1、BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06Rubber Determination of adhesion to rigid materials using conical shaped partsBS ISO 5600:2017 ISO 2017Rubber Determination of adhesionto rigid materials using conicalshaped partsCaoutchouc Dtermination de ladhrence aux
2、 matriaux rigides au moyen de pices coniquesINTERNATIONALSTANDARDISO5600Fifth edition2017-06Reference numberISO 5600:2017(E)National forewordThis British Standard is the UK implementation of ISO 5600:2017. It supersedes BS ISO 5600:2011, which is withdrawn.The UK participation in its preparation was
3、 entrusted to Technical Committee PRI/22, Testing and analysis of rubber.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct ap
4、plication. The British Standards Institution 2017 Published by BSI Standards Limited 2017ISBN 978 0 580 97189 1ICS 83.060Compliance with a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Commi
5、ttee on 30 June 2017.Amendments/corrigenda issued since publicationDate Text affectedBRITISH STANDARDBS ISO 5600:2017 ISO 2017Rubber Determination of adhesion to rigid materials using conical shaped partsCaoutchouc Dtermination de ladhrence aux matriaux rigides au moyen de pices coniquesINTERNATIONA
6、L STANDARDISO5600Fifth edition2017-06Reference numberISO 5600:2017(E)BS ISO 5600:2017ISO 5600:2017(E)ii ISO 2017 All rights reservedCOPYRIGHT PROTECTED DOCUMENT ISO 2017, Published in SwitzerlandAll rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilize
7、d otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below or ISOs member body in the country of the requester.ISO copyright o
8、fficeCh. de Blandonnet 8 CP 401CH-1214 Vernier, Geneva, SwitzerlandTel. +41 22 749 01 11Fax +41 22 749 09 47copyrightiso.orgwww.iso.orgBS ISO 5600:2017ISO 5600:2017(E)Foreword iv1 Scope . 12 Normative references 13 Terms and definitions . 14 Principle 25 Apparatus . 26 Calibration 27 Test piece 27.1
9、 Form and dimensions 27.2 Materials . 27.3 Preparation 37.4 Number of test pieces . 37.5 Conditioning of test pieces . 38 Procedure. 49 Expression of results 49.1 Adhesion value 49.2 Type of adhesion failure 410 Salvaging of bonded metal parts 411 Test report . 5Annex A (normative) Calibration sched
10、ule . 6 ISO 2017 All rights reserved iiiContents PageBS ISO 5600:2017ISO 5600:2017(E)ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out thro
11、ugh ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collabor
12、ates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval c
13、riteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).Attention is drawn to the possibility that some of the elements of this document may be the subj
14、ect of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www .iso .org/ patents).Any tr
15、ade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adher
16、ence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: www .iso .org/ iso/ foreword .htmlThis document was prepared by Technical Committee ISO/TC 45, Rubber and rubber products, Subcommittee SC 2, Testing and analysis.This fifth edition
17、cancels and replaces the fourth edition (ISO 5600:2011), of which it constitutes a minor revision to update the normative references in Clause 2.iv ISO 2017 All rights reservedBS ISO 5600:2017INTERNATIONAL STANDARD ISO 5600:2017(E)Rubber Determination of adhesion to rigid materials using conical sha
18、ped partsWARNING 1 Persons using this document should be familiar with normal laboratory practice. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to e
19、nsure compliance with any national regulatory conditions.WARNING 2 Certain procedures specified in this document might involve the use or generation of substances, or the generation of waste, that could constitute a local environmental hazard. Reference should be made to appropriate documentation on
20、 safe handling and disposal after use.1 ScopeThis document specifies a method for the determination of the static vulcanized adhesion strength of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by a cylinder of rubber.The adhesion is
21、obtained by a bonding system which can include not only the rigid material and the rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a single cement or both primer and cover cements. The bonding system for preparing the test pieces shoul
22、d be adequately specified by the user, but provision is made in this document for the evaluation of different types of failure related to a complex bonding system.The method is designed primarily for test pieces prepared in the laboratory under standard conditions in order to provide data for develo
23、pment and control of bonding systems and their components, such as cements or special rubber compounds, and of methods of manufacture. While intended to be applied where the rubber is bonded to rigid supporting pieces, it might not cover such cases where the support, although of high-modulus materia
24、l, has a low rigidity due to small transverse dimensions, as in the case of rubber bonded to metal wires, cords or thin sheets.2 Normative referencesThe following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For date
25、d references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 5893:2002, Rubber and plastics test equipment Tensile, flexural and compression types (constant rate of traverse) SpecificationISO 18899:2013, Ru
26、bber Guide to the calibration of test equipmentISO 23529, Rubber General procedures for preparing and conditioning test pieces for physical test methods3 Terms and definitionsNo terms and definitions are listed in this document. ISO and IEC maintain terminological databases for use in standardizatio
27、n at the following addresses: IEC Electropedia: available at h t t p :/ www .electropedia .org/ ISO Online browsing platform: available at h t t p :/ www .iso .org/ obp ISO 2017 All rights reserved 1BS ISO 5600:2017ISO 5600:2017(E)4 PrincipleThe test consists in measuring the force required to cause
28、 the rupture of a test piece of standard dimensions, comprising a cylinder of rubber bonded to two rigid conical parts.The particular geometry of the test piece produces in most cases an interfacial failure between the cylinder of rubber and the conical parts because of a stress concentration at the
