1、BRITISH STANDARD BS EN ISO 20823:2003 Petroleum and related products Determination of the flammability characteristics of fluids in contact with hot surfaces Manifold ignition test The European Standard EN ISO 20823:2003 has the status of a British Standard ICS 75.080 BS EN ISO 20823:2003 This Briti
2、sh Standard was published under the authority of the Standards Policy and Strategy Committee on 13 August 2003 BSI 13 August 2003 ISBN 0 580 42451 0 National foreword This British Standard is the official English language version of EN ISO 20823:2003. It is identical with ISO 20823:2003 The UK parti
3、cipation in its preparation was entrusted to Technical Committee PTI/13, Petroleum testing and terminology, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement inter
4、national or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purp
5、ort to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committe
6、e any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO
7、foreword page, the ISO title page, pages ii and iii, a blank page, pages 1 to 5, the Annex ZA page, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. Date CommentsEUROPE
8、ANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO20823 August2003 ICS75.080 Englishversion PetroleumandrelatedproductsDeterminationofthe flammabilitycharacteristicsoffluidsincontactwithhotsurfaces Manifoldignitiontest(ISO20823:2003) PtroleetproduitsconnexesDterminationdes caractristiquesdinflammabilitd
9、efluidesaucontactde surfaceschaudesEssaidinflammationsurmtalchaud (ISO20823:2003) MinerallerzeugnisseundverwandteProdukte BestimmungderEntflammbarkeitsCharakteristikvon FlssigkeitenbeiKontaktmitheienOberflchen Zndverfahren(ISO20823:2003) ThisEuropeanStandardwasapprovedbyCENon2July2003. CENmembersare
10、boundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember. This
11、EuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheManagementCentrehasthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,Czec
12、hRepublic,Denmark,Finland,France,Germany,Greece, Hungary,Iceland,Ireland,Italy,Luxembourg,Malta,Netherlands,Norway,Portugal,Slovakia,Spain,Sweden,SwitzerlandandUn ited Kingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,
13、36B1050Brussels 2003CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO20823:2003EINESO02:3282003(E) 2 Foreword Thisdocument(ENISO20823:2003)hasbeenpreparedbyTechnicalCommitteeISO/TC28 “Petroleumproductsandlubricants“incollaborationwithTechnicalComm
14、itteeCEN/TC19 “Petroleumproducts,lubricantsandrelatedproducts“,thesecretariatofwhichisheldbyNEN. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationof anidenticaltextorbyendorsement,atthelatestbyFebruary2004,andconflictingnational standardsshallbewithdrawnatthelatestbyFe
15、bruary2004. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsof thefollowingcountriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Czech Republic,Denmark,Finland,France,Germany,Greece,Hungary,Iceland,Ireland,Italy, Luxembourg,Malta,Netherlands,Norway,Portugal,S
16、lovakia,Spain,Sweden,Switzerlandand theUnitedKingdom. Endorsementnotice ThetextofISO20823:2003hasbeenapprovedbyCENasENISO20823:2003withoutany modifications. NOTENormativereferencestoInternationalStandardsarelistedinAnnexZA(normative). ENISO20823:2003 Reference number ISO 20823:2003(E) OSI 3002INTERN
17、ATIONAL STANDARD ISO 20823 First edition 2003-08-01 Petroleum and related products Determination of the flammability characteristics of fluids in contact with hot surfaces Manifold ignition test Ptrole et produits connexes Dtermination des caractristiques dinflammabilit de fluides au contact de surf
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21、s f,dnuo plsaee ifnrom ttneC ehlar Secterirata ta teh serddaig sleb nevwo. ISO 3002 All irthgs erse.devr lnUeto sswrehise specified, on trap fo this lbupictaion maeb y cudorperro de tuilizi den yna form ro na ybm ynae,s lecetrinoc ro mceinahcla, incliduntohp gcoiypodna gn micrfoilm, wittuoh repmissi
22、i now nritign from ietI rehSa Ot tsserdda eh ebolw or ISOs memreb i ydobn the cnuotfo yr ttseuqer ehe.r ISO cirypothg fofice saCe tsopale 65 eneG 1121-HC 02 av leT. 4 + 10 947 22 1 11 xaF0 947 22 14 + 9 74 E-mial coirypthgis.o gro We bwww.is.o groii ISO 3002 Allr ihgtsser edevrENISO20823:2003IS:3280
23、2 O3002(E) I SO 3002 All irhgts seredevr iiiForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each membe
24、r body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Elec
25、trotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopt
26、ed by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of paten
27、t rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 20823 was prepared by Technical Committee ISO/TC 28, Petroleum products and lubricants. ENISO20823:2003blank ENISO20823:2003INTENRATIONAL TSANDADR IS:32802 O3002(E)I SO 3002 All irhgts seredevr 1Petroleum
28、and related products Determination of the flammability characteristics of fluids in contact with hot surfaces Manifold ignition test WARNING The use of this International Standard may involve hazardous materials, operations and equipment. This International Standard does not purport to address all o
29、f the safety problems associated with its use. It is the responsibility of the user of this International Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1 Scope This International Standard specifies a test method
