1、BSI Standards PublicationBS EN 12697-41:2013Bituminous mixtures Testmethods for hot mix asphaltPart 41: Resistance to de-icing fluidsBS EN 12697-41:2013 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 12697-41:2013.It supersedes BS EN 12697-41:2005 which is with
2、drawn.The UK participation in its preparation was entrusted to TechnicalCommittee B/510/1, Asphalt products.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users a
3、re responsible for its correctapplication. The British Standards Institution 2014. Published by BSI StandardsLimited 2014ISBN 978 0 580 82145 5ICS 93.080.20Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theSt
4、andards Policy and Strategy Committee on 28 February 2014.Amendments issued since publicationDate Text affectedBS EN 12697-41:2013EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 12697-41 December 2013 ICS 93.080.20 Supersedes EN 12697-41:2005English Version Bituminous mixtures - Test methods fo
5、r hot mix asphalt - Part 41: Resistance to de-icing fluids Mlanges bitumineux - Mthodes dessai pour mlange hydrocarbon chaud - Partie 41: Rsistance aux fluides de dverglaage Asphalt - Prfverfahren fr Heiasphalt - Teil 41: Widerstand gegen chemische Auftaumittel This European Standard was approved by
6、 CEN on 26 October 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national stand
7、ards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and no
8、tified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary,
9、Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC M
10、anagement Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 12697-41:2013: EBS EN 12697-41:2013EN 12697-41:2013 (E) 2 Contents Page Foreword 3 1 Scope 6 2 Normative references 6 3 Term a
11、nd definition6 4 Principle 6 5 Apparatus .7 6 Solvent and other materials 8 7 Preparation of test specimens .8 8 Procedure .9 9 Calculation and expression of results .9 10 Report 10 11 Precision 11 Bibliography . 12 BS EN 12697-41:2013EN 12697-41:2013 (E) 3 Foreword This document (EN 12697-41:2013)
12、has been prepared by Technical Committee CEN/TC 227 “Road materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2014, and conflicting national s
13、tandards shall be withdrawn at the latest by June 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 12
14、697-41:2005. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association. This document is one of a series of standards as listed below: EN 12697-1, Bituminous mixtures Test methods for hot mix asphalt Part 1: Soluble binder content
15、 EN 12697-2, Bituminous mixtures Test methods for hot mix asphalt Part 2: Determination of particle size distribution EN 12697-3, Bituminous mixtures Test methods for hot mix asphalt Part 3: Bitumen recovery: Rotary evaporator EN 12697-4, Bituminous mixtures Test methods for hot mix asphalt Part 4:
16、Bitumen recovery: Fractionating column EN 12697-5, Bituminous mixtures Test methods for hot mix asphalt Part 5: Determination of the maximum density EN 12697-6, Bituminous mixtures Test methods for hot mix asphalt Part 6: Determination of bulk density of bituminous specimens EN 12697-7, Bituminous m
17、ixtures Test methods for hot mix asphalt Part 7: Determination of bulk density of bituminous specimens by gamma rays EN 12697-8, Bituminous mixtures Test methods for hot mix asphalt Part 8: Determination of void characteristics of bituminous specimens EN 12697-10, Bituminous mixtures Test methods fo
18、r hot mix asphalt Part 10: Compactibility EN 12697-11, Bituminous mixtures Test methods for hot mix asphalt Part 11: Determination of the affinity between aggregate and bitumen EN 12697-12, Bituminous mixtures Test methods for hot mix asphalt Part 12: Determination of the water sensitivity of bitumi
19、nous specimens EN 12697-13, Bituminous mixtures Test methods for hot mix asphalt Part 13: Temperature measurement EN 12697-14, Bituminous mixtures Test methods for hot mix asphalt Part 14: Water content BS EN 12697-41:2013EN 12697-41:2013 (E) 4 EN 12697-15, Bituminous mixtures Test methods for hot m
