1、BRITISH STANDARD BS EN 14016-1:2004 Binders for magnesite screeds Caustic magnesia and magnesium chloride Part 1: Definitions, requirements The European Standard EN 14016-1:2004 has the status of a British Standard ICS 01.040.91; 91.100.50 BS EN 14016-1:2004 This British Standard, was published unde
2、r the authority of the Standards Policy and Strategy Committee on 22 January 2004 BSI 22 January 2004 ISBN 0 580 43305 6 National foreword This British Standard is the official English language version of EN 14016-1:2004. EN 14016-1:2004 is a candidate “harmonized” European Standard and fully takes
3、into account the requirements of the European Commission mandate M/132, Floorings, given under the EU Construction Products Directive (89/106/EEC), and intended to lead to CE marking. The date of applicability of EN 14016-1:2004 as a “harmonized” European Standard, i.e. the date after which this sta
4、ndard may be used for CE marking purposes, is subject to an announcement in the Official Journal of the European Communities. The European Commission in consultation with Member States has agreed a transition period for the co-existence of “harmonized” European Standards and their corresponding nati
5、onal standard(s). It is intended that this period will comprise a period, usually nine months, after the date of availability of the European Standard, during which any required changes to national regulations are to be made, followed by a further period, usually of 12 months, for the implementation
6、 of CE marking. At the end of this co-existence period, the national standard(s) will be withdrawn. In the UK, there is no corresponding national standard. The UK participation in the preparation of EN 14016-1:2004 was entrusted by Technical Committee B/507, Paving units, kerbs, screeds and in situ
7、floorings, to Subcommittee B/507/6, Screeds and in situ floorings, which has the responsibility to: A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications refe
8、rred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provi
9、sions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation,
10、 or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 16, an inside back cover and a back cover.
11、 The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. Date CommentsEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM EN140161 January2004 ICS01.040.91;91.100.50 Englishversion BindersformagnesitescreedsCausticmagne
12、siaand magnesiumchloridePart1:Definitions,requirements LiantspourchapesbasedemagnsieMagnsie caustiqueetchloruredemagnsiumPartie1:Dfinitions, exigences BindemittelfrMagnesiaestricheKaustischeMagnesia undMagnesiumchloridTeil1:BegriffeundAnforderungen ThisEuropeanStandardwasapprovedbyCENon15September20
13、03. CENmembersareboundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheCentralSecretariatort
14、oanyCENmember. ThisEuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheCentralSecretariathasthesamestatusast heofficial versions. CENmembersarethenationalstandardsbodieso
15、fAustria,Belgium,Cyprus,CzechRepublic,Denmark,Estonia,Finland,France, Germany,Greece,Hungary,Iceland,Ireland,Italy,Latvia,Lithuania,Luxembourg,Malta,Netherlands,Norway,Poland,Portugal, Slovakia, Slovenia,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORM
16、ALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2004CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.EN140161:2004:EEN140161:2004(E) 2 Contents page Foreword3 1 Scope 4 2 Normativereferences 4 3 Termsanddefinitions.
17、 .4 4 Requirements .5 4.1 Magnesiumchloride 5 4.2 Causticmagnesia 5 4.2.1 Homogeneity 5 4.2.2 Chemicalcomposition .5 4.2.3 Loosedensity. 5 4.2.4 Finenessofgrind . 5 4.2.5 Settingtime .6 4.2.6 Flexuralandcompressivestrength . 6 4.3 Reactiontofire .6 5 Testing 6 6 Evaluationofconformity .6 6.1 General
18、6 6.2 Initialtypetesting(ITT) 7 6.3 Factoryproductioncontrol(FPC) 7 6.4 Technicalspecificationsforbindersformagnesitescreed . .7 7 Designation.7 8 Markingandlabelling . .8 9 Conformitycriteriaandassessmentprocedure .8 9.1 General8 9.2 Statisticalconformitycriteria . 8 9.2.1 General8 9.2.2 Checkbyvar
19、iables 8 9.2.3 Checkbyattributes. .9 9.3 Minimumtestingfrequencies . 10 AnnexZA (informative) ClausesofthisEuropeanStandardaddressingessentialrequirementsorother provisionsofEUDirectives. . 11 ZA.1 Scopeandrelevantcharacteristics . 11 ZA.2 Procedure(s)forattestationofconformityofbindersformagnesites
20、creedmaterials.12 ZA.2.1 System(s)ofattestationofconformity . .12 ZA.2.2 ECDeclarationofconformity . 13 ZA.3 CEmarkingandlabelling. .14 Bibliography 16EN140161:2004(E) 3 Foreword Thisdocument(EN140161:2004)hasbeenpreparedbyTechnicalCommitteeCEN/TC303,“Floorscreedsand insituflooringsinbuildings”,thes