29、 tip of the cones.5 Apparatus5.1 Tensile-testing machine, complying with the requirements of ISO 5893:2002, class 2, and with a rate of traverse of the moving grip of (50 5) mm/min.Inertia (pendulum) type dynamometers have a tendency to give results which differ because of inertial effects. A low-in
30、ertia type dynamometer (for example, using an electronic or optical transducer) gives results which are free from this effect, and is therefore to be preferred.5.2 Fixtures, for holding the test pieces in the test machine, which permit accurate centring of the applied load during the test.6 Calibrat
31、ionThe test apparatus shall be calibrated in accordance with Annex A.7 Test piece7.1 Form and dimensionsThe standard test piece (see Figure 1) is formed by two rigid cylindrical parts terminated by opposite conical ends, and a cylinder of rubber bonded to the conical ends. The determination of the d
32、imensions of the test piece shall be in accordance with ISO 23529.The diameter of this cylinder and of the cylindrical portion of the rigid parts shall be (25 0,5) mm. The distance between the tips of the conical ends shall be (12 1) mm. The half-angle of the cone vertex shall be 45 1 and the tip sh
33、all be rounded to a radius not greater than 0,8 mm.The cylindrical portion of each rigid part shall be not less than 5 mm in length and shall be terminated so as to match with the holding jaws (5.2) of the test machine (5.1).7.2 MaterialsThe materials used shall conform to the specifications for the
34、 bonding system to be investigated. If no specification is given for the material of the rigid parts, they shall be made from low-carbon steel bars and their conical ends shall be grit-blasted.2 ISO 2017 All rights reservedBS ISO 5600:2017ISO 5600:2017(E)Dimensions in millimetresKey1 rubber cylinder
35、2 rigid conical partsFigure 1 Standard test piece7.3 Preparation7.3.1 Clean the surfaces of the conical ends or treat in accordance with the bonding system under investigation and, if so specified, coat with primer and/or cover cement. Spread the adhesive coating over the conical area only.7.3.2 Dur
36、ing the preparation of the test pieces, take great care when handling the materials to keep the bonding interfaces between the rubber and the rigid parts free from dust, moisture and foreign matter. Do not touch the treated conical surfaces with the hands during assembly.7.3.3 Vulcanize the test pie
37、ces in a suitable transfer mould, properly insulated and provided with heaters and compression devices. Place the rigid parts and the rubber compound in the preheated mould for vulcanization. Use sufficient unvulcanized compound to fill the pot and provide some excess after filling the mould cavitie
38、s.The mould design should take account of the fact that machining the rigid parts for reuse will gradually reduce their size.7.3.4 Carry out the vulcanization under the specified conditions of time, temperature and pressure.7.3.5 At the conclusion of the cure, take great care when removing the test
39、pieces from the mould to avoid subjecting the bonded surfaces to undue stress before the test pieces have cooled.7.4 Number of test piecesPrepare and test a minimum of three test pieces.7.5 Conditioning of test piecesCondition the test pieces in accordance with the requirements of ISO 23529 for at l
40、east 16 h at a standard laboratory temperature of (23 2) C or (27 2) C. Use the same temperature throughout the test and throughout a series of tests intended to be comparable. ISO 2017 All rights reserved 3BS ISO 5600:2017ISO 5600:2017(E)8 Procedure8.1 Mount a test piece in the fixtures (5.2) of th
41、e tensile-testing machine (5.1). Take extreme care in centring and adjusting the test piece so that the tension is symmetrically distributed over the cross-section of the test piece during the test.8.2 Apply the tension by separating the jaws at a constant rate of (50 5) mm/min until the test piece
42、breaks. Record the maximum force.8.3 Recover the broken pieces and examine the failure surfaces.8.4 Repeat for the remaining test pieces.9 Expression of results9.1 Adhesion valueExpress the adhesion value, in newtons, required to produce failure. In cases where the failure is in the rubber bulk, the
43、 adhesion value is recognized as being higher than that recorded.9.2 Type of adhesion failureExpress the type of adhesion failure, as determined by examination of the broken test pieces, by one or more of the following symbols:R failure in the rubber bulk;RC failure at the rubber/cover cement interf
44、ace;CP failure at the cover cement/primer cement interface;M failure at the metal/primer cement interface.Each symbol shall be followed by the percentage of the conical surface involved in that type of failure, estimated to the nearest 5 %.NOTE The estimated percentage of the various types of failur
45、e can be expressed as in the following examples:R 50, RC-50 means that roughly 50 % of the failure was in the rubber and the other 50 % at the rubber/cover cement interface.R 25, RC-25, M-50 means three types of failure were present, with the M indicating that 50 % of the failure was at the metal/pr
46、imer cement interface.10 Salvaging of bonded metal partsBonded metal parts can be salvaged by the usual burning or chemical stripping techniques. Mechanical or chemical surface treatments can be used to re-establish a clean bonding surface.The sharpness of the conical tip can be reduced during salva
47、ging; this affects the reproducibility of the test results, and care shall be taken to re-establish the sharpness of the cone to a radius of 0,8 mm or less.4 ISO 2017 All rights reservedBS ISO 5600:2017ISO 5600:2017(E)11 Test reportThe test report shall include the following information:a) sample de
48、tails:1) a description of the bonding system used, including materials, treatments and rubber cure (if the materials are of undisclosed composition, sufficient information shall be given to identify them),2) the date of vulcanization,3) the time and temperature of vulcanization;b) a reference to thi
49、s document, i.e. ISO 5600;c) test details:1) the temperature of test,2) the type of dynamometer used,3) details of any operation not included in this document or in the International Standards to which reference is made, as well as any operation regarded as optional;d) test results:1) the adhesion values for each test piece, in newtons,2) a description of the types of failure for each test piece, expressed in accordance with 9.2,3) any unusual features noted during the determination;e) the date
