1、Designation: D 4970 05 (Reapproved 2007)e1Standard Test Method forPilling Resistance and Other Related Surface Changes ofTextile Fabrics: Martindale Tester1This standard is issued under the fixed designation D 4970; the number immediately following the designation indicates the year oforiginal adopt
2、ion or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.e1NOTEFootnote 3 was editorially corrected in August 2007.1. Scope1.1 This test meth
3、od covers the determination of the resis-tance to the formation of pills and other related surface changeson textile fabrics using the Martindale tester. The proceduregenerally is applicable to all types of fabrics, being particularlysuitable for woven fabrics.NOTE 1For other methods, if testing the
4、 pilling resistance of textiles,refer to Test Methods D 3511, D 3512, and D 3514.1.2 This test method is not suitable for fabrics thicker than3 mm (0.125 in.) because such fabrics cannot be mounted inthe specimen holder.1.3 The fabric may be laundered or dry cleaned beforetesting.1.4 The values stat
5、ed in SI units are to be regarded as thestandard. The values given in parentheses are provided forinformation only.1.5 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate
6、safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D 123 Terminology Relating to TextilesD 2514 Discontinued 1977; Tolerances for Fabrics Wovenfrom All-Cotton or from Cotton Man-Made Fiber Blends3D 3511 Test
7、Method for Pilling Resistance and Other Re-lated Surface Changes of Textile Fabrics: Brush PillingTesterD 3512 Test Method for Pilling Resistance and Other Re-lated Surface Changes of Textile Fabrics: Random TumblePilling Tester3. Terminology3.1 DefinitionsFor definitions of other textile terms used
8、in this test method, refer to Terminology D 123.3.2 Description of Terms Specific to This Standard:3.2.1 cycle, nin the Martindale tester, the sixteen move-ments required to complete one Lissajous figure.3.2.2 fuzz, nuntangled fiber ends that protrude from thesurface of a yarn or fabric.3.2.3 moveme
9、nt, none rotation of the outer gearing of theMartindale tester.3.2.4 pilling resistance, nresistance to formation of pillson the surface of a textile fabric.3.2.5 pills, nbunches or balls of tangled fibers, which areheld to the surface of a fabric by one or more fibers.4. Summary of Test Method4.1 P
10、illing and other changes in the surface appearance,such as fuzzing, that occur in normal wear are simulated on alaboratory testing machine. Fabrics are mounted on the Mar-tindale Tester, and the face of the test specimen is rubbedagainst the face of the same mounted fabric in the form of ageometric
11、figure, that is, a straight line, which becomes agradually widening ellipse, until it forms another straight linein the opposite direction and traces the same figure again underlight pressure for a specific number of movements. The degreeof fabric pilling or surface appearance change produced by thi
12、saction is evaluated by comparison of the tested specimen withvisual standards that may be actual fabrics, or photographs offabrics, showing a range of pilling resistance. The observedresistance to pilling is reported using an arbitrary rating scale.5. Significance and Use5.1 Acceptance TestingThis
13、method of testing fabricsresistance to pilling is not recommended for acceptance testing.If it is used for acceptance testing, it should be used withcaution because interlaboratory data are not available. In somecases the purchaser or supplier may have to test a commercial1This test method is under
14、the jurisdiction of ASTM Committee D13 on Textilesand is the direct responsibility of Subcommittee D13.60 on Fabric Test Methods,Specific.Current edition approved July 1, 2007. Published August 2007. Originallyapproved in 1999. Last previous edition approved in 2005 as D 4970 05.2For referenced ASTM
15、 standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Withdrawn.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, Wes
16、t Conshohocken, PA 19428-2959, United States.shipment of one or more specific materials by the best availablemethod even though the method has not been recommended foracceptance testing. Although this test method is not recom-mended for acceptance testing, it is useful because it is usedwidely outsi
17、de the United States.5.2 If there is a disagreement arising from differences invalues reported by the purchaser and the supplier when usingthis test method, the statistical bias, if any, between thelaboratory of the purchaser and the laboratory of the suppliershould be determined with comparison bei
18、ng based on testingspecimens randomly drawn from one sample of material of thetype being evaluated. Competent statistical assistance is rec-ommended for the investigation of bias. A minimum of twoparties should take a group of test specimens, which are ashomogeneous as possible and which are from a