21、ecretariatofwhichisheldbyBSI. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationofanidenticaltextor byendorsement,atthelatestbyJuly2004,andconflictingnationalstandardsshallbewithdrawnatthelatestby October2005. Thisdocumentbelongstoaseriesofstandardsforscreedmaterialandf
22、loorscreedswithinbuildingconstructions. NoexistingEuropeanStandardissuperseded. ThisdocumenthasbeenpreparedunderMandateM132“Floorings”giventoCENbytheEuropeanCommission andtheEuropeanFreeTradeAssociation,andsupportsessentialrequirementsofEUDirective(s). ForrelationshipwithEUDirective(s),seeinformativ
23、eannexZA,whichisanintegralpartofthisdocument. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsofthefollowingcoun triesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Cyprus,CzechRepublic,Denmark,Esto nia,Finland,France,Germany,Greece,Hungary,Iceland,Ireland,Ital
24、y,Latvia,Lithuania,Luxembourg,Malta, Netherlands,Norway,Poland,Portugal,Slovakia,Slovenia,Spain,Sweden,SwitzerlandandUnitedKingdom.EN140161:2004(E) 4 1Scope ThisEuropeanStandardspecifiesrequirementsforcausticmagnesiaandmagnesiumchloride,whichwillbeused formagnesitescreedmaterialandmagnesitescreedsas
25、specifiedinEN1 3813. 2 Normativereferences ThisEuropeanStandardincorporatesbydatedorundatedreference,provisionsfromotherpublications.These normativereferencesarecitedattheappropriateplacesinthetextandthepublicationsarelistedhereafter.For datedreferences,subsequentamendmentstoorrevisionsofanyofthesep
26、ublicationsapplytothisEuropean Standardonlywhenincorporatedinitbyamendmentorrevision.Forundatedreferencesthelatesteditionofthe publicationreferredtoapplies(includingamendments). EN1961, MethodsoftestingcementPart1:Determinationofstrength. EN13318:2000, ScreedmaterialsandfloorscreedsDefinitions. EN14
27、0162, BindersformagnesitescreedsCausticmagnesiaandmagnesiumchloridePart2:Testmeth ods. EN135011, FireclassificationofconstructionproductsandbuildingelementsPart1:Classificationusingtest datafromreactiontofiretests. ENISO9001, QualitymanagementsystemsRequirements(ISO9001:2000). 3 Termsanddefinitions
28、ForthepurposesofthisEuropeanStandard,thetermsanddefinitionsgiveninEN13318:2000andthefollowing apply. 3.1 magnesiumchloride compound(magnesiumchloride(MgCl 2 )whichmaycontainwaterinsolublesubstances,e.g.ferrousoxide(Fe 2 O 3 ) andmagnesiumoxide(MgO),aswellaswatersolublesubstances,e.g.sodiumchloride(N
29、aCl),potassiumchloride (KCl),calciumchloride(CaCl 2 )andmagnesiumsulfate(MgSO 4 );itistradedassolidsaltoraqueoussolution 3.2 causticmagnesia afinelygroundbinder,whichisburnedoutofnaturallyoccurringmagnesiumcarbonateMgCO 3 orothermagne siumcompounds;themainconstituentofthecausticmagnesiaismagnesiumox
30、ide(MgO);subconstituentsmay becarbonate(CO 3 ),silicicoxide(SiO 2 ),aluminiumoxide(Al 2 O 3 ),ferricoxide(Fe 2 O 3 ),calciumoxide(CaO)and sulfate(SO 4 )EN140161:2004(E) 5 4Requirements 4.1 Magnesiumchloride MagnesiumchlorideshallconformtotherequirementsbycompositiongiveninTable1: Table1Requirementsf
31、ormagnesiumchloride Subingredients Main constituent Waterinsoluble substances Watersoluble substances Trade form mass MgCl 2 (%) mass (%) NaCl+KCl mass (%) MgSO 4 mass (%) CaCl 2 mass (%) pHvalue Aqueous solution 20 0,05 1 0,5 0,5 Solidsalt 46 0,1 2 1 1 6 4.2Caustic magnesia 4.2.1Homogeneity Charges
32、shallbehomogenousandshowthesamecolourbyvisualinspection. 4.2.2 Chemicalcomposition Thechemicalcompositionshallfulfilthefollowingrequirements: a)magnesium oxide MgO 80%bymass b)hydrochloricacidinsoluble residues + sesquioxides 14%bymass c)calcium oxide CaO 1) 4%bymass d)ignition loss 8%bymass 4.2.3 L
33、oosedensity Theloosedensityshallnotbemorethan1000kg/m 3 . 4.2.4 Finenessofgrind BytestingthefinenessofthegrindtheresiduesinthesievesshallnotexceedthevalueinTable2. 1) AhighertotalamountofCaOisallowed,ifthefreeCaOcontentislowerthen1%bymass.EN140161:2004(E) 6 Table2Finenessofgrind Sievemeshwidth (mm)
34、Massofresidues (%) 0,09 30 4.2.5Setting time Thesettingprocessofthemagnesiapasteshallbegin30minutesaftermixingattheearliestandend5hafter mixingatthelatest. 4.2.6 Flexuralandcompressivestrength Themagnesiatestmortar,consistingofcausticmagnesia,magnesiumchlorideandCENstandardsandaccording toEN1961(see
35、EN140162)shallhaveatleastthestrengthcharacteristicsgiveninTable3. Table3Flexuralandcompressivestrength Age days Flexuralstrength N/mm 2 Compressivestrength N/mm 2 28 9 60 NOTE Whentestedattheageof3days,aflexuralstrengthofabout8N/mm 2 andacompressivestrengthofapproxi mately50N/mm 2 shouldbeobtained.
