1、Designation: D5267 97 (Reapproved 2012)Standard Test Method forDetermination of Extrudability of Cartridge Adhesives1This standard is issued under the fixed designation D5267; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the yea
2、r of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method measures the amount of force neces-sary to extrude an adhesive from a cartridge at a giventemper
3、ature.1.2 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any
4、, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D907 Terminology of Adhesives3. Terminology3.1 Defi
5、nitionsMany terms in this test method are definedin Terminology D907.4. Significance and Use4.1 Cartridge adhesives are typically used at job sites in awide variety of temperature ranges. These products may beexposed to cold temperatures, where one of the limitingapplication factors is whether the p
6、roduct can be extruded fromthe cartridge.4.2 The test method quantitatively measures the force nec-essary to extrude a cartridge adhesive at a given temperature.This provides the formulator with results that can assist informulation development and the end user with information foruse in selecting a
7、 product for general usage.4.3 By measuring (the ease of) extrusion from the cartridge,the test method can also be used as a quality control tool tomeasure the shelf life stability of a product.5. Apparatus5.1 The test fixture is shown in Fig. 1. Details are shown inFigs. 2-4.3Make the framework fro
8、m aluminum. Make the rodand plunger combination from steel.1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of Subcommittee D14.10 on WorkingPropertiesCurrent edition approved May 1, 2012. Published May 2012. Originallyapproved in 1992. L
9、ast previous edition approved in 2005 as D5267 97 (2005).DOI: 10.1520/D5267-97R12.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary pag
10、e onthe ASTM website.3The apparatus is also available from Browning Technology, Inc., 1256 StanleyAve., Dayton, OH 45404.FIG. 1 Test Fixture for Measuring Extrusion from Cartridge1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.5.2 Th
11、e test fixture is designed to be fitted onto a testmachine capable of measuring compressive strength.6. Conditioning6.1 Before measuring extrudability, condition the cartridgefilled with adhesive until it reaches the desired constanttemperature.7. Procedure7.1 Mount the test fixture to the test mach
12、ine for stability.7.2 After conditioning the cartridge, cut off enough of thetip, perpendicular to the cartridge, to ensure an inside diameterof14 in. (6.3 mm). If the cartridge has a foil or plastic liner,puncture it completely to allow passage of the material throughthe orifice. Record the tempera
13、ture of the adhesive by insertinga thermometer or suitable thermocouple into the cartridge.7.3 Set the crosshead speed to 5.0 in. (127.0 mm) per min oranother acceptable rate.7.4 Activate the machine to begin extrusion of the adhesivefrom the cartridge, measure the maximum force necessary tobegin th
14、e extrusion process as well as the force necessary tomaintain continued extrusion of the adhesive. The first value isthe force needed to release the plunger from the cartridge. Thesecond value is the force needed to extrude the adhesive fromthe cartridge continuously.8. Report8.1 Report the followin
15、g information:8.1.1 Complete identification of the adhesive, includingtype, source, date of test, etc.8.1.2 Complete identification of the cartridge, includingtype, composition, liner used, plunger design, source, size, etc.8.1.3 Temperature of adhesive.8.1.4 Crosshead speed used for extrusion.8.1.5
16、 Force (in psi) used initially to extrude the adhesivefrom the cartridge and the average to maintain a constant flowof adhesive.9. Precision and Bias9.1 Precision:9.1.1 Table 1 presents round robin data generated from threelaboratories. Three different cartridge adhesives were used togenerate the da
17、ta at two temperatures. The extrudability valueswere based on the average of three separate cartridge values.9.1.2 Repeatability at a given test site for the samplesyielded coefficients of variation from 2 to 18 % for Laboratory1, 1 to 10 % for Laboratory 2, and 2 to 13 % for Laboratory 3,with most
18、values in the range of 2 to 11 %.9.1.3 No statement of reproducibility from site to site isavailable at this time.9.2 BiasBias is the difference between the true forcenecessary to extrude an adhesive from a cartridge and the forcemeasured by a repeatable method. Bias arises from the consis-tency of
19、the adhesive packaged in the cartridge, the method bywhich the plunger is assembled into the cartridge, and insidediameter variations that may exist when the cartridge tip is cut.10. Keywords10.1 adhesive; cartridge; extrusionFIG. 2 Base Support for Test FixtureFIG. 3 Cartridge Brace and Rear Suppor
20、t AssemblyD5267 97 (2012)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infrin
21、gement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard
22、 or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views
23、 known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting
24、 ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).FIG. 4 Rod and Follower Plate AssemblyTABL
25、E 1 Cartridge Extrudability (in psi) for CartridgeAdhesivesRound Robin ResultsLaboratory1ALaboratory2BLaboratory3CRoom Temperature, 73 6 2F(236 1C)Adhesion A 67 6 3586 1416 1Adhesion B 118 6 15 41 6 1346 1Adhesion C 70 6 13 31 6 3206 1Low TemperatureAdhesion A 70 6 10D67 6 2E53 6 2FAdhesion B 178 6 8496 3436 3Adhesion C 128 6 2886 1 133 6 17ATested on an Instron 1120 machine.BTested on an Instron 1125 machine.CTested on a Thwing-Albert machine.DTested at 50 6 2F (10 6 1C).ETested at 45 6 2F (7 6 1C).FTested at 42 6 2F (5 6 1C).D5267 97 (2012)3
