1、Designation: D3115 95 (Reapproved 2014)Standard Test Method forExplosive Reactivity of Lubricants with Aerospace AlloysUnder High Shear1This standard is issued under the fixed designation D3115; the number immediately following the designation indicates the year oforiginal adoption or, in the case o
2、f revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method is used to evaluate for explosivereactivity of various lubricants in the pres
3、ence of aerospacealloys under high shear conditions.1.2 The values stated in SI units are to be regarded as thestandard. In cases where materials, products, or equipment areavailable in inch-pound units only, SI units are omitted.1.3 This standard is used to measure and describe theresponse of mater
4、ials, products, or assemblies to heat andflame under controlled conditions, but does not by itselfincorporate all factors required for fire hazard or fire riskassessment of the materials, products, or assemblies underactual fire conditions.1.4 This standard does not purport to address all of thesafe
5、ty concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2B209 Specification for Aluminum
6、and Aluminum-AlloySheet and PlateB221 Specification for Aluminum and Aluminum-Alloy Ex-truded Bars, Rods, Wire, Profiles, and Tubes2.2 ANSI Standard:B46.1 Surface Texture33. Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 explosive reactivity, noccurrence of sparks, smoke,or expl
7、osive (audible) sounds during this test.3.1.2 lubricants, nliquid materials used as lubricants orcutting fluids in the presence of aerospace alloys.4. Summary of Test Method4.1 A shaped dowel pin made of the test material is rotatedat 1760 rpm under a pressure of 689 MPa (1000 psi) for 1 minin a sha
8、ped hole (drilled into a block of the test material)containing the test lubricant. Observation for indications ofreaction is made.5. Significance and Use5.1 Explosive reactivity has resulted when parts made fromsome light alloys, typically high in aluminum and magnesium,are loaded under shear condit
9、ions while in contact with certainlubricants.Atypical example is a threaded part, lubricated witha chlorofluorocarbon grease, pulled up normally tight.6. Apparatus6.1 Fluted Ball-End End Mills,4two, 12.7 6 0.025 mm(0.500 6 0.001 in.) in diameter with a 6.35 6 0.025-mm(0.2506 0.001-in.) radius tip, f
10、inished to 0.203 to 0.406 m (8to 16 in.) rms.6.2 Drill Press, capable of rotating at 1760 rpm under a6.89-MPa (1000-psi) load.6.3 Drill Chuck, capacity 12.7-mm (12-in.) end mill.6.4 Loading Device, capable of putting a pressure of 6.89MPa (1000 psi) on the dowel test pin.6.5 Force Gauge, 1112 N (250
11、-lbf) force.51This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility ofSubcommittee D02.L0.07 on Engineering Sciences of High Performance Fluids andSolids (Formally D02.1100). ASTM Committee F07 on Aerospac
12、e and Aircraftmaintains a continued interest in this test method and will make use of it in thefuture.Current edition approved Dec. 1, 2014. Published February 2015. Originallyapproved in 1972. Last previous edition approved in 2009 as D3115 95 (2009).DOI: 10.1520/D3115-95R14.2For referenced ASTM st
13、andards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Available from American National Standards Institute (ANSI), 25 W. 43rd St.,4th Flo
14、or, New York, NY 10036, http:/www.ansi.org.4Carbide tipped ball-end end mills are available and may be used when workingwith metals harder than aluminum.5The sole source of supply of the gauge known to the committee at this time isAMETEK, Inc., Testing Equipment Div., Box 288, Lansdale, PA 19446. If
15、 you areaware of alternative suppliers, please provide this information to ASTM Interna-tional Headquarters. Your comments will receive careful consideration at a meetingof the responsible technical committee,1which you may attend.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, Wes
16、t Conshohocken, PA 19428-2959. United States16.6 Drill Press Vise, capable of holding the test block inposition.6.7 Surface Texture Standards, conforming to AmericanNational Standard for Surface Texture (ANSI B46.1).6.8 Transparent Safety Shield.6.9 Thermocouple and Potentiometer , optional, for mea
17、sur-ing hole-bottom temperature.6.10 Desiccator, maintained at 50 6 5 % relative humidity.Water saturated with Ca(NO3)24H2O at 294 K (70F) issatisfactory.7. Materials7.1 Blocks, of the appropriate alloy, 25.4 mm (1 in.) thick by38 mm (1.5 in.) wide by 165 mm (6.5 in.) long. Unlessotherwise specified
