1、December 2013 Translation by DIN-Sprachendienst.English price group 7No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).IC
2、S 91.100.23!%*“2076198www.din.deDDIN EN ISO 10545-9Ceramic tiles Part 9: Determination of resistance to thermal shock (ISO 10545-9:2013);English version EN ISO 10545-9:2013,English translation of DIN EN ISO 10545-9:2013-12Keramische Fliesen und Platten Teil 9: Bestimmung der Temperaturwechselbestndi
3、gkeit (ISO 10545-9:2013);Englische Fassung EN ISO 10545-9:2013,Englische bersetzung von DIN EN ISO 10545-9:2013-12Carreaux et dalles cramiques Partie 9: Dtermination de la rsistance aux chocs thermiques (ISO 10545-9:2013);Version anglaise EN ISO 10545-9:2013,Traduction anglaise de DIN EN ISO 10545-9
4、:2013-12SupersedesDIN EN ISO 10545-9:1996-09www.beuth.deDocument comprises 8 pagesIn case of doubt, the German-language original shall be considered authoritative.11.13 DIN EN ISO 10545-9:2013-12 2 A comma is used as the decimal marker. National foreword The text of ISO 10545-9:2013 has been prepare
5、d by Technical Committee ISO/TC 189 “Ceramic tile” and has been taken over as EN ISO 10545-9:2013 by Technical Committee CEN/TC 67 “Ceramic tiles” (Secretariat: UNI, Italy). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Co
6、mmittee), Working Committee NA 062-02-73 AA Prfung von keramischen Bauteilen fr Wand- und Bodenbelge. The DIN Standard corresponding to the International Standard referred to in this document is as follows: ISO 10545-3 DIN EN ISO 10545-3 Amendments This standard differs from DIN EN ISO 10545-9:1996-
7、09 as follows: a) the dependency of the different procedures on the water absorption (tests with or without immersion) has been stated in the scope; b) it has been specified that test specimens are to be selected at random; c) the standard has been editorially revised. Previous editions DIN 18166: 1
8、960-06, 1965-07, 1974-10, 1986-04, 1986-10 DIN 18167: 1960-07 DIN 51093: 1960-01 DIN EN 104: 1985-03, 1992-01 DIN EN ISO 10545-9: 1996-09 National Annex NA (informative) Bibliography DIN EN ISO 10545-3, Ceramic tiles Part 3: Determination of water absorption, apparent porosity, apparent relative den
9、sity and bulk density EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 10545-9 July 2013 ICS 91.100.23 Supersedes EN ISO 10545-9:1996English Version Ceramic tiles - Part 9: Determination of resistance to thermal shock (ISO 10545-9:2013) Carreaux et dalles cramiques - Partie 9: Dtermination d
10、e la rsistance aux chocs thermiques (ISO 10545-9:2013) Keramische Fliesen und Platten - Teil 9: Bestimmung der Temperaturwechselbestndigkeit (ISO 10545-9:2013) This European Standard was approved by CEN on 9 July 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which s
11、tipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This Europe
12、an Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are
13、the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Roma
14、nia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation in any form and by any means r
15、eserved worldwide for CEN national Members. Ref. No. EN ISO 10545-9:2013: EContents PageForeword .31 Scope . 42 Normative References . 43 Principle 44 Apparatus . 45 Test specimens 56 Procedure. 56.1 Preliminary check of the test specimens 56.2 Test with immersion 56.3 Test without immersion 56.4 Te
16、mperature cycling . 56.5 Examination. 57 Test report . 5Bibliography 6DIN EN ISO 10545-9:2013-12 EN ISO 10545-9:2013 (E) 2 Foreword This document (EN ISO 10545-9:2013) has been prepared by Technical Committee ISO/TC 189 “Ceramic tile” in collaboration with Technical Committee CEN/TC 67 “Ceramic tile
17、s” the secretariat of which is held by UNI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2014, and conflicting national standards shall be withdrawn at the latest by January 2014. Atten
18、tion is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 10545-9:1996. According to the CEN-CENELEC Internal Regulat
19、ions, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Ital
20、y, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 10545-9:2013 has been approved by CEN as EN ISO 10545-9:2013 without any modification. EN ISO 105
21、45 consists of the following parts, under the general title Ceramic tiles: Part 1: Sampling and basis for acceptance Part 2: Determination of dimensions and surface quality Part 3: Determination of water absorption, apparent porosity, apparent relative density and bulk density Part 4: Determination
22、of modulus of rupture and breaking strength Part 5: Determination of impact resistance by measurement of coefficient of restitution Part 6: Determination of resistance to deep abrasion for unglazed tiles Part 7: Determination of resistance to surface abrasion for glazed tiles Part 8: Determination o
