ASTM D6751-2007be1 260 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels.pdf
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1、Designation: D 6751 07be1An American National StandardStandard Specification forBiodiesel Fuel Blend Stock (B100) for Middle DistillateFuels1This standard is issued under the fixed designation D 6751; the number immediately following the designation indicates the year oforiginal adoption or, in the
2、case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.e1NOTECorrected EN 14110 mass percent in Table 1 editorially in March 2008.1. Scope*1.1 This specif
3、ication covers biodiesel (B100) Grades S15and S500 for use as a blend component with middle distillatefuels.1.2 This specification prescribes the required properties ofdiesel fuels at the time and place of delivery. The specificationrequirements may be applied at other points in the productionand di
4、stribution system when provided by agreement betweenthe purchaser and the supplier.1.3 Nothing in this specification shall preclude observanceof federal, state, or local regulations which may be morerestrictive.NOTE 1The generation and dissipation of static electricity can createproblems in the hand
5、ling of distillate fuel oils with which biodiesel maybe blended. For more information on the subject, see Guide D 4865.1.4 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.2. Referenced Documents2.1 ASTM Standards:2D93 Test Meth
6、ods for Flash Point by Pensky-MartensClosed Cup TesterD 130 Test Method for Corrosiveness to Copper fromPetroleum Products by Copper Strip TestD 189 Test Method for Conradson Carbon Residue ofPetroleum ProductsD 445 Test Method for Kinematic Viscosity of Transparentand Opaque Liquids (and Calculatio
7、n of Dynamic Viscos-ity)D 524 Test Method for Ramsbottom Carbon Residue ofPetroleum ProductsD 613 Test Method for Cetane Number of Diesel Fuel OilD 664 Test Method forAcid Number of Petroleum Productsby Potentiometric TitrationD 874 Test Method for Sulfated Ash from Lubricating Oilsand AdditivesD 97
8、4 Test Method for Acid and Base Number by Color-Indicator TitrationD 975 Specification for Diesel Fuel OilsD 976 Test Method for Calculated Cetane Index of Distil-late FuelsD 1160 Test Method for Distillation of Petroleum Productsat Reduced PressureD 1266 Test Method for Sulfur in Petroleum Products
9、(Lamp Method)D 1796 Test Method for Water and Sediment in Fuel Oils bythe Centrifuge Method (Laboratory Procedure)D 2274 Test Method for Oxidation Stability of DistillateFuel Oil (Accelerated Method)D 2500 Test Method for Cloud Point of Petroleum ProductsD 2622 Test Method for Sulfur in Petroleum Pr
10、oducts byWavelength Dispersive X-ray Fluorescence SpectrometryD 2709 Test Method for Water and Sediment in MiddleDistillate Fuels by CentrifugeD 2880 Specification for Gas Turbine Fuel OilsD3117 Test Method for WaxAppearance Point of DistillateFuelsD 3120 Test Method for Trace Quantities of Sulfur i
11、n LightLiquid Petroleum Hydrocarbons by Oxidative Microcou-lometry1This specification is under the jurisdiction of ASTM Committee D02 onPetroleum Products and Lubricants and is the direct responsibility of SubcommitteeD02.E0 on Burner, Diesel, Non-Aviation Gas Turbine, and Marine Fuels.Current editi
12、on approved Sept. 15, 2007. Published October 2007. Originallyapproved in 1999 as PS 12199. Adopted as a standard in 2002 as D 675102. Lastprevious edition approved in 2007 as D 675107a.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceas
13、tm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1*A Summary of Changes section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United S
14、tates.D 3242 Test Method for Acidity in Aviation Turbine FuelD 3828 Test Methods for Flash Point by Small Scale ClosedCup TesterD 4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD 4177 Practice for Automatic Sampling of Petroleum andPetroleum ProductsD 4294 Test Method for Sulfur
15、 in Petroleum and PetroleumProducts by Energy-Dispersive X-ray Fluorescence Spec-trometryD 4530 Test Method for Determination of Carbon Residue(Micro Method)D 4737 Test Method for Calculated Cetane Index by FourVariable EquationD 4865 Guide for Generation and Dissipation of StaticElectricity in Petr
16、oleum Fuel SystemsD 4951 Test Method for Determination of Additive Ele-ments in Lubricating Oils by Inductively Coupled PlasmaAtomic Emission SpectrometryD 5453 Test Method for Determination of Total Sulfur inLight Hydrocarbons, Spark Ignition Engine Fuel, DieselEngine Fuel, and Engine Oil by Ultrav
17、iolet FluorescenceD 5773 Test Method for Cloud Point of Petroleum Products(Constant Cooling Rate Method)D 6217 Test Method for Particulate Contamination inMiddle Distillate Fuels by Laboratory FiltrationD 6450 Test Method for Flash Point by ContinuouslyClosed Cup (CCCFP) TesterD 6469 Guide for Micro
18、bial Contamination in Fuels andFuel SystemsD 6584 Test Method for Determination of Free and TotalGlycerin in B-100 Biodiesel Methyl Esters By Gas Chro-matographyD 6890 Test Method for Determination of Ignition Delayand Derived Cetane Number (DCN) of Diesel Fuel Oils byCombustion in a Constant Volume
19、 ChamberD 7039 Test Method for Sulfur in Gasoline and Diesel Fuelby Monochromatic Wavelength Dispersive X-ray Fluores-cence Spectrometry2.2 Government Standard:40 CFR Part 79 Registration of Fuels and Fuel AdditivesSection 211(b) Clean Air Act32.3 Other Documents:4UOP 389 Trace Metals in Oils by Wet
20、 Ashing and ICP-OESUOP 39191 Trace Metals in Petroleum Products or Organ-ics by AASEN 14112 Fat and oil derivativesFatty acid methyl esters(FAME)Determination of oxidation stability (Acceler-ated oxidation test)5EN 14110 Fat and oil derivativesFatty acid methyl esters(FAME)Determination of methanol
21、content5EN 14538 Fat and oil derivativesFatty acid methyl esters(FAME)Determination of Ca, K, Mg and Na content byoptical emission spectral analysis with inductivelycoupled plasma (ICP OES)53. Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 biodiesel, na fuel comprised of mono-al
22、kyl esters oflong chain fatty acids derived from vegetable oils or animalfats, designated B100.3.1.1.1 DiscussionBiodiesel, as defined above, is regis-tered with the U.S. EPA as a fuel and a fuel additive underSection 211(b) of the Clean Air Act. There is, however, otherusage of the term biodiesel i
23、n the marketplace. Due to its EPAregistration and the widespread commercial use of the termbiodiesel in the U.S. marketplace, the term biodiesel will bemaintained for this specification.3.1.1.2 DiscussionBiodiesel is typically produced by areaction of a vegetable oil or animal fat with an alcohol su
24、ch asmethanol or ethanol in the presence of a catalyst to yieldmono-alkyl esters and glycerin, which is removed. The finishedbiodiesel derives approximately 10 % of its mass from thereacted alcohol. The alcohol used in the reaction may or maynot come from renewable resources.3.1.2 biodiesel blend, B
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