18、, use metal conforming to SpecificationB209, Grade 2024-T4.7.2 Dowel Pins, of the appropriate alloy, 6.35 6 0.025 mm(0.250 6 0.001 in.) in diameter by 76 6 2.5 mm (3.0 6 0.1 in.)long and the end having a hemispherical surface with a 6.35 60.025 mm (0.250 6 0.01-in.) radius and an 0.203 to 0.406 m(8
19、to 16-in.) finish. Unless otherwise specified, use metalconforming to Specification B221, Grade 2024-T4.NOTE 1Both ends of each dowel pin may be so prepared and eachconsidered a new test pin under 9.8 provided that the dimensions aremaintained as required.7.3 Acetone, reagent grade.67.4 Test Lubrica
20、nt, sufficient for at least one test series (thatis, 6 mL).8. Test Specimen8.1 Prepare the block, as shown in Fig. 1, by drilling sixholes with the 12.7 mm (0.500-in.) ball-end end mill to a depthof 12.7 mm 6 0.254 mm (0.500 6 0.100 in.) measured to thetip of the hole. The hole centers shall not be
21、less than 12.7 mm(0.500 in.) from the edge of the block or another hole. The ballend mill will create the correct surface finish in the hole whendriven at 500 to 600 rpm with no lubricant.8.1.1 If it is desired to determine the temperature attainedduring the test, a thermowell shall be cross-drilled
22、 to a point6Reagent Chemicals, American Chemical Society Specifications, AmericanChemical Society, Washington, DC. For Suggestions on the testing of reagents notlisted by the American Chemical Society, see Annual Standards for LaboratoryChemicals, BDH Ltd., Poole, Dorset, U.K., and the United States
23、 Pharmacopeiaand National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,MD.mm in.0.254 0.0106.35 0.25012.7 0.500FIG. 1 Block, Drilled for TestsD3115 95 (2014)2directly under the hole tip 60.127 mm (60.005 in.) with ametal thickness between holes of 0.127 6 0.025 mm (0.005 60.001 i
24、n.), using a No. 80 0.343 mm (0.135 in.) drill. Abare-tipped thermocouple made from iron and constantan wiresofNo.40B that is, 295 to 301 K (72to 82F).9.6 Lower the dowel pin to the bottom of the hole.9.7 Apply the load to the dowel pin.9.8 Position the safety shield.9.9 Start the motor on the drill
25、 press and run the test underload for 60 6 5 s, or until reaction is evident, and stop whilestill loaded.9.10 During the test period, observe the hole for sparks,smoke, and explosive (audible) sounds.9.11 After terminating the run, release the load and examinethe residue for changes in appearance. R
26、ecord the results.9.12 Repeat 9.5 9.8 to a total of six runs, using a new holeand dowel-end for each test.10. Report10.1 Report the materials used for the dowel pin and blockand the identification of the lubricant being tested.10.2 Report the number and type of reactions for each run ofthe series. T
27、able 1 illustrates a typical report.11. Precision and Bias11.1 PrecisionThe precision of this test method as deter-mined by the statistical examination of interlaboratory testresults involving five laboratories and nine samples is asfollows:11.1.1 RepeatabilityDuplicate results obtained by thesame o
28、perator with the same apparatus under constant operat-ing conditions on identical test material would, in the long run,in the normal and correct operation of the test method exceedmore than one reaction per set of six runs only in one case intwenty.11.1.2 ReproducibilityThe difference between indepe
29、n-dent results obtained by different operators working in differentlaboratories on identical test material would, in the long run,exceed a difference of 108 % of the mean number of reactionsonly in one case in twenty.11.2 BiasNo statement is made about the bias of this testmethod since the results c
30、annot be compared to any form of astandard value.12. Keywords12.1 aerospace alloys; explosive reactivity; lubricants; reac-tivity; shearTABLE 1 Typical ReportSample No. Date X/Y/69 Dowel 2024-T4 Block 2024-T4 Lubricant Grease XYZ (Lot No.) Received X/Z/69Run Sparks Bangs Smoke Residue Reaction Time,
31、 s Remarks1 3 1 black darkened 192 0 0 white unchanged no reaction3 1 1 (weak) gray darkened 504 5 0 gray slightly dark 605 2 2 (weak-1) black darkened 306 1 1 black darkened 20D3115 95 (2014)3ASTM International takes no position respecting the validity of any patent rights asserted in connection wi
32、th any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible tech
33、nical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful considerat
34、ion at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Ha
35、rbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 95 (2014)4
