1、Designation: E 1617 09Standard Practice forReporting Particle Size Characterization Data1This standard is issued under the fixed designation E 1617; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A numbe
2、r in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.INTRODUCTIONCorrelation and comparison of particle size measurement data are of general importance toresearchers, processors, suppliers, vendors, and us
3、ers of particulate materials. Since there arenumerous methods and devices in use, comparisons of size measurement data are subject to perceivedinconsistencies that may be much reduced by the use of standardized reporting.Data generated by any one size measurement method may be consistent in many res
4、pects, yet betroublesome to correlate due to variances in data processing and reporting formats among equipmentmanufacturers. Data generated from methods employing different physical principles present seriouscorrelation problems due to their sensing of different parameters related to particle size
5、and someunrelated, such as density, shape and optical properties. Standardized reporting may reduce confusionresulting from different particle size measurement practices.1. Scope1.1 This practice covers reporting particle size measurementdata.1.2 This practice applies to particle size measurement me
6、th-ods, devices, detail levels, and data formats for dry powders,and wet suspensions of solids, gels, or emulsion droplets. Thispractice does not pertain to liquid particles.NOTE 1For information on reporting liquid particle measurementdata, refer to Practice E 799.1.3 This practice does not concern
7、 particle concentrationinformation.1.4 This practice uses SI (Systme International) units asstandard. State all numerical values in terms of SI units unlessspecific instrumentation software reports particle size informa-tion, including percentiles, indices, and distributions as tabu-lations and grap
8、hs using alternate units. In this case, presentboth reported and equivalent SI units in the final written report.Refer to Practice E 380 for proper usage of SI units.1.5 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of t
9、he user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2E 177 Practice for Use of the Terms Precision and Bias inASTM Test MethodsE 380 Practice for Use of the In
10、ternational System of Units(SI)3E 456 Terminology Relating to Quality and StatisticsE 691 Practice for Conducting an Interlaboratory Study toDetermine the Precision of a Test MethodE 799 Practice for Determining Data Criteria and Process-ing for Liquid Drop Size Analysis3. Significance and Use3.1 Wh
11、en evaluating the particle size information, if theprocedures of the data processing are not available, the user ofthe data must make assumptions concerning the reported datain the event of analytical inconsistencies. In order for differentdata sets to be compared it is crucial that the parties repo
12、rt theanalytical techniques and methods or procedures for evaluat-ing, calculating, compiling or otherwise processing the data tobe reported.3.2 Particle size characterization information can be re-ported in three levels of detail in order to satisfy users needs.1This practice is under the jurisdict
13、ion of ASTM Committee E29 on Particle andSpray Characterization and is the direct responsibility of Subcommittee E29.02 onNon-Sieving Methods.Current edition approved March 1, 2009. Published April 2009. Originallyapproved in 1994. Last previous edition approved in 2007 as E 1617 97(2007).2For refer
14、enced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Withdrawn.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box
15、 C700, West Conshohocken, PA 19428-2959, United States.3.2.1 Level 1 applies when only basic information about thematerial is required, and shall be provided with each shipment.This level represents the minimum information that shall bereported. Level 1 information may be sufficient in such cases as
16、identifying a certain grade of a material or when detailedknowledge of analytical methodology is not needed.3.2.2 Level 2 presumes the need for knowledge of method-ology on the users part and allows the user to make a moreinformed judgment about the information provided in Level 1.3.2.3 Level 3 prov
17、ides detailed written procedures to allowduplication of the measurement.3.2.4 Information provided through Levels 2 and 3 willallow users to perform comparative material evaluations be-tween several suppliers, set specifications or define a purchaseagreement, perform inter-laboratory studies and mos