19、lot of materialof the type in question. The test specimens then should beassigned randomly in equal numbers to each laboratory fortesting. The average test results from the two laboratoriesshould be compared using an acceptable statistical protocol andprobability level chosen by the two parties befo
20、re the testing isstarted. Appropriate statistical disciplines for comparing datamust be used when the purchaser and supplier cannot agree. Ifa bias is found, either its cause must be found and corrected, orthe purchaser and the supplier must agree to interpret futureresults with consideration for th
21、e known bias.5.3 The pilling of textile fabrics is a very complex propertybecause it is affected by many factors that include: type of fiberor blends, fiber dimensions, yarn and fabric construction, andfabric finishing treatments. The pilling resistance of a specificfabric in actual wear varies more
22、 with general conditions of useand individual wearers than in replicate fabric specimenssubjected to controlled laboratory tests. This experience shouldbe borne in mind when adopting levels of acceptability for aseries of standards.5.4 Finishes and fabric surface changes may exert a largeeffect on p
23、illing. It is recommended that fabrics be tested afterlaundering or drycleaning, or both. Testing before refurbishingalso may be advisable. Prior agreement between interestedparties should determine the state of the test.5.5 Pills vary appreciably in size and appearance anddepend on the presence of
24、lint and degree of color contrast.These factors are not evaluated when pilling is rated solely onthe number of pills. The development of pills may be accom-panied by other surface phenomena, such as loss of cover,color change, or the development of fuzz. Since the overallacceptability of a specific
25、fabric is dependent on both thecharacteristics of the pills and the other factors affecting thesurface appearance, it is suggested that fabrics tested in thelaboratory be evaluated subjectively with regard to theiracceptability and not rated solely on the number of pillsdeveloped.Aseries of standard
26、s, based on graduated degrees ofsurface change of the fabric type being tested, may be set up toprovide a basis for subjective ratings. The visual standards aremost advantageous when the laboratory test specimens corre-late closely in appearance with worn fabrics and show a similarratio of pills to
27、fuzz. Counting the pills and weighing theirnumber with respect to their size and contrast, as a combinedmeasure of pilling resistance, is not recommended because ofthe excessive time required for counting, sizing, and calcula-tion.5.6 The degree of fabric pilling is evaluated by comparingthe tested
28、specimens with visual standards, which may beactual fabrics or photographs of fabrics, showing a range ofpilling resistance. The observed resistance to pilling is reportedon an arbitrary scale ranging from 5 to 1 (no pilling to verysevere pilling).5.7 This test method is applicable to a wide variety
29、 ofwoven and knitted fabrics that vary in pilling propensity as aresult of variations in fiber, yarn and fabric structure, andFIG. 1 Martindale Abrasion TesterFIG. 2 Apparatus for Fabric EvaluationD 4970 05 (2007)e12finish. The applicability of this test method to nonwovenfabrics has not been determ
30、ined.6. Apparatus and Materials6.1 Martindale Tester4(see Fig. 1).6.2 Standard Felt, of mass 750 6 50 g/m2(22 6 1.5 oz/yd2)and 3 6 0.3 mm (0.12 6 0.01 in.) thick.6.3 Apparatus for Fabric Evaluation Facilities for illumi-nation (cool white fluorescent tube) and simultaneous viewingtest specimens and
31、fabric or photographic rating standards.Apparatus and options for visual evaluation are listed in Table1.6.4 Standard In-House Pilling Test Fabric, having an estab-lished pilling resistance rating for checking machine perfor-mance. No universal standard fabric is available. Each testfacility must de
32、cide on an appropriate fabric.6.5 Rating Standards:6.5.1 Fabric, a series of tested specimens of a specific fabrictype, which show degrees of pilling or other distortion, or both,for the fabric to be tested. Store the fabric rating standards andhandle them under conditions that will preserve their o
33、riginalform and appearance. Mounting with thick cardboard framingaround the specimens is recommended.6.5.2 PhotographicA set of five photographs 105 mm(.125 in.), numbered 1 to 5, illustrating varying degrees ofpilling from “very severe pilling” to “no pilling.”56.5.3 Digital imaging and/or rating s
34、ystem.6.6 Fabric Punches or Press Cutters, 38 mm (1.5 in.) and140 mm (5.5 in.) in diameter.6.7 Facilities for Laundering Samples, if needed.6.8 Facilities for Drycleaning Samples, if needed.7. Sampling7.1 Primary Sampling UnitConsider rolls of fabric orfabric components of fabricated systems to be t
