1、Designation: C1312 97 (Reapproved 2012)Standard Practice forMaking and Conditioning Chemical-Resistant SulfurPolymer Cement Concrete Test Specimens in theLaboratory1This standard is issued under the fixed designation C1312; the number immediately following the designation indicates the year oforigin
2、al adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers procedures for making and condi-tioning test
3、 specimens of chemical-resistant sulfur polymercement concrete (SC) in the laboratory. The specimens are castunder accurate control of materials and test conditions usingaggregate and sulfur polymer cement (SPC) to make SC thatcan be consolidated by rodding, as described in this practice.1.2 Sulfur
4、polymer cement may be furnished as a single ormultiple component system.1.3 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.4 This stan
5、dard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 A
6、STM Standards:2C470/C470M Specification for Molds for Forming ConcreteTest Cylinders VerticallyC904 Terminology Relating to Chemical-Resistant Nonme-tallic Materials2.2 National Institute of Standards and Technology:Handbook 44: Specifications, Tolerances and Other Techni-cal Requirements for Weighi
7、ng and Measuring Devices33. Terminology3.1 DefinitionsFor definitions of terms used in thispractice, refer to Terminology C904.4. Significance and Use4.1 This practice is for making specimens of SC in astandard way so that comparative testing can be performed byvarious producers and users. Use of th
8、is practice to preparespecimens for laboratory testing will reduce variability thatmight be introduced by different methods of casting and by theuse of a variety of specimen shapes and sizes.5. Apparatus5.1 Molds:5.1.1 Molds for Specimens or Fastenings Thereto in Contactwith the SC shall be made of
9、steel, cast iron, or othernonabsorbent materials that are nonreactive with concretescontaining either SPC, its components, or other polymercements.5.1.2 Size of the Molds shall conform to the dimensions andtolerances specified in the procedure for which the specimensare required. Molds shall hold th
10、eir dimensions and shapeunder conditions of severe use.5.1.3 Condition of the Molds for Casting shall be watertight.A suitable sealant, such as modeling clay, shall be used wherenecessary to prevent leakage through joints. Positive meansshall be provided to hold base plates firmly to the molds. Ifcy
11、linders are filled vertically and immediately stored horizon-tally for cooling, positive means also shall be provided to holdtop plates firmly to the molds. Reusable molds shall be lightlycoated with mineral oil or a suitable nonreactive releasematerial before use.5.2 Cylinder Molds:5.2.1 Molds for
12、Casting Specimens Vertically shall conformto the requirements of 5.1 and Specification C470/C470M.5.2.2 Molds for Casting Specimens Vertically and StoringHorizontally shall conform to the requirements for symmetryand dimensional tolerances of Specification C470/C470M.Provision shall be made for fixi
13、ng both end plates firmly to themold.1This practice is under the jurisdiction of ASTM Committee C03 on Chemical-Resistant Nonmetallic Materialsand is the direct responsibility of SubcommitteeC03.02 on Monolithics, Grouts and Polymer Concretes.Current edition approved Aug. 1, 2012. Published Septembe
14、r 2012. Originallyapproved in 1996. Last previous edition approved in 2008 as C1312 97 (2008).DOI: 10.1520/C1312-97R12.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer
15、to the standards Document Summary page onthe ASTM website.3Available from National Institute of Standards and Technology (NIST), 100Bureau Dr., Stop 1070, Gaithersburg, MD 20899-1070, http:/www.nist.gov.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-295
16、9. United States15.3 Beam and Prism Molds shall be rectangular in crosssection (unless otherwise specified) and of the dimensionsrequired to produce the desired specimen size. The insidesurfaces of the molds shall be smooth and free from indenta-tions. The sides, bottom, and ends shall be at either
17、equal orright angles to each other and shall be straight, true, and free ofwarpage. Maximum variation from the nominal cross sectionshall not exceed18 in. (3.2 mm) for molds with depth orbreadth of 6 in. (152 mm) or more, or116 in. (1.6 mm) formolds of smaller depth or breadth. Except for flexurespe
18、cimens, molds shall not vary from the nominal length bymore than116 in. Flexure molds shall not be shorter than therequired specimen length but may exceed it.5.4 Consolidation, Mixing, and Other Miscellaneous Equip-ment shall be specified by the manufacturer see AppendixX1.5.5 Weighing Equipment sha
19、ll be capable of weighingmaterials or specimens to 60.3 % accuracy. The weighingequipment shall meet the National Institute of Standards andTechnology requirements for sensitivity and tolerances.5.6 Concrete Mixer A power-driven revolving-paddlemixer or suitable equivalent capable of thoroughly mixi
20、ngbatches of the prescribed sizes at the required temperaturesshall be used.6. Test Specimens6.1 Cylindrical SpecimensCylinders for such tests ascompressive strength, modulus of elasticity, creep, and split-ting tensile strength may be of various sizes with a minimumof 1 in. (25 mm) diameter by 2 in
21、. (50 mm) length. Otherwise,dimensions are governed in accordance with 6.4 and the testmethod concerned.6.1.1 Cylindrical specimens for tests shall be molded withthe axis of the cylinder vertical but may be allowed to hardenin the horizontal position.6.2 Prismatic SpecimensBeams for flexural strengt
22、h,cubes for compressive strength, prisms for freezing andthawing, bond, length change, volume change, and so forth,shall be cast with their long axes vertical, unless otherwiserequired by the method of test in question, and shall conformin dimension to the requirements of the specific test method.6.
