1、Designation: D5396 04 (Reapproved 2015)Standard Specification forReclaimed Perchloroethylene1,2This standard is issued under the fixed designation D5396; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A
2、number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the grade of perchloroethylenetypically needed in various industries for noncriticalapplications, such as in
3、metal cleaning formulations. It is notrecommended for dry cleaning applications (see SpecificationD4081). It may be used as a reference document by purchasersor by persons establishing in-house perchloroethylene recoveryprograms.2. Referenced Documents2.1 ASTM Standards:3D2108 Test Method for Color
4、of Halogenated OrganicSolvents and Their Admixtures (Platinum-Cobalt Scale)D2109 Test Methods for Nonvolatile Matter in HalogenatedOrganic Solvents and Their AdmixturesD2111 Test Methods for Specific Gravity and Density ofHalogenated Organic Solvents and Their AdmixturesD2942 Test Method for Total A
5、cid Acceptance of Haloge-nated Organic Solvents (Nonreflux Methods)D2988 Test Methods for Water-Soluble Halide Ion in Halo-genated Organic Solvents and Their AdmixturesD2989 Test Method for Acidity-Alkalinity of HalogenatedOrganic Solvents and Their AdmixturesD3401 Test Methods for Water in Halogena
6、ted OrganicSolvents and Their AdmixturesD3741 Test Methods for Appearance of Admixtures Con-taining Halogenated Organic SolventsD4081 Specification for Drycleaning-Grade Perchloroethyl-eneD6806 Practice for Analysis of Halogenated Organic Sol-vents and Their Admixtures by Gas ChromatographyE1064 Tes
7、t Method for Water in Organic Liquids by Coulo-metric Karl Fischer Titration2.2 Government Documents:429 CFR 1910.1200 Department of Labor, OSHA Regula-tions on Hazard Communication49 CFR 100 to 199 Department of Transportation HazardousMaterials Regulations3. Classification3.1 Type IGenerally recog
8、nized for use in precision ap-plications.3.2 Type IIUse for less demanding precision applications.3.3 Type IIIGeneral-purpose technical grade.4. Properties4.1 Reclaimed perchloroethylene, Type I, shall meet therequirements of Table 1.4.2 Reclaimed perchloroethylene, Type II, shall meet therequiremen
9、ts of Table 1.4.3 Reclaimed perchloroethylene, Type III, shall meet therequirements of Table 1.5. Packaging and Package Marking5.1 Industrial or commercial quantities shall be packagedand labeled in accordance with DOT regulations as found in49 CFR 100 to 199, in accordance with state and localregul
10、ations, and in accordance with OSHAregulations found in29 CFR 1910.1200.6. Keywords6.1 halogenated solvent; perchlor; perchloroethylene, TypesI, II, and III; perk; reclaimed1This specification is under the jurisdiction of ASTM Committee D26 onHalogenated Organic Solvents and Fire Extinguishing Agent
11、s and is the directresponsibility of Subcommittee D26.02 on Vapor Degreasing.Current edition approved June 1, 2015. Published June 2015. Originallyapproved in 1993. Last previous edition approved in 2010 as D5396 04(2010).DOI: 10.1520/D5396-04R15.2Tetrachloroethylene: CAS #127-18-4.3For referenced A
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17、e, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.or
18、g). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 PropertiesProperty Specification Test MethodType I Type II Type IIISpecific gravity, 25/25 1.60 to 1.62 1.60 to 1.62 1.59 to 1.
19、62 D2111Chloride, ppm, max 1.0 1.0 1.0 D2988Nonvolatile residue, ppm, max 10 20 25 D2109Water, ppm, max 25 50 100 D3401 or E1064Assay, weight % 99.5 99.0 97.0 D68061,1,1-Trichloroethane content,weight %, max0.02 0.05 0.5 D6806Color, Pt-Co, max 10 10 25 D2108Appearance clear and free fromsuspended matterclear and free fromsuspended matterclear and free fromsuspended matterD3741Acid acceptance, as NaOH,weight %, min0.16 0.16 0.16 D2942Acidity, as HCl, ppm, max 1.0 1.0 1.0 D2989D5396 04 (2015)2
