1、Designation: D 768 01 (Reapproved 2007)Standard Specification forYellow Iron Oxide Hydrated1This standard is issued under the fixed designation D 768; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A num
2、ber in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This specification covers the pigment commerciallyknown
3、as yellow iron oxide, hydrated.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.2. Referenced Documents2.1 ASTM Standards:2D50 Test Methods for Chemical Analysis of Yellow, Or-ange, Red, and Brown Pigments Containing Iron an
4、dManganeseD 185 Test Methods for Coarse Particles in PigmentsD 280 Test Methods for Hygroscopic Moisture (and OtherMatter Volatile Under the Test Conditions) in PigmentsD 1208 Test Methods for Common Properties of CertainPigments3. Composition and Properties3.1 The pigment shall be a manufactured ye
5、llow iron oxideobtained by chemical reaction. It shall be a soft, finelypowdered pigment, free of admixtures of other substances andshall conform to the following requirements:Total hydrated oxide of iron, min, % 93Total oxide of iron,Amin, % 83Loss on ignition,Amax, % 13Moisture and other volatile
6、matter, max, % 1.0Water soluble matter, max, % 0.50Coarse particles (total residue retained on a No. 325(45-m) sieve), max, %0.5Hydrogen ion concentration (pH value) 4.5 to 8.0_ATotal hydrated oxide of iron shall be the sum of iron oxide and loss on ignition.Loss on ignition shall be calculated on t
7、he dry material.3.2 Paste in OilThe paste in oil shall be made bythoroughly grinding the specified pigment with linseed oil(with or without a small amount of volatile thinner) togetherwith (where necessary) small amounts of wetting or dispersingagents to a semipaste or fluid type consistency. As rec
8、eived, itshall not be caked in the container and shall break up readily inoil to form a smooth paint of brushing consistency. It shall mixreadily in all proportions, without curdling, with linseed oil,turpentine, or volatile petroleum spirits, or any mixtures ofthese substances. The paste shall conf
9、orm to the followingrequirements:Pigment, min, % 55Nonvolatile vehicle, min, % of vehicle 80Moisture by distillation, max, % 2.0Coarse particles and skins (total residue retained on aNo. 325 (45-m) sieve), max, percent of the drypigment1.0Consistency by the Stormer viscometer:At shearing rate of 100
10、 revolutions/30 s, min, g 700AAt shearing rate of 100 revolutions/35 s, max, g 1200B_AEquivalent to a rating of 125 Krebs Units.BEquivalent to a rating of 145 Krebs Units.3.3 The mass color character of the tint and the tintingstrength formed by a mixture with a white pigment shall bewithin mutually
11、 agreed upon limits of a standard acceptable toboth the purchaser and the seller.4. Sampling4.1 Two samples shall be taken at random from differentpackages from each lot, batch, days pack, or other unit ofproduction in a shipment. When no markings distinguishingbetween units of production appear, sa
12、mples shall be takenfrom different packages in the ratio of two samples for each4540 kg or 10 000 lb, except that for shipments of less than10 000 lb, two samples shall be taken. At the option of thepurchaser, the samples may be tested separately or afterblending in equal quantities the samples from
13、 the sameproduction unit to form a composite sample.5. Test Methods5.1 GeneralTests shall be conducted in accordance withthe appropriate ASTM test methods. Test procedures notcovered by ASTM test methods shall be mutually agreed uponbetween the purchaser and the seller.5.1.1 Chemical AnalysisTest Me
14、thods D50.5.1.2 Coarse Particles in PigmentsTest Methods D 185.5.1.3 Moisture in PigmentsTest Methods D 280.1This specification is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.31 on Pigment
15、Specifications.Current edition approved Nov. 1, 2007. Published November 2007. Originallyapproved in 1944. Last previous edition approved in 2001 as D 768 01.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of A
16、STMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.5.1.4 Water Soluble MatterTest Methods D 1208.5.1.5 Hydrogen Ion ConcentrationTest Metho
17、ds D 1208.5.1.6 Pigment and Linseed Oil in Paste in OilTest Meth-ods D 1208.6. Keywords6.1 hydrated; pigment; yellow iron oxideASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are
18、expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not re
19、vised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you
20、may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D 768 01 (2007)2