18、t impor-tantly resolve disputes between supplier and users.3.3 Reported particle size measurement is a function of boththe actual particle dimension and shape factor as well as theparticular physical or chemical properties of the particle beingmeasured. Caution is required when comparing data fromin
19、struments operating on different physical or chemical param-eters or with different particle size measurement ranges.Sample acquisition, handling and preparation can also affectthe reported particle size results.4. Procedure4.1 The particle size characterization report shall includeLevel 1 informati
20、on with Level 2 or 3, or both, being suppliedupon agreement between supplier and user. Level 2 reportsshall include all information provided in Level 1. Level 3reports shall include all information provided in Levels 1 and2.4.2 The supplier of a product lot shall provide the user withat least Level
21、1 information in a mutually agreed upon timeframe relative to delivery of the product. Structure the reportusing 5.2 through 5.2.8 as guidelines.4.3 Levels 2 and 3 shall be made available to the user atmutually agreeable costs and terms of disclosure. Structure thereports using 5.3 through 5.3.14.3
22、and 5.4 through 5.4.18,respectively, as guidelines.4.4 Particle Size Characterization Data SheetLevel 1:4.4.1 The Level 1 report shall contain the designation of thisASTM standard practice (E 1617).4.4.2 The report shall contain sample identification infor-mation such as material type, sample source
23、 or submitter, andsample lot number.4.4.3 The report shall include a minimum reporting of sizeparameter(s). Minimum reporting will be defined by agreementbetween supplier and user of the data, such as a calculatedmean diameter, median diameter, or both.4.4.4 The report shall include the principle of
24、 measurement,such as sieving, sedimentation, light blockage, electronic zonesensing, laser light scattering, and so forth. Often, the mea-surement principle can be defined by describing the instrumen-tation or apparatus used for the analysis. All references to“diameter” shall include appropriate adj
25、ectives to indicate thesensing basis.4.4.5 The report shall include the bases for the reportedparameters. Examples of parameter basis are frequently distri-bution, scattering area distribution, and mass distribution.4.4.6 The report shall include the range of size measure-ment, in appropriate SI uni
26、ts.4.5 Particle Size Characterization Data SheetLevel 2:4.5.1 The Level 2 report shall include all information listedunder 4.4.4.5.2 The report shall include the manufacturers identifica-tion of the instrument or apparatus used to perform the particlesize measurement.4.5.3 The report shall include a
27、ll of the parameters requiredto use the instrument or apparatus.4.5.4 The report shall include the software version num-ber(s) of any computerized instrument used to measure particlesize.4.5.5 The report shall include a description of the basis ofcalculations performed by the instrument, to the exte
28、nt avail-able from the instrument manufacturer. Also, the report shallinclude description of any additional calculations performedoutside of the instrument software package.4.5.6 The report shall include basic statistical information,such as standard deviation, number of degrees of freedom, andconfi
29、dence interval, and shall include a description of thecalculations used to produce this statistical information.4.5.7 The report shall include the specifications or limits ofthe measurement as defined by the instrument manufacturer.4.5.8 The report shall include a complete description ofsample prepa
30、ration.4.6 Particle Size Characterization Data SheetLevel 3:4.6.1 The Level 3 report shall include all information listedunder 4.4 and 4.5.4.6.2 The report shall include operating procedures associ-ated with the particle size measurement and the completedesignation of any published procedures, such
31、as ASTM orindustry standard test methods.4.6.3 The report shall include a complete description of anyinstrument operational and calibration procedures not specifiedby a published procedure.4.6.4 The report shall include a statement of precision andbias of the particle size measurement data where ava
32、ilable.5. Report Guidelines5.1 Typical reports based upon the information categoriespresented in items 4.4 through 4.6.4 are shown below. Theactual text of the report will depend upon the particular particlesize measurement technique used. Users and suppliers shouldagree in advance on the particular
