1、June 2010 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83
2、.180!$f3L“1671641www.din.deDDIN EN ISO 11339Adhesives T-peel test for flexible-to-flexible bonded assemblies (ISO 11339:2010)English translation of DIN EN ISO 11339:2010-06Klebstoffe T-Schlprfung fr geklebte Verbindungen aus flexiblen Fgeteilen (ISO 11339:2010)Englische bersetzung von DIN EN ISO 113
3、39:2010-06Adhsifs Essai de pelage en T dassemblages colls flexible sur flexible (ISO 11339:2010)Traduction anglaise de DIN EN ISO 11339:2010-06SupersedesDIN EN ISO 11339:2005-08www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered authoritative.1105.1
4、0 DIN EN ISO 11339:2010-06 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 61 “Plastics” in collaboration with Technical Committee CEN/TC 193 “Adhesives” (Secretariat: AENOR, Spain). The responsible German body involved in its pr
5、eparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Technical Committee NA 062-04-55 AA Prfung von Konstruktionsklebstoffen, -klebverbindungen und Kernverbunden. The DIN Standards corresponding to the International Standards referred to in this document are as f
6、ollows: ISO 291 DIN EN ISO 291 ISO 10365 DIN EN ISO 10365 Amendments This standard differs from DIN EN ISO 11339:2005-08 as follows: a) A safety statement has been included. b) Adherend materials have been given in more detail. c) The peel strength values calculated are now reported in newtons per 1
7、00 mm of specimen width. d) The standard has been editorially revised. Previous editions DIN EN ISO 11339: 2005-08 DIN EN 14173: 2002-04 National Annex NA (informative) Bibliography DIN EN ISO 291, Plastics Standard atmospheres for conditioning and testing DIN EN ISO 10365, Adhesives Designation of
8、main failure patterns 2 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 11339 February 2010 ICS 83.180 Supersedes EN ISO 11339:2005English Version Adhesives - T-peel test for flexible-to-flexible bonded assemblies (ISO 11339:2010) Adhsifs - Essai de pelage en T dassemblages colls flexible s
9、ur flexible (ISO 11339:2010) Klebstoffe - T-Schlprfung fr geklebte Verbindungen aus flexiblen Fgeteilen (ISO 11339:2010) This European Standard was approved by CEN on 11 February 2010. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving
10、 this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official versi
11、ons (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium,
12、 Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTE
13、E FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 11339:2010: EContents Page Foreword 3
14、1 Scope4 2 Normative references4 3 Terms and definitions .4 4 Principle5 5 Apparatus.5 6 Test specimens5 7 Procedure.6 8 Expression of results7 9 Precision.710 Test report8 Bibliography9 EN ISO 11339:2010 (E) DIN EN ISO 11339:2010-06 2Foreword This document (EN ISO 11339:2010) has been prepared by T
15、echnical Committee ISO/TC 61 “Plastics“ in collaboration with Technical Committee CEN/TC 193 “Adhesives” the secretariat of which is held by AENOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by
16、August 2010, and conflicting national standards shall be withdrawn at the latest by August 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such pate
17、nt rights. This document supersedes EN ISO 11339:2005. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finl
18、and, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 11339:2010 has been approved by CEN as a EN
19、ISO 11339:2010 without any modification. EN ISO 11339:2010 (E) DIN EN ISO 11339:2010-06 3SAFETY STATEMENT Persons using this document should be familiar with normal laboratory practice, if applicable. This document does not purport to address all of the safety problems, if any, associated with its u
20、se. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any regulatory conditions. It is recognized that some of the materials permitted in this document may have a negative environmental impact. As technological advances lead to mo
21、re acceptable alternatives for such materials, they will be eliminated to the greatest extent possible. At the end of the test, care should be taken to dispose of all waste in an appropriate manner in accordance with local regulations. 1 Scope This International Standard specifies a T-peel test for
22、the determination of the peel strength of an adhesive by measuring the peeling force of a T-shaped bonded assembly of two flexible adherends. This test procedure does not provide design information. NOTE This method was originally developed for use with metal adherends but other, flexible, adherends
23、 may also be used. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 291
24、, Plastics Standard atmospheres for conditioning and testing ISO 10365, Adhesives Designation of main failure patterns ISO 17212, Structural adhesives Guidelines for the surface preparation of metals and plastics prior to adhesive bonding 3 Terms and definitions For the purposes of this document, th
25、e following terms and definitions apply. 3.1 peel strength force per unit width necessary to bring an adhesive joint to the point of failure and/or maintain a specified rate of failure by means of a stress applied in a peeling mode ISO 472:1999 EN ISO 11339:2010 (E) DIN EN ISO 11339:2010-06 43.2 fle
26、xible adherend adherend having dimensions and physical properties that permit bending through any angle up to 90 without breaking or cracking 4 Principle For the T-peel test for a flexible-to-flexible assembly, the force is applied to the unbonded ends of the specimen. The angle between the bond lin
27、e and the direction of the applied force is not fixed. Adherends are separated at an approximately steady rate from an open edge of a prepared bond so that separation occurs progressively along the bond line. 5 Apparatus 5.1 Tensile-testing machine1), capable of maintaining a predetermined constant
28、crosshead rate (preferred rate 100 mm/min). It shall be provided with a suitable self-aligning grip to hold the specimen. Each set of jaws of the grip shall firmly engage the outer 25 mm of the unbonded ends of the flexible adherends. The grip and attachments shall be constructed in such a way that
29、they will move into alignment with the specimen as soon as the force is applied. The machine shall produce a chart that can be read in terms of millimetres of crosshead movement as a function of the applied force. The machine shall permit the measurement and recording of the applied force with an ac