23、f linear thermal expansion Part 9: Determination of resistance to thermal shock Part 10: Determination of moisture expansion Part 11: Determination of crazing resistance for glazed tiles Part 12: Determination of frost resistance Part 13: Determination of chemical resistance Part 14: Determination o
24、f resistance to stains Part 15: Determination of lead and cadmium given off by glazed tiles Part 16: Determination of small colour differencesDIN EN ISO 10545-9:2013-12 EN ISO 10545-9:2013 (E) 3 1 ScopeThis part of ISO 10545 specifies a test method for determining the resistance to thermal shock of
25、all ceramic tiles under normal conditions of use.Depending on the water absorption of the tiles, different procedures (tests with or without immersion) are used unless there is an agreement to the contrary.NOTE ISO 13006 provides property requirements for tiles and other useful information on these
26、products.2 Normative ReferencesThe following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 10545-3, Cerami
27、c tiles Part 3: Determination of water absorption, apparent porosity, apparent relative density and bulk density3 PrincipleDetermination of the resistance to thermal shock of a whole tile by cycling 10 times between the temperatures of 15 C and 145 C.4 Apparatus4.1 Low-temperature water bath, throug
28、h which cold water flows at (15 5) C.One example is a bath 55 cm long, 35 cm wide and 20 cm deep, with a water flowrate of 4 l/min. Any other suitable apparatus may be used.For the case of testing with immersion, applicable to all tiles having a water absorption coefficient less than or equal to a m
29、ass fraction of 10 % (determined in accordance with ISO 10545-3), the bath shall not be covered and shall be of sufficient depth to allow the tiles to be placed vertically and immersed completely.For the case of testing without immersion, applicable to glazed tiles having a water absorption coeffici
30、ent greater than a mass fraction of 10 % (determined in accordance with ISO 10545-3), the bath shall be covered with a thick aluminium plate in such a manner that the water, directed towards the surface, is in contact with the plate. The aluminium plate shall be covered with a layer approximately th
31、ick of 5 mm aluminium granules with diameters in the range of 0,3 mm to 0,6 mm.4.2 Oven, capable of being operated at 145 C to 150 C.DIN EN ISO 10545-9:2013-12 EN ISO 10545-9:2013 (E) 4 5 Test specimensTest specimens shall be selected at random from the lot to be tested. A minimum of five whole tile
32、s shall be tested.6 Procedure6.1 Preliminary check of the test specimensFirst examine the tiles for visible defects by viewing them with the naked eye (or with the aid of spectacles if usually worn) from a distance of 25 cm to 30 cm under a minimum illumination of 300 lux. All test specimens shall b
33、e free from defects at the commencement of the test. The methylene blue solution described in 6.5 may be used to detect pre-test defects.6.2 Test with immersionIn the case of low-porosity tiles having a water absorption coefficient less than or equal to 10 % of their dry masses, immerse them vertica
34、lly in cold water at (15 5) C so that the tiles are not in contact with each other.6.3 Test without immersionIn the case of glazed tiles having a water absorption coefficient greater than 10 % of their dry mass fractions, place the glazed face downwards in contact with the aluminium granules over th
35、e cold-water bath (4.1) maintained at (15 5) C.6.4 Temperature cyclingFor both tests, after 15 min at the low temperature, immediately transfer the test specimens to the oven (4.2) maintained at (145 5) C until a uniform temperature is achieved (usually 20 min), then immediately transfer them back t
36、o the low-temperature conditions.Repeat this process 10 times.6.5 ExaminationThen examine the test specimens for visible defects by viewing them with the naked eye (or with the aid of spectacles if usually worn) from a distance of 25 cm to 30 cm under a minimum illumination of 300 lux. To assist in
37、detecting defects, a suitable stain (such as a 1 % aqueous solution of methylene blue containing a small quantity of wetting agent) may be brushed onto the proper surfaces of the test specimens. After 1 min, wipe off the stain with a damp cloth.7 Test reportThe test report shall include the followin
38、g information:a) reference to this part of ISO 10545, i.e. ISO 10545-9:2013;b) a description of the tiles;c) the water absorption coefficient of the tiles;d) the type of test performed (with or without immersion);e) the number of test specimens with visible defects.DIN EN ISO 10545-9:2013-12 EN ISO 10545-9:2013 (E) 5 BibliographyISO 13006, Ceramic tiles Definitions, classification, characteristics and markingDIN EN ISO 10545-9:2013-12 EN ISO 10545-9:2013 (E) 6
