1、BS EN ISO10416:2009ICS 75.180.10NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBRITISH STANDARDPetroleum and naturalgas industries Drilling fluids Laboratory testingNational forewordThis British Standard is the UK implementation of EN ISO 10416:2009. It is identical to ISO 104
2、16:2008. It supersedes BS ISO 10416:2008 which is withdrawn.The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, to Subcommittee PSE/17/-/3, Drilling and completion fluids and well cement
3、s. A list of organizations represented on this subcommittee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunity
4、 from legal obligations.BS EN ISO 10416:2009This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 July 2008 BSI 2010ISBN 978 0 580 68013 7Amendments/corrigenda issued since publicationDate Comments 28 February 2010 This corrigendum renumbers BS
5、ISO 10416:2008 as BS EN ISO 10416:2009EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 10416 December 2009 ICS 75.100; 75.180.10 English Version Petroleum and natural gas industries - Drilling fluids - Laboratory testing (ISO 10416:2008) Industries du ptrole et du gaz naturel - Fluides de fo
6、rage -Essais en laboratoire (ISO 10416:2008) Erdl- und Erdgasindustrie - Bohrsplungen - Laborversuche (ISO 10416:2008) This European Standard was approved by CEN on 15 November 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving t
7、his European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official version
8、s (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, B
9、ulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STAND
10、ARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 10416:2009: EForeword The text of ISO 10416:2008
11、 has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 10416:2009 by Technical Committee CEN/TC 12 “Materi
12、als, equipment and offshore structures for petroleum, petrochemical and natural gas industries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2010
13、, and conflicting national standards shall be withdrawn at the latest by June 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. Ac
14、cording to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, La
15、tvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 10416:2008 has been approved by CEN as a EN ISO 10416:2009 without any modification. BS EN ISO 10416:2009EN IS
16、O 10416:2009 (E)ii ISO 2010iiiContents Page Introduction vii 1 Scope 1 2 Normative references 1 3 Terms and definitions .2 4 Symbols and abbreviations3 5 Barite.6 5.1 Principle6 5.2 Reagents and apparatus .6 5.3 Sampling.7 5.4 Calculation of moisture content.7 5.5 Sieve analysis 7 5.6 Sedimentation
17、analysis.8 6 Barite performance12 6.1 Principle12 6.2 Reagents and apparatus .12 6.3 Base drilling fluid preparation13 6.4 Rheology test .13 6.5 Calculation14 7 Abrasiveness of weighting materials 14 7.1 Principle14 7.2 Reagents and apparatus .15 7.3 Determination of abrasion 15 8 Mercury in drillin
18、g fluid barite 17 8.1 Principle17 8.2 Reagents and apparatus .17 8.3 Preparation of standards 19 8.4 Sample digestion .19 8.5 Check for recovery of Hg during digestion.20 8.6 Analysis of standards and samples.20 8.7 Calculation20 9 Cadmium and lead in drilling fluid barite 21 9.1 Principle21 9.2 Rea
19、gents and apparatus .21 9.3 Preparation of combined cadmium and lead standards .22 9.4 Sample digestion .22 9.5 Analysis of standards and samples.22 9.6 Calculation23 10 Arsenic in drilling fluid barite .23 10.1 Principle23 10.2 Reagents and apparatus .24 10.3 Preparation of standards 25 10.4 Sample
20、 digestion .25 10.5 Analysis of standards and samples.26 10.6 Calculation26 11 Bridging materials for regaining circulation.26 BS EN ISO 10416:2009EN ISO 10416:2009 (E) ISO 2010iv 11.1 Principle . 26 11.2 Apparatus. 27 11.3 Preparation of test drilling fluid. 27 11.4 Static slot test 27 11.5 Dynamic
21、 slot test 28 11.6 Static marble bed test. 28 11.7 Dynamic marble bed test 28 11.8 Static ball bearings (BB shot) bed test . 29 11.9 Dynamic ball bearings (BB shot) bed test 29 12 Filtration-control agents. 29 12.1 Principle . 29 12.2 Reagents and apparatus 29 12.3 General instructions for preparati
