fire Points by Cleveland Open Cup Tester (DoD adopted) ASTM D97 - Standard Test Method for Pour Point of Petroleum Products (DoD adopted) ASTM D129 - Standard Test Method for Sulfur in Petroleum Pr
14、oducts (General Bomb Method) (DoD adopted) ASTM D130 - Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test (DoD adopted) ASTM D287 - Standard Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer Method) (DoD adopted) ASTM D445 -
15、Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity) (DoD adopted) ASTM D874 - Standard Test Method for Sulfated Ash from Lubricating Oils and Additives (DoD adopted) ASTM D892 - Standard Test Method for Foaming Characteristics of
16、Lubricating Oils (DoD adopted) ASTM D1091 - Standard Test Methods for Phosphorus in Lubricating Oils and Additives (DoD adopted) ASTM D1298 - Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method (D
17、oD adopted) ASTM D1552 - Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method) (DoD adopted) ASTM D2270 - Standard Practice for Calculating Viscosity Index from Kinematic Viscosity at 40 and 100C (DoD adopted) Provided by IHSNot for ResaleNo reproduction or networking permi
18、tted without license from IHS-,-,-MIL-PRF-009000K(SH) 3 ASTM D2622 - Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-Ray Fluorescence Spectrometry (DoD adopted) ASTM D2896 - Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid
19、Titration (DoD adopted) ASTM D3228 - Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method (DoD adopted) ASTM D4047 - Standard Test Method for Phosphorus in Lubricating Oils and Additives by Quinoline Phosphomolybdate Method (DoD adopted) ASTM D4052 -
20、Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter (DoD adopted) ASTM D4057 - Standard Practice for Manual Sampling of Petroleum and Petroleum Products (DoD adopted) ASTM D4485 - Standard Specification for Performance of Engine Oils ASTM D4628 - Standard Test M
21、ethod for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oil by Atomic Absorption Spectrometry (DoD adopted) ASTM D4629 - Standard Test Method for Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection (DoD adopte
22、d) DELETED - DELETED DELETED - DELETED ASTM D4927 - Standard Test Methods for Elemental Analysis of Lubricant and Additive Components - Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy (DoD adopted) ASTM D4951 - Standard Test Method for Determina
23、tion of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (DoD adopted) ASTM D5182 - Standard Test Method for Evaluating the Scuffing Load Capacity of Oils (FZG Visual Method) DELETED - DELETED ASTM D5762 - Standard Test Method for Nitrogen in Petroleum
24、 and Petroleum Products by Boat-Inlet Chemiluminescence ASTM D5949 - Standard Test Method for Pour Point of Petroleum Products (Automatic Pressure Pulsing Method) ASTM D5950 - Standard Test Method for Pour Point of Petroleum Products (Automatic Tilt Method) DELETED - DELETED ASTM D6443 - Standard Te
25、st Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure) Provided by IHSNot for ResaleNo reproduction or networking permitted
26、 without license from IHS-,-,-MIL-PRF-009000K(SH) 4 ASTM D6481 - Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy ASTM D6557 - Standard Test Method for Evaluation of Rust Preventive Characteristic
27、s of Automotive Engine Oils ASTM E29 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications (DoD adopted) (Copies of these documents are available from ASTM International, 100 Barr Harbor Dr., PO Box C700, West Conshohocken, PA 19428-2959 or online
28、 at www.astm.org.) 2.4 Order of precedence. Unless otherwise noted herein or in the contract, in the event of a conflict between the text of this document and the references cited herein (except for related specification sheets), the text of this document takes precedence. Nothing in this document,
29、however, supersedes applicable laws and regulations unless a specific exemption has been obtained. 3. REQUIREMENTS 3.1 Qualification. The lubricating oil furnished under this specification shall be products that are authorized by the qualifying activity for listing on the applicable qualified produc
30、ts list before contract award (see 4.2 and 6.3). 3.1.1 Requalification. The continued qualification of products shall be verified every 5 years by submission of a signed statement by the oil supplier attesting that no formulation changes have been made in the qualified product. Any changes in the fo
31、rmulation of the product submitted for qualification testing shall be approved by NAVSEA. Minor changes, such as an increase in pour point additive, may require only notification; however, the extent of supporting test data required is at the discretion of NAVSEA. 3.2 Material. The oil shall consist
32、 of refined mineral oil blended with additives as necessary to conform to this specification. 3.3 Lubrication. The oil shall lubricate oil-lubricated high-output marine diesel engine parts, engine-driven generator bearings, and associated equipment. 3.4 Performance. The oil shall perform when used w