36、4.3 Reactiontofire Bindersformagnesitescreedmaterialswhichdonotcontainmorethan1%oforganicmaterialbymassorvolume (whicheveristhemoreonerous)areclassifiedA1 fl withouttheneedfortesting 2) .Allothermaterialsshallbetested andclassifiedinaccordancewithEN135011. 5Testing Testing,exceptforreactiontofire,sh
37、allbecarriedoutasspecifiedinEN140162. 6 Evaluationofconformity 6.1General Evaluationofconformityiscarriedoutbydeclaringconformityofbindersformagnesitescreeds,causticmagnesia andmagnesiumchloride,withtherequirementsofthisstandardonthebasisof: Initialtypetesting(ITT); Factoryproductioncontrol(FPC). Th
38、econformitycriteriaandassessmentprocedurearegiveninclause9. 2) SeeCommissionDecision96/603/EC,asamended.EN140161:2004(E) 7 6.2 Initialtypetesting(ITT) Aninitialtypetestingshallbecarriedouttoshowconformityoftheproducttothisstandard.Additionally,aninitial typetestingshallbecarriedoutatthebeginningofpr
39、oductionofanewproducttype.Beforestartingproduction andintroductionoftheproductintothemarket,suitableinitialtypetestingshallbecarriedouttoconfirmthatthe predictedproductpropertiesconformtotherequirementsinthisstandardandcorrespondtothedeclaredvalues. Initialtypetestsshallalsobecarriedoutifthespecific
40、ationforthebindersorthemanufacturingmethodhavebeen changed. Testspreviouslyperformedinaccordancewiththeprovisionsofthisstandardmaybetakenintoaccountprovided thatproductcharacteristic(s),testmethod,samplingprocedureandsystemofattestationofconformityareidenti cal. 6.3 Factoryproductioncontrol(FPC) Fac
41、toryproductioncontrolmeansthepermanentinternalcontrolofproductionexercisedbythemanufacturerorhis agentundertheresponsibilityofthemanufacturerhimself. Thepurposeofthefactoryproductioncontrolistoensurethatbindersformagnesitescreedsplacedonthemarket conformtotheirtechnicalspecificationsgiveninclause4.S
42、amplingandtestsshallbecarriedoutasdescribedin EN140162,exceptasprovidedforin6.4. Themanufacturershallrecordtheresultsofproductioncontrol(manufacturersrecord).Theserecordsshallinclude atleastthefollowing: identificationoftheproducttested; date of sampling; testmethodsused; testandinspectionresults; d
43、ateoftests; identificationofthepersonresponsibleforthetests; calibrationrecords. AnFPCsystemconformingtotherequirementsinENISO9001andcorrespondingtotherequirementsinthis standardisconsideredasasystemwhichfulfilstherequirementsmentionedabove. 6.4 Technicalspecificationsforbindersformagnesitescreed Th
44、etechnicalspecificationsandpropertiesspecifiedinthisstandardaredefinedintermsofreferencetestmethods (seeEN140162),whichshallbeusedtodemonstratetheconformityoftheproductstothisEuropeanStandard. Forfactoryproductioncontrol,othertestmethodsmaybeusedprovidedthat: a) theycanshowarelationshiptoexistbetweentheresultsfromtheCEN