1、February 2011 Translation by DIN-Sprachendienst.English price group 7No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).IC
2、S 87.040!$mP2“1744515www.din.deDDIN EN ISO 8130-12Coating powders Part 12: Determination of compatibility (ISO 8130-12:1998)English translation of DIN EN ISO 8130-12:2011-02Pulverlacke Teil 12: Bestimmung der Mischbarkeit (ISO 8130-12:1998)Englische bersetzung von DIN EN ISO 8130-12:2011-02Poudres p
3、our revtement Partie 12: Dtermination de la compatibilit (ISO 8130-12:1998)Traduction anglaise de DIN EN ISO 8130-12:2011-02SupersedesDIN ISO 8130-12:2005-03www.beuth.deDocument comprises pagesIn case of doubt, the German-language original shall be considered authoritative.11 02.11 DIN EN ISO 8130-1
4、2:2011-02 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes”, Subcommittee SC 9 “General test methods for paints and varnishes” (Secretariat: BSI, United Kingdom) in collaboration with Technical Committee
5、 CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe und Beschichtungen (Coatings and Coating Materials Standards Committee), Working Committee NA 002-00-07 AA Allgemeine Prfverfahren fr Be
6、schichtungsstoffe und Beschichtungen. DIN EN ISO 8130 consists of the following parts, under the general title Coating powders: Part 1: Determination of particle size distribution by sieving Part 2: Determination of density by gas comparison pyknometer (referee method) Part 3: Determination of densi
7、ty by liquid displacement pyknometer Part 4: Calculation of lower explosion limit Part 5: Determination of flow properties of a powder/air mixture Part 6: Determination of gel time of thermosetting coating powders at a given temperature Part 7: Determination of loss of mass on stoving Part 8: Assess
8、ment of the storage stability of thermosetting powders Part 9: Sampling Part 10: Determination of deposition efficiency Part 11: Inclined-plane flow test Part 12: Determination of compatibility Part 13: Particle size analysis by laser diffraction Part 14: Terminology The DIN Standards corresponding
9、to the International Standards referred to in this document are as follows: ISO 1514 DIN EN ISO 1514 ISO 2813 DIN EN ISO 2813 ISO 8130-9 DIN EN ISO 8130-9 DIN EN ISO 8130-12:2011-02 3 Amendments This standard differs from DIN ISO 8130-12:2005-03 as follows: a) the status of the standard has been cha
10、nged to that of a European Standard. Previous editions DIN ISO 8130-12: 2005-03 National Annex NA (informative) Bibliography DIN EN ISO 1514, Paints and varnishes Standard panels for testing DIN EN ISO 2813, Paints and varnishes Determination of specular gloss of non-metallic paint films at 20, 60 n
11、d 85 DIN EN ISO 8130-9, Coating powders Part 9: Sampling aDIN EN ISO 8130-12:2011-02 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 8130-12 November 2010 ICS 87.040 English Version Coating powders - Part 12: Determination of compatibility (ISO 8130-12:199
12、8) Poudres pour revtement - Partie 12: Dtermination de la compatibilit (ISO 8130-12:1998) Pulverlacke - Teil 12: Bestimmung der Mischbarkeit (ISO 8130-12:1998) This European Standard was approved by CEN on 16 October 2010. CEN members are bound to comply with the CEN/CENELEC Internal Regulations whi
13、ch stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European S
14、tandard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national
15、 standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland
16、 and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO
17、 8130-12:2010: EContents DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2010 (E) 2 Page Foreword3 1 Scope 4 2 Normative references 5 3 Principle5 4 Apparatus .5 5 Sampling.5 6 Procedure .6 7 Expression of results 6 8 Precision.7 9 Test report 7 Foreword The text of ISO 8130-12:1998 has been prepared by T
18、echnical Committee ISO/TC 35 “Paints and varnishes” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 8130-12:2010 by Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which is held by DIN. This European Standard shall be given the s
19、tatus of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2011, and conflicting national standards shall be withdrawn at the latest by May 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject
20、of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgar
21、ia, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice T
22、he text of ISO 8130-12:1998 has been approved by CEN as a EN ISO 8130-12:2010 without any modification. 3 DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2010 (E) 1ScopeThis part of ISO 8130 is one of a series of standards dealing with the sampling and testing of paints,varnishes and related products.It s
23、pecifies a method for the determination of the tendency for the mixing of two different coating powdersto result in the deterioration of the surface quality of the final coating. The results depend on the followingcharacteristics of the coating powders:a) their chemical reactivity;b) their chemical
24、composition;c) their melt properties.The onset of the deterioration in appearance, its nature and its extent will depend greatly on the ratio inwhich the powders are mixed.The test is useful in predicting the possibility of incompatibility arising from mixing different powders bothduring the manufac
25、turing process and during the application of the coating powder.The nature of the deterioration in surface appearance may manifest itself in various ways, including:- change in gloss level;- the presence of pinholes, including micro-pinholes;- the appearance of orange peel;- the presence of craters;
26、- the presence of bittiness (graininess);- the presence of colour contamination.NOTE Deterioration in mechanical properties may also be experienced. However, this part of ISO 8130 isonly concerned with changes in appearance.DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2010 (E) 4 2 Normative referencesT
27、he following standards contain provisions which, through reference in this text, constitute provisions of thispart of ISO 8130. At the time of publication, the editions indicated were valid. All standards are subject torevision, and parties to agreements based on this part of ISO 8130 are encouraged
28、 to investigate thepossibility of applying the most recent editions of the standards indicated below. Members of IEC and ISOmaintain registers of currently valid International Standards.ISO 8130-9:1992, Coating powders Part 9: Sampling.ISO 1514:1993, Paints and varnishes Standard panels for testing.