30、curacy of 2 %. All equipment shall be calibrated regularly. It is recommended that a clamping device with low inertia be used. 5.2 Device for measuring thickness, with an accuracy of 0,01 mm, or a means of checking the thickness to that tolerance. 6 Test specimens 6.1 Test specimens of the dimension
31、s shown in Figure 1 shall be prepared, either individually or cut from bonded laminates. Test specimens shall consist of two flexible adherends properly prepared and bonded together. 6.2 Surface treatment shall be such as to obtain optimum strength in the bonded assembly. The preparation of the surf
32、ace shall be in accordance with ISO 17212, and details of the preparation shall be stated in the test report. The adhesive shall be applied in accordance with the manufacturers instructions to obtain an optimum bond with minimum variation; the procedure used shall be reported in the test report. NOT
33、E Direct comparison of different adhesives can be made only when specimen construction, adherend materials and dimensions, and test conditions are identical. 6.3 The thickness of the flexible adherends shall be reported. The preferred thicknesses are 0,5 mm 0,02 mm for steel (type XES)2)and 0,7 mm 0
34、,02 mm or 0,5 mm 0,02 mm for aluminium (type 5754, H111)3)unless otherwise specified. 1) See for instance ISO 58934. 2) XES = low-carbon steel: composition (in mass %) C = 0,05, Cr 0,01, Cu = 0,013, Mn = 0,018, Al = 0,064, Ni = 0,02; Youngs modulus E = 210 GPa; initial yield stress y= 150 MPa; strai
35、n-hardening coefficient = 0,4. 3) See ISO 2091and ISO 21073. EN ISO 11339:2010 (E) DIN EN ISO 11339:2010-06 56.4 Test specimens shall be cut from the bonded panels (see Figure 1) by a method that is not deleterious to the bond. The width shall be either a) 25 mm (preferred width) or b) any other con
36、venient width, provided that the test equipment is suitably adapted and the width is stated in the test report. NOTE The method of cutting the specimens is dependent upon the adherend and adhesive compositions and the specimen width tolerance specified in Figure 1. Milling and bandsawing are two met
37、hods commonly used for this purpose. 6.5 Before the test is carried out, the test specimen shall be bent in a manner that does not affect the bonded joint. The two unbonded ends of the flexible adherends shall be bent in opposite directions until each end is perpendicular to the bonded assembly, to
38、form a T-shaped specimen (see Figure 1) for clamping in the grips of the test machine. 6.6 The number of specimens tested shall be not less than five. 6.7 The specimens shall be conditioned and tested in one of the standard laboratory atmospheres specified in ISO 291, which shall be reported in the
39、test report. 7 Procedure On the at least five specimens, using the device described in 5.2, measure with an accuracy of 0,01 mm the average thickness of the adhesive layer after formation of the bond. Clamp each unbonded end of the T-shaped specimen in the grips of the test machine, taking care that
40、 the end is accurately aligned between the grips so that the tension applied is distributed evenly across the width. If one adherend is more flexible than the other, attach the less flexible adherend to the moveable grip. Set the machine in motion at the selected separation rate and record the force
41、 applied versus the distance of grip separation. NOTE A separation rate of 100 mm/min is generally used for metals and 10 mm/min for other adherends. Continue the test until at least 150 mm of the bonded length is separated. Note the type of failure in accordance with ISO 10365. EN ISO 11339:2010 (E
42、) DIN EN ISO 11339:2010-06 6Dimensions in millimetres Key 1 specimen cut at panel edge 2 specimen 3 direction of pull aBonded. bUnbonded. Figure 1 Panel before cutting and individual specimen after cutting 8 Expression of results Determine from the recorded curve, for about 100 mm of peeling (disreg
43、arding the first 25 mm and the last 25 mm), the average, maximum and minimum peeling force, in newtons, required to separate the adherends. The average force shall be determined from the curve by drawing the best straight line, or by using other suitable means if a more accurate result is required.
44、Record the average, maximum and minimum peeling forces for each individual specimen. From the peeling forces thus recorded, calculate the average, maximum and minimum peel strengths for each individual specimen, in newtons per 100 mm of specimen width. 9 Precision The precision of this test method i
45、s not known because interlaboratory data are not available. When interlaboratory data are obtained, a precision statement will be added at the following revision. EN ISO 11339:2010 (E) DIN EN ISO 11339:2010-06 710 Test report The test report shall include the following information: a) a reference to
46、 this International Standard; b) all information necessary for complete identification of the adhesive tested, including type, source, manufacturers code number, batch or lot number, form, etc.; c) all information necessary for complete identification of the adherends, including the nature and the t
47、hickness of the material, the width and the surface preparation; d) a description of the bonding process, including the method of application of the adhesive, the drying or precuring conditions (where applicable) and the curing time, temperature and pressure; e) the average thickness of the adhesive
48、 layer after formation of the bond; f) a complete description of the specimen, whether individual or cut from a panel, including the dimensions and construction of the specimen, the conditions used for cutting out individual specimens, the number of test panels represented and the number of individu
49、al specimens (when edge specimens are tested, they shall be designated “edge specimens”); g) the conditioning procedure used prior to testing and the test atmosphere; h) the crosshead separation rate; i) the method for determining the average peeling force; j) the average, maximum and minimum peeling force values, in newtons, for each individual specimen (edge specimens shall be reported separately); k) the calculated average, maximum and minimum peel strength values, in newtons per 100 mm of specimen width, for each s
