1、Designation: F309 04 (Reapproved 2018)Standard Practice forLiquid Sampling of Noncryogenic Aerospace Propellants1This standard is issued under the fixed designation F309; the number immediately following the designation indicates the year of originaladoption or, in the case of revision, the year of
2、last revision. A number in parentheses indicates the year of last reapproval. A superscriptepsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers procedures for obtaining a sampleof noncryogenic aerospace propellant. Two procedures arecovered
3、as follows:Procedure 1Closed System (Section 6), andProcedure 2Open-End Procedure (Section 7).1.2 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety, health, and e
4、nvironmental practices and deter-mine the applicability of regulatory limitations prior to use.For hazard statements see Sections 4 and 5.1.3 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Princip
5、les for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2F311 Practice for Processing Aerospace Liquid Samples forParticulate Contamination Analysis Usin
6、g Membrane Fil-ters3. Summary of Practice3.1 Samples are withdrawn from the system by (1) a closedvessel capture, and (2) an open-end vessel (see Fig. 1). Bothprocedures are practical for most liquid aerospace propellantsnot excessively corrosive or toxic.4. Apparatus4.1 Stainless Steel Pressure Sam
7、pling Cylinders, 1-Lcapacity, equipped with stainless steel valves on each end.4.1.1 CautionPressure sampling cylinders must bemarked for the liquid being sampled. Cylinders for onematerial must not be interchanged with sampling cylinders ofother materials because of the possibility of incompatibili
8、ty.4.2 Full Protective Suits.4.2.1 CautionDue to the toxic and corrosive nature ofmost propellent fluids and their vapors, extreme care must beexercised in handling. Full protective suits must be worn whensampling these fluids.4.3 Polyethylene Wash Bottle, 1-L capacity, filled withdemineralized wate
9、r, filtered in the manner described in Prac-tice F311.4.4 Stainless Steel Bucket.4.5 Miscellaneous Fittings, as needed for sample pointadaption.5. Hazards5.1 Care should be taken when handling propellants sincemost of them are toxic to some degree. Care should also betaken when sampling fluids from
10、a system under dynamicconditions.PROCEDURE 1CLOSED SYSTEM6. Procedure6.1 Sampling cylinders must be clean, particulate-controlledin accordance with system requirements, and have a partialvacuum of 10 % of atmospheric pressure.6.2 After removing protective caps, connect both ends of thesampling cylin
11、der to the system sampling ports, using fittingsas necessary.6.3 Open both sampling valves and both sampling cylindervalves, and allow fluid to flow through the sampling cylinderfor 10 min.6.4 Close all four valves downstream side first, and removethe sampling cylinder from the system.6.5 Rinse the
12、valve ends with demineralized water filteredthrough a 0.8 to 2.0-m absolute membrane.6.6 Replace the protective caps on the sampling cylinderand sampling valves.6.7 Submit the full sampling cylinder for analysis.1This practice is under the jurisdiction of ASTM Committee E21 on SpaceSimulation and Ap
13、plications of Space Technology and is the direct responsibility ofSubcommittee E21.05 on Contamination.Current edition approved Sept. 1, 2018. Published September 2018. Originallyapproved in 1966. Last previous edition approved in 2010 as F309 04 (2010).DOI: 10.1520/F0309-04R18.2For referenced ASTM
14、standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocke
15、n, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organizat
16、ion Technical Barriers to Trade (TBT) Committee.1PROCEDURE 2OPEN-END PROCEDURE7. Procedure7.1 Sampling cylinders must be clean and particulate-controlled in accordance with system requirements, and have avacuum of 10 % of atmospheric pressure.7.2 After removing protective caps, connect the samplingc
17、ylinder to the sampling valve of the system and inlet valve ofthe sampling cylinder.7.3 Open the sampling valve of the system and inlet valve ofthe sampling cylinder.7.4 Slowly open the outlet valve of the sampling cylinderand catch the overflow in a bucket. Adjust the valve until thecylinder is ful
18、l.7.5 Close all three valves.7.6 Remove the sampling cylinder from system.7.7 Rinse the valve ends with demineralized water filteredthrough a 0.8 to 2.0-m absolute membrane.7.8 Replace the protective caps on the cylinder and sam-pling valves.7.9 Submit the full sampling cylinder for analysis.8. Prec
19、ision and Bias8.1 Neither the precision nor the bias for this practice hasbeen determined.9. Keywords9.1 aerospace propellants; fluid sampling; samplingASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Us
20、ers of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed ever
21、y five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible techni
22、cal committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocke
23、n, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Two Systems for Obtaining a Sampling of NoncryogenicAerospace FluidF309 04 (2018)2