29、ISO 2813:1994, Paints and varnishes Determination of specular gloss of non-metallic paint films at 20,60 and 85.3 PrincipleThe coating powders are mixed together in a range of ratios and each mixture is applied to standard testpanels, stoved and the surface inspected for evidence of incompatibility.
30、4 ApparatusOrdinary laboratory apparatus, together with the following:4.1 Clean and degreased steel panels, as described in ISO 1514, with holes drilled at one end forhanging.4.2 Powder spray system, consisting of a corona charge gun or a tribo charge gun and an air extractionspray booth with a suit
31、able powder collection device.4.3 Suitable clean container, capable of holding a mass of the powder suitable for processing in thespray system (4.2).NOTE Plastic bags have been found to be suitable for non-metallic powders.4.4 Balance, accurate to 10 mg.4.5 Oven, capable of stoving the coated test p
32、anels.5 SamplingPrepare a representative sample of the powder under test, as described in ISO 8130-9. The quantity ofpowder required will depend on the powder spray system (4.2).NOTE A quantity of between 10 g and 200 g is normally suitable for each test.5 DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2
33、010 (E) 6 ProcedureCarry out the test in duplicate.6.1 In the absence of agreement between the interested parties, prepare mixtures in the following massratios in a quantity required for the test, weighing each component to an accuracy of 10 mg:Powder A 100,0 99,9 99,0 90,0 50,0 10,0 1,0 0,1 0,0Powd
34、er B 0,0 0,1 1,0 10,0 50,0 90,0 99,0 99,9 100,06.2 Place each of the samples prepared in 6.1 in a clean container (4.3) and agitate for sufficient time toensure complete homogenization.NOTE Vigorous shaking by hand of a partially filled container for 15 s to 30 s has proved to be adequate.6.3 Spray
35、each of the mixed samples onto a test panel (4.1), using the spray gun (4.2), to a thicknessappropriate to the application.It is extremely important that the spraying apparatus is thoroughly cleaned between each application. In anycase, it is mandatory that the order of application of the samples be
36、 in increasing order of each minorconstituent, thus:100,0 A : 0,0 B to 50,0 A : 50,0 Band then:100,0 B : 0,0 A to 90,0 B : 10,0 A.6.4 Place the coated panels in the oven (4.5) and stove in accordance with the prescribed stovingschedule of the slower-reacting component. If no schedule is available, i
37、t shall be agreed on between theinterested parties.6.5 Remove the panels from the oven and allow to cool.6.6 Examine the coated surfaces for pinholes, craters and other imperfections.NOTE Where appropriate, a quantitative measure of change in gloss may be obtained by measuring glossvalues in accorda
38、nce with ISO 2813.7 Expression of resultsA verbal description of the appearance of the coatings will be sufficient for the purposes of this standardmethod. Where quantitative measurements of gloss have been undertaken, these shall be quoted numerically.NOTE As very small amounts of contamination can
39、 greatly influence the level of gloss, it may be useful toplot the gloss measurements graphically. In this case, it is recommended that a probability chart be employedin which the gloss measurements are plotted as abscissae and the mass ratios of the powders in the mixtureare plotted as a probabilit
40、y distribution on the ordinate scale. In this way, it is possible to obtain acompatibility curve in which the influence of small concentrations of one powder on the other are clearlydemonstrated.DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2010 (E) 6 8 PrecisionPrecision data are inappropriate for non-
41、quantitative measurements. The precision of any glossmeasurements shall be as detailed in ISO 2813.9 Test reportThe test report shall contain the following information:a) all details necessary to identify the products tested;b) a reference to this part of ISO 8130 (ISO 8130-12);c) the recommended st
42、oving schedule for each powder;d) the stoving schedule used in the test, if no schedule is available (see 6.4);e) the gun used, i.e. either corona or tribo (see 4.2);f) the coating thickness;g) the results of the test as indicated in clause 7;h) any deviation from the test method specified;i) the date of the test.7 DIN EN ISO 8130-12:2011-02 EN ISO 8130-12:2010 (E)