20、ix asphalt Part 15: Determination of the segregation sensitivity EN 12697-16, Bituminous mixtures Test methods for hot mix asphalt Part 16: Abrasion by studded tyres EN 12697-17, Bituminous mixtures Test methods for hot mix asphalt Part 17: Particle loss of porous asphalt specimen EN 12697-18, Bitum
21、inous mixtures Test methods for hot mix asphalt Part 18: Binder drainage EN 12697-19, Bituminous mixtures Test methods for hot mix asphalt Part 19: Permeability of specimen EN 12697-20, Bituminous mixtures Test methods for hot mix asphalt Part 20: Indentation using cube or cylindrical specimens (CY)
22、 EN 12697-21, Bituminous mixtures Test methods for hot mix asphalt Part 21: Indentation using plate specimens EN 12697-22, Bituminous mixtures Test methods for hot mix asphalt Part 22: Wheel tracking EN 12697-23, Bituminous mixtures Test methods for hot mix asphalt Part 23: Determination of the indi
23、rect tensile strength of bituminous specimens EN 12697-24, Bituminous mixtures Test methods for hot mix asphalt Part 24: Resistance to fatigue EN 12697-25, Bituminous mixtures Test methods for hot mix asphalt Part 25: Cyclic compression test EN 12697-26, Bituminous mixtures Test methods for hot mix
24、asphalt Part 26: Stiffness EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sampling EN 12697-28, Bituminous mixtures Test methods for hot mix asphalt Part 28: Preparation of samples for determining binder content, water content and grading EN 12697-29, Bituminous mixtures
25、Test methods for hot mix asphalt Part 29: Determination of the dimensions of a bituminous specimen EN 12697-30, Bituminous mixtures Test methods for hot mix asphalt Part 30: Specimen preparation by impact compactor EN 12697-31, Bituminous mixtures Test methods for hot mix asphalt Part 31: Specimen p
26、reparation by gyratory compactor EN 12697-32, Bituminous mixtures Test methods for hot mix asphalt Part 32: Laboratory compaction of bituminous mixtures by vibratory compactor EN 12697-33, Bituminous mixtures Test methods for hot mix asphalt Part 33: Specimen prepared by roller compactor EN 12697-34
27、, Bituminous mixtures Test methods for hot mix asphalt Part 34: Marshall test EN 12697-35, Bituminous mixtures Test methods for hot mix asphalt Part 35: Laboratory mixing BS EN 12697-41:2013EN 12697-41:2013 (E) 5 EN 12697-36, Bituminous mixtures Test methods for hot mix asphalt Part 36: Determinatio
28、n of the thickness of a bituminous pavement EN 12697-37, Bituminous mixtures Test methods for hot mix asphalt Part 37: Hot sand test for the adhesivity of binder on pre-coated chippings for HRA EN 12697-38, Bituminous mixtures Test methods for hot mix asphalt Part 38: Common equipment and calibratio
29、n EN 12697-39, Bituminous mixtures Test methods for hot mix asphalt Part 39: Binder content by ignition EN 12697-40, Bituminous mixtures Test methods for hot mix asphalt Part 40: In situ drainability EN 12697-41, Bituminous mixtures Test methods for hot mix asphalt Part 41: Resistance to de-icing fl
30、uids EN 12697-42, Bituminous mixtures Test methods for hot mix asphalt Part 42: Amount of foreign matter in reclaimed asphalt EN 12697-43, Bituminous mixtures Test methods for hot mix asphalt Part 43: Resistance to fuel EN 12697-44, Bituminous mixtures Test methods for hot mix asphalt Part 44: Crack
31、 propagation by semi-circular bending test EN 12697-45, Bituminous mixtures Test methods for hot mix asphalt Part 45: Saturation ageing tensile stiffness (SATS) conditioning test EN 12697-46, Bituminous mixtures Test methods for hot mix asphalt Part 46: Low temperature cracking and properties by uni
32、axial tension tests EN 12697-47, Bituminous mixtures Test methods for hot mix asphalt Part 47: Determination of the ash content of natural asphalts prEN 12697-48, Bituminous mixtures Test methods for hot mix asphalt Part 48: Interlayer Bonding (Torque bond test TBT, Shear bond test SBT, Tensile Adhe
33、sion Test TAT) prEN 12697-49, Bituminous mixtures Test methods for hot mix asphalt Part 49: Determination of friction after polishing prCEN/TS 12697-50, Bituminous mixtures Test methods for hot mix asphalt Part 50: Resistance to scuffing According to the CEN-CENELEC Internal Regulations, the nationa
34、l standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithua
