1、Designation: D 5396 04Standard Specification forReclaimed Perchloroethylene1, 2This standard is issued under the fixed designation D 5396; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in paren
2、theses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the grade of perchloroethylenetypically needed in various industries for noncritical applica-tions, such as in metal cleani
3、ng formulations. It is not recom-mended for dry cleaning applications (see SpecificationD 4081). It may be used as a reference document by purchasersor by persons establishing in-house perchloroethylene recoveryprograms.2. Referenced Documents2.1 ASTM Standards:3D 2108 Test Method for Color of Halog
4、enated OrganicSolvents and Their Admixtures (Platinum-Cobalt Scale)D 2109 Test Methods for Nonvolatile Matter in Haloge-nated Organic Solvents and Their AdmixturesD 2111 Test Methods for Specific Gravity of HalogenatedOrganic Solvents and Their AdmixturesD 2942 Test Method for Total Acid Acceptance
5、of Haloge-nated Organic Solvents (Nonreflux Methods)D 2988 Test Method for Water-Soluble Halide Ion in Halo-genated Organic Solvents and Their AdmixturesD 2989 Test Method for Acidity-Alkalinity of HalogenatedOrganic Solvents and Their AdmixturesD 3401 Test Methods for Water in Halogenated OrganicSo
6、lvents and Their AdmixturesD 3741 Test Method for Appearance of Admixtures Con-taining Halogenated Organic SolventsD 4081 Specification for Drycleaning-Grade Perchloroeth-yleneD 6806 Practice for Analysis of Halogenated Organic Sol-vents and Their Admixtures by Gas ChromatographyE 1064 Test Method f
7、or Water in Organic Liquids byCoulometric Karl Fischer Titration2.2 Other Documents:29 CFR 1910.1200 Department of Labor, OSHA Regula-tions, Hazard Communication449 CFR 100 to 199 Department of Transportation Hazard-ous Materials Regulations43. Classification3.1 Type IGenerally recognized for use in
8、 precision ap-plications.3.2 Type IIUse for less demanding precision applications.3.3 Type IIIGeneral-purpose technical grade.4. Properties4.1 Reclaimed perchloroethylene, Type I, shall meet therequirements of Table 1.4.2 Reclaimed perchloroethylene, Type II, shall meet therequirements of Table 1.4.
9、3 Reclaimed perchloroethylene, Type III, shall meet therequirements of Table 1.5. Packaging and Package Marking5.1 Industrial or commercial quantities shall be packagedand labeled in accordance with DOT regulations as found in 49CFR 100 to 199, in accordance with state and local regulations,and in a
10、ccordance with OSHA regulations found in 29 CFR1919.1200.6. Keywords6.1 halogenated solvent; perchlor.; perchloroethylene,Types I, II, and III; perk; reclaimed1This specification is under the jurisdiction of ASTM Committee D26 onHalogenated Organic Solvents and Fire Extinguishing Agents and is the d
11、irectresponsibility of Subcommittee D26.02 on Vapor Degreasing.Current edition approved Jan. 1, 2004. Published March 2004. Originallyapproved in 1993. Last previous edition approved in 2000 as D 5396 00.2Tetrachloroethylene: CAS #127-18-4.3For referenced ASTM standards, visit the ASTM website, www.
12、astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4Code of Federal Regulations, available from the Superintendent of Documents,Government Printing Office, Washington, DC 2
13、0402.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are express
14、ly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,
15、either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may att
16、end. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States.
17、Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).TABLE 1 PropertiesProperty Specification Test MethodType I Ty
18、pe II Type IIISpecific gravity, 25/25 1.60 to 1.62 1.60 to 1.62 1.59 to 1.62 D 2111Chloride, ppm, max 1.0 1.0 1.0 D 2988Nonvolatile residue, ppm, max 10 20 25 D 2109Water, ppm, max 25 50 100 D 3401 orE 1064Assay, weight % 99.5 99.0 97.0 D 68061,1,1-Trichloroethane content,weight %, max0.02 0.05 0.5 D 6806Color, Pt-Co, max 10 10 25 D 2108Appearance clear and free fromsuspended matterclear and free fromsuspended matterclear and free fromsuspended matterD 3741Acid acceptance, as NaOH,weight %, min0.16 0.16 0.16 D 2942Acidity, as HCl, ppm, max 1.0 1.0 1.0 D 2989D5396042