33、ith all types of diesel engine bearing materials, shall cause neither excessive ring sticking nor clogging of oil channels, shall keep cylinder and ring wear down to a minimum, and shall not cause excessive lacquer, carbon, or sludge deposits on any part of the engines in which it is intended for us
34、e. Oils qualified under this specification shall comply with the acceptance criteria in ASTM D4485 for CF and DDC 6V-92TA tests (see 4.6.2). 3.5 Compatibility. The addition of a new diesel engine lubricating oil to any other new lubricating oil conforming to this specification shall not cause separa
35、tion of components (see 4.6.3). 3.6 Homogeneity. Additive agents, when used, shall remain uniformly distributed throughout the oil at all temperatures above the pour point up to 180 C. If the oil is cooled below its pour point, it shall regain its homogeneity at a temperature of 6 C above its pour p
36、oint within 24 hours (see 4.6.4). 3.7 Chemical and physical requirements. The oils shall conform to the chemical and physical requirements shown in table I. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-009000K(SH) 5 TABLE I. Chemical and p
37、hysical requirements. Characteristics Requirements Methods (ASTM unless otherwise noted) Appearance Clear, homogenous, and free from visible water, particles, and sediments Visual examination Ash, sulfated, % 1/ D874 Corrosion test at 100 C, (copper strip) appearance, maximum 1b D130 2/ Flash point,
38、 C, minimum 225 D92 Foam (stability only), mL maximum Sequences I & III (at 24 C) Sequence II (at 93.5 C) 30 5 ASTM D892 3/ Gravity, degree API 1/ D287, D1298, D4052 Metals/Elements Barium, ppm Calcium, ppm Magnesium, ppm, maximum Nitrogen, ppm Phosphorus, ppm Zinc, ppm 1/ 1/ 100 1/ 1/ 1/ 4/ D4628,
39、D4927, D4951 D4628, D4927, D4951, D6443, D6481 D4628, D4927, D4951, D6443 D3228, D4629, D5762 D1091, D4047, D4927, D4951, D6443, D6481 D4628, D4927, D4951, D6443, D6481 Pour point, C, maximum -12 D97, D5949, D5950 Rust prevention, rating, minimum 100 D6557 Scuffing load capacity (FZG), failure load
40、stage, minimum 11 D5182 Sulfur 1/ D129, D1552, D2622, D4927, D6443, D6481 Total base number, mg KOH/g, minimum 12 D2896 Viscosity index, minimum 90 D2270 Viscosity, cSt at 100 C 12.5 to 16.3 D445 Viscosity, cSt at 40 C, minimum 120 D445 NOTES: 1/ No limiting requirements. In conformance testing, val
41、ues are compared to qualification results (see 4.5). 2/ Test shall be run for 3 hours at specified temperature. 3/ Option A shall not be used. A ring of bubbles around the edge of the graduate shall be considered complete collapse or 0 mL. 4/ The contractor shall certify that if zinc is present, it
42、is present as zinc dialkyl dithiophosphate, as zinc diaryl dithiophosphate, or as a combination of the two. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-009000K(SH) 6 TABLE II. Chemical and physical requirements (SAE 15W40 Grade). DELETED
43、TABLE III. Conformance tests with tolerances. Test Tolerances, if applicable Appearance - Gravity, API +1.0 Viscosity, cSt at 100 C +0.5 1/ Viscosity, cSt at 40 C +10 1/ Viscosity index - Flash point, C +8 1/ Pour point, C - Foam test, mL - Sulfur, mass % +20% of original value Phosphorus, ppm +10%
44、Zinc, calcium, and magnesium, ppm +10% Total base number, mg KOH/g - NOTE: 1/ Shall meet specification requirements. 3.8 Toxicity. When evaluated in accordance with 4.6.5, the oil shall have no adverse effect on the health of personnel when used for its intended purpose. The oil shall be assessed by
45、 the Navy and Marine Corps Public Health Center (NMCPHC) using the administrative Health Hazard Assessment (HHA). A flowchart for this process can be found as enclosure (1) of BUMEDINST 6270.8. The HHA is a review of the oil based on information submitted by the manufacturer to assess health hazards
46、 associated with the handling, application, use, and removal of the product. The oil shall not cause any environmental problems during waste disposal (see 4.6.5 and 6.8). 3.9 Off-gassing. The oil shall be certified for and assigned a usage category of “Limited” in accordance with NAVSEA S9510-AB-ATM
47、-010 chapter titled “Material Control Program” (see 4.6.6 and 6.9). 3.10 2,6-Di-tert-butylphenol (DTBP). The addition of DTBP (Chemical Abstract Service Number 128-39-2) in any lubricating oil produced under this specification is prohibited. This applies to both surface ship and submarine use. DTBP
48、shall not be intentionally added to the oil. The level of DTBP, if detected, shall not exceed 10 parts per million. (see 4.6.7) 3.11 Ozone depleting substances (ODS). The use of ODS in the composition of the lubricating oil under this specification directly or referenced in any federal test method i
49、s hereto prohibited. Environmentally safe and non-ODS alternative solvents shall be substituted in test methods for any previously specified ODS. 4. VERIFICATION 4.1 Classification of inspections. The inspection requirements specified herein are classified as follows: a. Qualification inspection (see 4.2). b. Conformance inspection (see 4.5). 4.2 Qualification inspection. Qualification tests shall be conducted at a laborato