33、 size parameters reported.5.2 Particle Size Characterization Data SheetLevel 1:5.2.1 This ASTM designation,5.2.2 Material,5.2.3 Source,5.2.4 Lot number, and5.2.5 Size Parameter(s). For Example:5.2.5.1 Geometric mean diameter,5.2.5.2 Modal diameter,5.2.5.3 Median diameter, and5.2.5.4 Other defined si
34、ze related parameter.5.2.6 Data basis (frequency, mass, etc.),E16170925.2.7 Measurement range, and5.2.8 Measurement principle.5.3 Particle Size Characterization Data SheetLevel 2:5.3.1 This ASTM designation,5.3.2 Material,5.3.3 Source,5.3.4 Lot Number, and5.3.5 Size Parameter(s). For Example:5.3.5.1
35、 Geometric mean diameter,5.3.5.2 Modal diameter,5.3.5.3 Median diameter, and5.3.5.4 Other defined size related parameter.5.3.6 Data Basis (frequency, mass, etc.),5.3.7 Measurement range,5.3.8 Measurement principle,5.3.9 Instrument and model,5.3.10 Measurement ConditionsInstrument operationalparamete
36、rs,5.3.11 Software version number(s),5.3.12 Calculation method,5.3.13 Basic Statistics (Refer to Terminology E 456):5.3.13.1 Standard deviation,5.3.13.2 Degrees of freedom, and5.3.13.3 Confidence level.5.3.14 Sample Preparation:5.3.14.1 Dispersion medium:5.3.14.2 Dispersion steps: (equipment, power
37、rating, dura-tion), and5.3.14.3 Dispersion verification.5.4 Particle Size Characterization Data SheetLevel 3:5.4.1 This ASTM designation,5.4.2 Material,5.4.3 Source,5.4.4 Lot Number,5.4.5 Size Parameter(s). (For Example):5.4.5.1 Geometric mean diameter,5.4.5.2 Modal diameter,5.4.5.3 Median diameter,
38、 and5.4.5.4 Other defined size related parameter.5.4.6 Data basis (frequency, mass, etc.),5.4.7 Measurement range,5.4.8 Measurement principle,5.4.9 Instrument and model,5.4.10 Measurement ConditionsInstrument operationalparameters,5.4.11 Software version,5.4.12 Calculation method,5.4.13 Basic Statis
39、tics (Refer to Terminology E 456):5.4.13.1 Standard deviation,5.4.13.2 Degrees of freedom, and5.4.13.3 Confidence level.5.4.14 Sample Preparation:5.4.14.1 Dispersion medium,5.4.14.2 Dispersion steps: (equipment, power rating, dura-tion), and5.4.14.3 Dispersion verification.5.4.15 Analytical procedur
40、e and number,5.4.16 Precision and bias (refer to Practices E 177 andE 691),5.4.17 Test or assay number, and5.4.18 Calibration or standardization procedure.5.5 Example Report FormAn example of a report form(data sheet) incorporating all the required parameters may befound in Appendix Appendix X1.6. K
41、eywords6.1 particle characterization; particle size; particle sizeanalysis; particle size characterization; particle size distribu-tion; and particle size reportAPPENDIX(Nonmandatory Information)X1. Particle Size Characterization ReportX1.1 This appendix contains a suggested form (data sheet)for rep
42、orting particle size characterization data according tothis Standard Practice.NOTE X1.1The size parameters shown in the example in X1.2 areonly suggestions. Other size parameters, or additional size parameters,may be included in the report, as indicated in 5.2.5,5.3.5.1, and 5.4.5.X1.1.1 Page 1 of t
43、he report form (X1.2) contains all theinformation necessary for a Level 1 report (See 5.2), such thatonly page 1 will be necessary if reporting to Level 1. Completeonly page 1, column 1, for a Level 1 reportX1.1.2 Page 2 of the report form (X1.3) contains theadditional information necessary for a Le
44、vel 2 report (See5.3.), such that only pages 1 and 2 will be necessary ifreporting to Level 2. Complete both pages 1 and 2 (column 2on both pages) for a Level 2 report.X1.1.3 Page 3 of the report form (X1.4) contains theinformation for a Level 3 report, which is in addition to theLevel 1 and Level 2
45、 information (See 5.4.), such that all threepages will be necessary if reporting to Level 3. Complete allthree pages (column 3 on all three pages) for a Level 3 report.X1.2 Example Report Form Page 1 Level 1 Report SeeFig. X1.1.X1.3 Example Report Form Page 2 Level 2 Report SeeFig. X1.2.X1.4 Example
46、 Report Form Page 3 Level 3 Report SeeFig. X1.3.E1617093FIG. X1.1 ASTM E 1617 Particle Size Characterization Report (Page 1)E1617094.FIG. X1.2 ASTM E 1617 Particle Size Characterization Report (Page 2)E1617095ASTM International takes no position respecting the validity of any patent rights asserted
47、in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the
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49、reful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or servic