35、he primarysampling unit, as applicable.7.2 Laboratory Sampling UnitFrom each primary sam-pling unit take one full-width piece of fabric that is 1 m (1 yd)in length along the selvage (machine direction), after firstremoving a 1 m (1 yd) length. For fabric components offabricated systems use the entir
36、e system,8. Test Specimens: Selection, Number, and Preparation8.1 Unless otherwise specified, samples should be washedor drycleaned before cutting the test specimens. Conditionsappropriate for the fabric end-use or conditions agreed upon byinterested parties should be used.8.2 Cut a pair of circular
37、 specimens from each swatch in thelaboratory sample with one of each pair of specimens being 38mm (1.5 in.) in diameter and the other 140 mm (5.5 in.) indiameter.8.3 Take the specimens evenly-spaced across the width ofthe laboratory sample or from two different panels in agarment. Specimens should b
38、e staggered in such a manner thatno specimens contain the same yarns. Avoid areas withwrinkles and other distortions. Unless otherwise specified, donot cut specimens nearer the selvage less than110 of the widthof the fabric.9. Preparation of Apparatus9.1 Maintenance CheckFollow instruction manual fo
39、rproper maintenance of apparatus.10. Conditioning10.1 Condition specimens in the standard atmosphere fortesting textiles, which is 21 6 1C (70 6 20F) and 65 % RH6 2 % relative humidity for at least 4 h prior to testing.11. Procedure11.1 Make all tests in the standard atmosphere for testingtextiles.1
40、1.2 Mount one 140-mm (5.5-in.) diameter of standard feltand one fabric specimen on each table (see Fig. 1). Place one38-mm (1.5-in.) diameter disk of 3-mm polyurethane foam anda specimen of the same fabric in each of the holders, makingsure the face of the fabric is exposed for both specimens.11.3 P
41、lace the specimen holders on the same table as theother fabric specimen and insert a spindle into each specimenholder to give a pressure on the larger specimen of approxi-mately 3 kPa (0.44 psi). This pressure is the same as any othersetup but without additional weights.11.4 Start the machine and al
42、low it to run for 100 move-ments.12. Evaluation12.1 Place the 38-mm (1.5-in.) disk specimen squarely onthe double-faced tape in the viewing cabinet (see Fig. 2).12.1.1 Using the viewing apparatus and options selectedfrom Table 1 and either suitable fabric or photograpic standards(6.5), subjectively
43、rate the face of each specimen, using therating standards and the following scale (Note 2):5no pilling4slight pilling3moderate pilling2severe pilling1very severe pillingNOTE 2If the test method is to be used as a referee method, aminimum of two graders, the agreed-upon standards, and the viewing4App
44、aratus and accessories are available commercially.5Available from ASTM International Headquarters. Order Adjunct No.ADJD3512.TABLE 1 Viewing Apparatus and OptionsApparatus Specimen PreparationASTM Lightbox (Fig. 2)A0.78 rad (45)LightboxB0.78 rad (45)LightboxBflatLightboxBcritical angleAs determined
45、by the buyer and supplierAThe source of supply of the apparatus known to the committee at this time isStandard Scientific Supply Co., 601 West Market Street, Bethlehem, PA180185208. If you are aware of alternate suppliers, please provide this informa-tion to ASTM Headquarters. Your comments will rec
46、eive careful consideration at ameeting of the responsible technical committee, which you may attend.BAvailable commercially.D 4970 05 (2007)e13apparatus and option selected from Table 1 for fabric evaluation shall beused.12.1.2 A digital imaging or rating system may be used asagreed upon by the purc
47、haser and supplier.12.1.3 Average the rating for each laboratory sampling unitand for the lot.13. Report13.1 State that the specimens were tested as directed in TestMethod D 4970. Describe the material or product sampled andthe method of sampling used.13.2 Report the following information:13.2.1 Rat
48、ings of each individual specimen for pilling, theaverage rating of the four specimens from each laboratorysampling unit, and the average for the lot.13.2.2 If the fabric was washed before testing, launderingconditions used.13.2.3 If the fabric was drycleaned before testing, condi-tions used.13.2.4 N
49、umber of movements.13.2.5 Type of viewing apparatus, viewing option, andrating standard used.14. Precision and Bias14.1 PrecisionTwo fabrics were evaluated on each of twodays by two operators.Fabric #1day #1 day #2operator 1 operator 2 operator 1 operator 24.0 4.0 3.5 4.03.5 4.5 4.0 4.04.0 4.0 4.0 4.54.0 4.5 4.0 4.54.0 4.5 4.0 4.5Fabric #2day #1 day #2operator 1 operator 2 operator 1 operator 23.0 3.0 3.0 3.03.5 3.5 3.0 3.03.0 3.0 3.0 3.53.0 3.5 4.5 3.53.0 3.0 4.0 3.5The reproducibility of this test method is being determinedand will be made available.14.