22、on of base drilling fluids . 31 12.4 Salt-saturated drilling fluid. 31 12.5 High-hardness, salt-saturated drilling fluid 32 12.6 10 % potassium chloride (KCl) drilling fluid. 32 12.7 Pre-hydrated bentonite slurry 33 12.8 Modified seawater drilling fluid . 33 12.9 Low-salinity drilling fluid 33 12.10
23、 Lime-treated drilling fluid . 34 12.11 Low solids, non-dispersed drilling fluid . 34 12.12 Freshwater lignosulfonate drilling fluid 35 12.13 Initial performance test. 35 12.14 Performance after heat ageing 36 13 Methylene blue test for drilled solids and commerical bentonite 36 13.1 Methylene blue
24、capacity of drill solids . 36 13.2 Methylene blue capacity of commercial bentonite 39 13.3 Solids content 40 14 Deflocculation test for thinner evaluation 41 14.1 Principle . 41 14.2 Reagents and apparatus 42 14.3 Procedure for moisture content 43 14.4 Calculation of moisture content 43 14.5 Prepara
25、tion of drilling fluid base. 43 14.6 Calculation. 44 14.7 Determination of rheological properties. 44 14.8 Calculation of thinner efficiency 46 15 Testing base oils used in drilling fluids 46 15.1 General . 46 15.2 Reagents and apparatus 46 15.3 Density, relative density (specific gravity), or API g
26、ravity-hydrometer method (see ISO 3675) 46 15.4 Density and relative density of liquids using a digital density meter (see ASTM D 4052) 47 15.5 Kinematic viscosity of transparent and opaque oils Calibrated capillary tube method (see ISO 3104) 47 15.6 Distillation (see ISO 3405) 47 15.7 Aniline point
27、 and mixed aniline point (see ISO 2977:1997). 48 15.8 Pour point (see ISO 3016). 48 15.9 Flash point by Pensky-Martens closed tester (see ISO 2719) 49 15.10 Aromatics content (see IP 391 or ASTM D 5186) 49 16 Potassium ion content Ion-selective electrode method. 50 16.1 Principle . 50 16.2 Reagents
28、and apparatus 50 16.3 Preparation of electrodes. 51 16.4 Operational check of electrode system 51 16.5 Measurements using a meter with direct concentration readout capability 52 BS EN ISO 10416:2009EN ISO 10416:2009 (E) ISO 2010v16.6 Measurements with instruments that provide either a digital or an
29、analogue readout in millivolts .52 17 Calcium ion content Ion-selective electrode method53 17.1 Principle53 17.2 Reagents and apparatus .53 17.3 Preparation of electrodes .54 17.4 Operational check of electrode system.55 17.5 Measurements using a meter with direct concentration readout capability .5
30、5 17.6 Measurements with instruments that provide either a digital or an analogue readout in millivolts .55 18 Sodium ion content Ion-selective electrode method 56 18.1 Principle56 18.2 Reagents and apparatus .57 18.3 Preparation and operational check of the electrode system 57 18.4 Measurements usi
31、ng a meter with a direct concentration-readout capability58 18.5 Measurements using a meter with readout in millivolts58 19 Density of solids Stereopycnometer method.59 19.1 Principle59 19.2 Apparatus .59 19.3 Procedure Stereopycnometer method59 19.4 Calculation Stereopycnometer method 60 20 Density
32、 of solids Air comparison pycnometer method 61 20.1 Principle61 20.2 Apparatus .61 20.3 Procedure Air comparison pycnometer method .61 20.4 Calculation Air comparison pycnometer method61 21 Ageing of water-based drilling fluids.62 21.1 Principle62 21.2 Practices common to preparation, handling and t
33、esting over all temperature ranges62 21.3 Drilling fluid sample preparation and ageing at ambient temperature 63 21.4 Drilling fluid ageing at moderate temperatures ambient to 65 C (150 F)64 21.5 Drilling fluid ageing at substantially elevated temperatures over 65 C (150 F) .66 21.6 Inertness and ch
34、emical compatibility in high-temperature ageing cells.68 21.7 Obtaining supplies and services for the ageing of drilling fluid samples.69 22 Ageing of oil-based drilling fluids69 22.1 Principle69 22.2 Apparatus .70 22.3 Practices common to preparation, handling and testing over all temperature range
35、s71 22.4 Drilling fluid ageing at ambient temperatures 72 22.5 Drilling fluid ageing at moderate temperatures ambient to 65 C (150 F)73 22.6 Drilling fluid ageing at substantially elevated temperatures over 65 C (150 F) .74 22.7 Inertness and chemical compatibility in high-temperature ageing cells.7
36、5 22.8 Obtaining supplies and services for the ageing of drilling fluid samples.76 23 Shale-particle disintegration test by hot rolling .76 23.1 Principle76 23.2 Reagents and apparatus .77 23.3 Procedure .77 23.4 Calculation78 24 Drilling fluid materials High-viscosity polyanionic cellulose (PAC-HV)