35、nia, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN 12697-41:2013EN 12697-41:2013 (E) 6 1 Scope This European Standard specifies a test method to determine the resistance of bituminous materials
36、to de-icing fluids such as solutions of acetate and formate. The procedure determines the surface tensile strength of a specimen of asphalt which has been stored in de-icing fluid. This European Standard is primarily used as a test on asphalt to be laid on airfields, but it can be used for asphalt t
37、o be laid on roads or other paved areas. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the
38、 referenced document (including any amendments) applies. EN 12697-6, Bituminous mixtures Test methods for hot mix asphalt Part 6: Determination of bulk density of bituminous specimens EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sampling EN 12697-30, Bituminous mixtures
39、 Test methods for hot mix asphalt Part 30: Specimen preparation by impact compactor EN 12697-31, Bituminous mixtures Test methods for hot mix asphalt Part 31: Specimen preparation by gyratory compactor EN 12697-32, Bituminous mixtures Test methods for hot mix asphalt Part 32: Laboratory compaction o
40、f bituminous mixtures by vibratory compactor EN 12697-33, Bituminous mixtures Test methods for hot mix asphalt Part 33: Specimen prepared by roller compactor EN 12697-35, Bituminous mixtures Test methods for hot mix asphalt Part 35: Laboratory mixing 3 Term and definition For the purposes of this do
41、cument, the following terms and definitions apply. 3.1 surface tensile strength tensile stress at maximum force when testing the surface tensile strength according to this test method 4 Principle Testing is performed on a sawn cylindrical specimen of asphalt on which a well-defined test surface has
42、been drilled out in the bituminous mixture to a depth of about 5 mm. Four specimens are stored and four are not stored in a de-icing fluid. A steel plate is bonded to the test surface of each specimen in turn. During testing, the plate is pulled off with a tensile force increasing at a rate of 200 N
43、/s, the force being applied perpendicular to the test specimen surface. The tensile force at failure load and the mode of failure are recorded. The results are compared with those for specimens which have not been stored in de-icing fluid. BS EN 12697-41:2013EN 12697-41:2013 (E) 7 5 Apparatus 5.1 Ve
44、ssel with a tight-fitting lid for storing specimens in the de-icing fluid. 5.2 Vacuum desiccator. 5.3 Vacuum pump for evacuation of the desiccator. The pump shall be capable of achieving a pressure of 6,7 kPa within 10 min and maintaining this pressure within 0,3 kPa throughout the vacuum treatment.
45、 5.4 Coring rig (optional). 5.5 Steel plates with a diameter of 50 mm and a tolerance of 0,5 mm. The steel plate shall be attached by suitable means (e.g. screwed) to the tensile test machine. Minimum thickness of steel plate shall be 10 mm from bottom of steel plate to bottom of screw hole. 5.6 Bas
46、e and holder for fixing the specimen prior to testing (see Figure 1). Figure 1 Example of base, test specimen and tensile test machine 5.7 Tensile test machine, with force increasing rate control and automatic load recording fitted with suitable clamps and base to ensure that the tensile force can b
47、e applied without momentum perpendicular to the test specimen. 5.8 Circular saw capable of cutting asphalt with finish that has no imperfections discernible by touch. 5.9 Equipment for drilling out a test surface. BS EN 12697-41:2013EN 12697-41:2013 (E) 8 5.10 Conditioning device capable of maintain
48、ing a constant temperature of (23 1) C. 5.11 Heating cabinet capable of maintaining a constant temperature of (40 2) C. 6 Solvent and other materials 6.1 Epoxy adhesive. 6.2 Desiccator grease. 6.3 De-icing fluid, the concentration of which shall correspond to the highest concentration intended for use on site. 7 Preparation of test specimens 7.1 Prepare a laboratory sample of asphalt mixture in accordance with EN 12697-35 or at an asphalt mixing plant. 7.2 Compact a sample of a height of (60 10) mm by roller compactor in accorda