BS EN ISO 105-E06-2006 Textiles - Tests for colour fastness - Colour fastness to spotting - Alkali《纺织品 色牢度试验 耐碱滴腐蚀色牢度》.pdf

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1、 g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58AlkaliThe European Standard EN ISO 105-E06:2006 has the status of a British StandardICS 59.080.01Te

2、xtiles Tests for colour fastness Part E06: Colour fastness to spotting: BRITISH STANDARDBS EN ISO 105-E06:2006BS EN ISO 105-E06:2006This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 July 2006 BSI 2006ISBN 0 580 48880 2Cross-referencesThe Bri

3、tish Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards On

4、line.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations.Summary of pagesThis document comprises a front cover, an insi

5、de front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii and iii, a blank page, pages 1 to 3 and a back cover.The BSI copyright notice displayed in this document indicates when the document was last issued.Amendments issued since publicationAmd. No. Date Comments

6、A list of organizations represented on this committee can be obtained on request to its secretary. present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep UK interests informed; monitor related international and European deve

7、lopments and promulgate them in the UK.National forewordThis British Standard is the official English language version of EN ISO 105-E06:2006. It is identical with ISO 105-E06:2006. It supersedes BS EN ISO 105-E06:1997 which is withdrawn.The UK participation in its preparation was entrusted to Techn

8、ical Committee TCI/81, Textiles Colour fastness and colour measurement, which has the responsibility to: aid enquirers to understand the text;EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 105-E06July 2006ICS 59.080.01English VersionTextiles - Tests for colour fastness - Part E06: Colour fast

9、nessto spotting: Alkali (ISO 105-E06:2006)Textiles - Essais de solidit des teintures - Partie E06:Solidit des teintures aux alcalis (ISO 105-E06:2006)Textilien - Farbechtheitsprfungen - Teil E06: Farbechtheitgegen Flecken: Alkali (ISO 105-E06:2006)This European Standard was approved by CEN on 21 Jun

10、e 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained

11、 on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretaria

12、t has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, R

13、omania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2006 CEN All rights of exploitation in any form and by any means reservedw

14、orldwide for CEN national Members.Ref. No. EN ISO 105-E06:2006: EForeword This document (EN ISO 105-E06:2006) has been prepared by Technical Committee ISO/TC 38 “Textiles“ in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products“, the secretariat of which is held by BSI. T

15、his European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2007, and conflicting national standards shall be withdrawn at the latest by January 2007. According to the CEN/CENELEC Internal Regulations,

16、 the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, P

17、oland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 105-E06:2006 has been approved by CEN as EN ISO 105-E06:2006 without any modifications. EN ISO 105-E06:2006Reference numberISO 105-E06:2006(E)INTERNATIONAL STANDARD ISO105-

18、E06Fourth edition2006-07-15Textiles Tests for colour fastness Part E06: Colour fastness to spotting: Alkali Textiles Essais de solidit des teintures Partie E06: Solidit des teintures aux alcalis EN ISO 105-E06:2006ii Foreword ISO (the International Organization for Standardization) is a worldwide fe

19、deration of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that com

20、mittee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accord

21、ance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard require

22、s approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 105-E06 was prepared by Technica

23、l Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. This fourth edition cancels and replaces the third edition (ISO 105-E06:1989), which has been technically revised. It also incorporates Technical Corrigendum ISO 105-E06:1989/Cor. 1:2002. ISO 105 was previ

24、ously published in 13 “parts”, each designated by a letter (e.g. “Part A”), with publication date between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (e.g. “Section A01”). These sections are now being repub

25、lished as separate documents, themselves designated “parts“ but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. EN ISO 105-E06:2006blank1Textiles Tests for colour fastness Part E06: Colour fastness to spotting: Alkali 1 Scope This part of IS

26、O 105 specifies a method for determining the resistance of the colour of textiles of all kinds, and in all forms, to the action of dilute alkaline solutions. Three tests differing in severity are provided. Any or all may be used, depending on the nature of the fibre. 2 Normative references The follo

27、wing referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 105-A01, Textiles Tests for colour fastness Part A01:

28、General principles of testing ISO 105-A02, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour ISO 105-A05, Textiles Tests for colour fastness Part A05: Instrumental assessment of change in colour for determination of grey scale rating ISO 105-E07, Textiles Tests f

29、or colour fastness Part E07: Colour fastness to spotting: Water 3 Principle The specimens are steeped in or spotted with prepared reagents by means of simple laboratory equipment. The change in the colour of the textile, while it is still wet and after drying, is assessed either visually or instrume

30、ntally. 4 Reagents and materials 4.1 Pipette or dropper. 4.2 Glass rod, with rounded end. 4.3 Glass beaker. 4.4 Grey scale for assessing change in colour, complying with ISO 105-A02. 4.5 Sodium carbonate solution, containing 100 g of anhydrous sodium carbonate (Na2CO3) per litre of water (4.8). EN I

31、SO 105-E06:20062 4.6 Calcium hydroxide paste, containing 1 g of calcium hydroxide Ca(OH)2 mixed with 1 g to 2 g of water (4.8). 4.7 Ammonium hydroxide, solution containing 28 % of ammonium hydroxide (NH4OH). 4.8 Grade 3 water (see ISO 105-A01). NOTE See Table 1 for a list of the chemicals and pH lev