37、 (regular)79 24.1 Principle79 24.2 Determination of moisture content79 24.3 Procedures with test fluid containing PAC-HV.80 25 Drilling fluid materials Low-viscosity polyanionic cellulose (PAC-LV).82 25.1 Principle82 25.2 Determination of moisture content83 BS EN ISO 10416:2009EN ISO 10416:2009 (E)
38、ISO 2010vi 25.3 Procedures with test fluid containing PAC-LV 83 26 Preparation and evaluation of invert-emulsion drilling fluids 86 26.1 Principle . 86 26.2 Reagents and apparatus 86 26.3 Mixing of the initial drilling fluid 87 26.4 Testing the properties of the initial drilling fluid . 88 26.5 Prep
39、aration of the sample contaminated by seawater 88 26.6 Preparation of the sample contaminated by base evaluation clay 89 26.7 Preparation of the sample contaminated by mixed-salt brine . 89 26.8 Procedure for hot-rolling 89 26.9 Procedure for static ageing 89 26.10 Procedure for testing after heat a
40、geing 90 27 High-temperature/high-pressure filtration testing of drilling fluids using the permeability plugging apparatus and cells with set-screw-secured end caps. 90 27.1 Principle . 90 27.2 Safety considerations. 90 27.3 Apparatus Permeability-plugging apparatus (PPA) with set-screw-secured end
41、caps 92 27.4 Procedure for high-temperature/high-pressure (HTHP) filtration 94 27.5 Test conclusion and disassembly. 97 27.6 Data reporting 99 28 High-temperature/high-pressure filtration testing of drilling fluids using the permeability-plugging apparatus and cells with threaded end caps . 100 28.1
42、 Principle . 100 28.2 Safety considerations. 100 28.3 Apparatus Permeability-plugging apparatus (PPA) with threaded end caps 102 28.4 Procedure for high-temperature/high-pressure (HTHP) filtration 104 28.5 Test conclusion and disassembly. 106 28.6 Data reporting 108 Bibliography . 109 BS EN ISO 1041
43、6:2009EN ISO 10416:2009 (E) ISO 2010vii Introduction This International Standard, which establishes testing methodologies for drilling fluid materials, is based on API RP 13I, seventh edition/ISO 10416:20022. This International Standard was developed in response to a demand for more exacting testing
44、 methodologies. The tests contained herein were developed over several years by a group of industry experts and were identified as being those which can yield reproducible and accurate results. The tests are anticipated to be performed in a laboratory setting, but can be applicable in a field situat
45、ion with more rigorous apparatus and conditions than normally found in a drilling fluid field-test kit. These tests are designed to assist in the evaluation of certain parameters for drilling fluids, with these properties not necessarily used for the maintenance of a drilling fluid in field use. The
46、 tests provide either more precision or different properties than those given in the field-testing standards ISO 10414-1 and ISO 10414-2. It is necessary that users of this International Standard be aware that further or differing requirements can be needed for individual applications. This Internat
47、ional Standard is not intended to inhibit a vendor from offering, or the purchaser from accepting, alternative equipment or engineering solutions for the individual application. This may be particularly appropriate where there is innovative or developing technology. Where an alternative is offered,
48、the vendor should identify any variations from this International Standard and provide details. As with any laboratory procedure requiring the use of potentially hazardous chemicals, the user is expected to have received proper knowledge and training in the use and disposal of these chemicals. The u
49、ser is responsible for compliance with all applicable local, regional, and national regulations for worker and local health, safety and environmental liability. This International Standard contains footnotes giving examples of apparatus, reagents and sometimes the supplier(s) of those materials that are available commercially. This information is given for the convenience of users of this International Standard and does not constitute an endorsement by ISO of the products named. Equivalent products may be used if they can be s