23、3 Other Specimens Other shapes and sizes of specimensfor particular tests may be molded as desired following thegeneral procedures set forth in this practice.6.4 Specimen Size Versus Aggregate SizeThe diameter ofa cylindrical specimen or minimum cross-sectional dimensionof a rectangular section shal
24、l be at least three times themaximum size of the coarse aggregate in the SC (see Note).Occasional oversize aggregate particles (of a size not normallyfound in the average aggregate grading) shall be removed byhand picking during the molding of the specimens.NOTE 1The nominal maximum size of coarse a
25、ggregate is that sizenext larger than the largest sieve on which at least 15 % of the aggregateby weight is retained.6.5 Number of SpecimensThe number of specimens andthe number of test batches are dependent on establishedpractice and the nature of the test program. Guidance is usuallygiven in the t
26、est method or specification for which thespecimens are made. Usually, three or more specimens aremolded for each test age and test condition unless otherwisespecified.7. Materials Preparation7.1 Sulfur Polymer CementStore the SPC or its compo-nents in a dry location away from any sources of heat.7.2
27、 Equipment and Materials Temperature :7.2.1 For casting SC specimens, heat the mold, hand tools,and mixing equipment to 240F295F (115145C) unlessotherwise specified by the manufacturer.7.2.2 Until added to the coarse and fine aggregates, the SPCor its components and mineral filler shall remain at am
28、bientroom temperature and not exposed to any sources of heat.7.3 Aggregates:7.3.1 A sufficient amount of coarse aggregate and fineaggregate shall be combined for each batch in the proportionsand in the manner specified by the manufacturer to produce thedesired grading before drying and heating.7.3.2
29、 Before incorporating mineral filler and SPC or itscomponents into the concrete mixer, make sure that the desiredtemperature has been reached and that the final mixturetemperature can be maintained within the allowable range asspecified by the manufacturer.8. Procedure8.1 Mixing Sulfur Polymer Cemen
30、t Concrete:8.1.1 GeneralMix SC according to manufacturers rec-ommendations in a suitable mixer in batches of such size as toleave about 10 % excess after molding the test specimens.Mixing sequence and procedure from batch to batch should notvary unless the effect of such variation is under study.8.2
31、 Making Specimens:8.2.1 Casting Molds Cast specimens as near as practi-cable to the place where they are to be stored during the first 2h. Place molds on a rigid surface free from vibration and otherdisturbances. Avoid jarring, tilting, or damaging of the surfacewhen moving the specimens to the stor
32、age place.8.2.2 CastingPlace SC in the molds using appropriatehand tools and ensure that it is representative of the batch.8.2.2.1 Number of Layers Make the specimens in twoapproximately equal layers of SC, making sure to overfill themold with the second layer.8.3 Consolidation The method of consoli
33、dating shall beas recommended by the manufacturer.8.4 Finishing:8.4.1 Vertically Cooled Cylinders After consolidation,finish the surface of the SC to produce a flat, even surface thatis flush with the overfill rim or extended edge of the mold.8.4.2 Horizontally Cooled Cylinders AlternativeAfterconso
34、lidation, strike off the specimen level with the top of themold, secure the top cap on the mold, and immediately lay thefilled mold in a horizontal position to cool.C1312 97 (2012)29. Conditioning9.1 Sulfur polymer cement concrete shall be conditioned at73 6 4F (23 6 2C) before testing. The time bet
35、ween castingand testing the SC specimens is usually 24 h.10. Keywords10.1 conditioning; molds; sulfur polymer cement (SPC);sulfur polymer cement concrete or sulfur concrete (SC); testspecimensAPPENDIX(Nonmandatory Information)X1. CONSOLIDATION, MIXING, AND OTHER MISCELLANEOUS EQUIPMENTX1.1 Tamping R
36、odsTwo sizes are required for use incasting samples, depending on mold size. Each shall be around, straight, steel rod with at least the tamping end roundedto a hemispherical tip of the same diameter as the rod. Bothends may be rounded if preferred, or an oak handle may beaffixed to one end of the r
37、od for convenience.X1.1.1 Larger Rod,58 in. (16 mm) in diameter and approxi-mately 24 in. (610 mm) long.X1.1.2 Smaller Rod,38 in. (10 mm) in diameter andapproximately 12 in. (305 mm) long for use on molds up to 6in. high.X1.2 MalletsA mallet with a rubber or rawhide headweighing 1.25 6 0.50 lb (0.57
38、 6 0.23 kg) may be required.X1.3 Small ToolsTools and items such as shovels, pails,trowels, oak wood float, blunted trowels, straightedge, feelergage, scoops, rulers, rubber gloves, and metal mixing bowlsmay be required.ASTM International takes no position respecting the validity of any patent right
39、s asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any t
40、ime by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will
41、 receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM
42、 International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).C1312 97 (2012)3