32、els of the reagents used in this method. 5 Test specimen 5.1 Prepare a test specimen as described in 5.2 to 5.4 for each alkali to be used. 5.2 If the textile to be tested is fabric, use a specimen measuring 40 mm 100 mm. 5.3 If the textile to be tested is yarn, knit it into fabric and use a specime

33、n measuring 40 mm 100 mm, or make a wick of parallel lengths 100 mm long and about 5 mm in diameter, tied near both ends. 5.4 If the textile to be tested is loose fibre, comb and compress enough of it to form a sheet measuring 40 mm 100 mm. 6 Procedure 6.1 Sodium carbonate 6.1.1 Place the specimen i

34、n a clean dry flat-bottomed dish. Spot the specimen at room temperature with the sodium carbonate solution (4.5) so that after working the solution into the specimen with the glass rod, a spot of diameter approximately 20 mm is formed. In the case of water-repellent fabrics, the amount of solution s

35、hall not exceed 0,5 ml. 6.1.2 Place the specimen on a flat surface and allow to dry at room temperature; brush it to remove the sodium carbonate residues. 6.1.3 If brushing is not enough to completely eliminate the whitish ring caused by spotting with sodium carbonate, rinse the specimen in a glass

36、beaker for 1 min with 100 ml of Grade 3 water (4.8) at room temperature. Allow the specimen to dry at room temperature. 6.2 Calcium hydroxide 6.2.1 Spot the specimen at room temperature with the calcium hydroxide paste (4.6). 6.2.2 Place the specimen on a flat surface and allow to dry at room temper

37、ature; brush it to remove the calcium hydroxide residues. 6.2.3 If brushing is not enough to completely eliminate the whitish ring caused by spotting with calcium hydroxide, rinse the specimen in a glass beaker for 1 min with 100 ml of Grade 3 water (4.8) at room temperature. Allow the specimen to d

38、ry at room temperature. 6.3 Ammonium hydroxide 6.3.1 Steep the specimen for 2 min in ammonium hydroxide solution (4.7) at room temperature. 6.3.2 Place the specimen on a flat surface and allow to dry at room temperature without rinsing. EN ISO 105-E06:200636.4 Assess the change in colour Assess the

39、change in colour of the specimen using either the grey scale or instrumentally (See ISO 105-A02 and ISO 105-A05) for each alkali used. Assess the change in colour of the wet spot after 10 min, if applicable. 6.5 Resistance to water spotting It is recommended that the test for resistance to water spo

40、tting (see ISO 105-E07) also be carried out to ascertain that the change in colour is not due to the action of water alone. 7 Test report The test report shall include the following: a) a reference to this part of ISO 105 (ISO 105-E06:2006); b) all details necessary for the identification of the sam

41、ple tested; c) the numerical grey scale rating or instrumental assessment for change in colour of the specimen for each type of alkali used and for change when wet, if of interest; d) the result of the resistance to water spotting (6.5); e) any deviation, by agreement or otherwise, from the procedur

42、e specified. Table 1 pH levels of chemicals used Chemical pH Ammonium hydroxide 13,5 13,7 Calcium hydroxide 12,3 12,5 Sodium carbonate 11,5 11,7 EN ISO 105-E06:2006BS EN ISO BSI389 Chiswick High RoadLondonW4 4AL105-E06:2006BSI British Standards InstitutionBSI is the independent national body respons

43、ible for preparing British Standards. It presents the UK view on standards in Europe and at the international level. It is incorporated by Royal Charter.RevisionsBritish Standards are updated by amendment or revision. Users of British Standards should make sure that they possess the latest amendment

44、s or editions.It is the constant aim of BSI to improve the quality of our products and services. We would be grateful if anyone finding an inaccuracy or ambiguity while using this British Standard would inform the Secretary of the technical committee responsible, the identity of which can be found o

45、n the inside front cover. Tel: +44 (0)20 8996 9000. Fax: +44 (0)20 8996 7400.BSI offers members an individual updating service called PLUS which ensures that subscribers automatically receive the latest editions of standards.Buying standardsOrders for all BSI, international and foreign standards pub

46、lications should be addressed to Customer Services. Tel: +44 (0)20 8996 9001. Fax: +44 (0)20 8996 7001. Email: ordersbsi-. Standards are also available from the BSI website at http:/www.bsi-.In response to orders for international standards, it is BSI policy to supply the BSI implementation of those

47、 that have been published as British Standards, unless otherwise requested.Information on standardsBSI provides a wide range of information on national, European and international standards through its Library and its Technical Help to Exporters Service. Various BSI electronic information services a

48、re also available which give details on all its products and services. Contact the Information Centre. Tel: +44 (0)20 8996 7111. Fax: +44 (0)20 8996 7048. Email: infobsi-.Subscribing members of BSI are kept up to date with standards developments and receive substantial discounts on the purchase pric

49、e of standards. For details of these and other benefits contact Membership Administration. Tel: +44 (0)20 8996 7002. Fax: +44 (0)20 8996 7001. Email: membershipbsi-.Information regarding online access to British Standards via British Standards Online can be found at http:/www.bsi- information about BSI is available on the BSI website at http:/www.bsi-.CopyrightCopyright subsists in all BSI publications. BSI

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