30、to determine the relative flammability of fluids when contacted with a hot metal surface at a fixed temperature, but it is also possible to gauge fluid ignition temperatures by adjustment of the manifold temperature. It is primarily used to assess the resistance to ignition of fire-resistant hydraul
31、ic fluids which are, by definition, difficult to ignite. It may be used with other types of more flammable fluids at lower surface temperatures, but this could significantly increase the hazards of this procedure. NOTE The procedure given in this International Standard is specified in ISO 12922:1999
32、, Lubricants, industrial oils and related products (class L) Family H (Hydraulic systems) Specifications for categories HFAE, HFAS, HFB, HFC, HFDR and HFDU. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only th
33、e edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 3170: 1) , Petroleum liquids Manual sampling 3 Principle A 10 ml test portion of fluid is dropped from a predetermined height and at a specified rate, onto a tube he
34、ated to 700 C, or another temperature in a series. The resulting spray is examined for flash or burn, both on the tube and after dripping from the tube. 1)To be published. (Revision of ISO 3170:1988)ENISO20823:2003IS:32802 O3002(E) 2 I SO 3002 All irhgts seredevr4 Reagents and materials 4.1 Steel wo
35、ol 4.2 Absorbent cotton (cotton wool) 4.3 Cleaning solvent: any suitable light hydrocarbon solvent for wiping the tube. NOTE 2,2,4-trimethylpentane, heptane or petroleum spirit boiling between 60 C and 80 C are suitable. 5 Apparatus 5.1 Simulated manifold test rig 5.1.1 General The rig consists of a
36、 heated simulated manifold supported in a box frame, and is illustrated in Figure 1. It shall be located in a fire-resistant enclosure with adequate ventilation to remove toxic and/or noxious combustion or decomposition products. 5.1.2 Manifold support A sheet metal box of dimensions 300 mm 300 mm 4
37、50 mm, open at the top and front. Holes of 78 mm nominal diameter shall be cut in the sides in such a position that the manifold is positioned and supported so that its major axis is held at an angle of 7 to the horizontal, and the centre-point of the manifold is 270 mm 10 mm above the surface of th
38、e drip tray or bottom of the support. The bottom of the box shall either contain a separate drip tray, or be so shaped as to contain all drips of liquid falling from the manifold. The diameter of the holes in the box should be just sufficient to accommodate the simulated manifold (5.1.3) complete wi
39、th external rod. Dimensions in millimetres Key 1 sheet metal box 300 300 450 2 thermocouple 3 tube of corrosion-resistant steel: 75 outer diameter 1 wall thickness 500 4 rod of corrosion-resistant steel: diameter 3 250 Figure 1 Simulated manifold test rig ENISO20823:2003IS:32802 O3002(E) I SO 3002 A
40、ll irhgts seredevr 35.1.3 Simulated manifold The manifold, illustrated in Figure 2, is constructed from corrosion-resistant steel tubing of 75 mm nominal outside diameter and 1 mm wall thickness. It shall be 500 mm 50 mm in length. The exterior of the tube shall be sandblasted. A corrosion-resistant
41、 steel rod, 3 mm in diameter and 250 mm in length, is tack welded to the exterior surface of the tube such that the major axes are parallel, and the mid-point of the long axis of the rod corresponds to that of the tube. 5.1.4 Manifold heater A heating element shall be mounted centrally within the ma
42、nifold tube by means of suitable washers constructed from thermal insulation material. The element shall be capable of heating and maintaining a temperature of 700 C 5 C on the exterior surface of the manifold tube over the central portion of approximately 305 mm of the tube, whilst the enclosure ve
43、ntilation (5.1.1) is switched on. The terminals to the tube heater shall be enclosed. NOTE A rod pattern, silicon carbide type or equivalent, of 25 mm diameter and overall length 790 mm, and nominal electrical resistance 0,62 , has been found suitable. 5.1.5 Temperature sensors Temperature sensors s
44、hall be mounted in contact with the manifold tube surface in order to monitor the temperature close to the expected point of impact of the fluid. Each sensor shall be connected to a temperature indicator. Take care to minimize any additional radiating surfaces in the attachment of the sensor(s). NOT
45、E A mobile spring-loaded plate temperature sensor is preferred. If not available, three sensors located approximately 145 mm apart over the central portion of the manifold tube surface, placed to avoid fluid running off across the sensors, will be satisfactory. 5.2 Fluid dispenser A device, mounted
46、vertically above the centre-line of the manifold, that can measure 10 ml 0,5 ml of fluid, and dispense it at a controlled and constant rate over 50 s 10 s. The dispenser shall be mounted on a stand that allows measured movements horizontally along the axis of the tube and parallel to it. The height
47、of the dispenser outlet above the surface shall be measured and recorded. NOTE Manual use of a burette or similar device is not recommended in view of the safety hazard associated with the fluid igniting on the manifold. Dimensions in millimetres Key 1 packing to hold central element in tube 2 heating element 3 tube of corrosion-resistant steel: 75 outer diameter 1 wall thickness 500 4 rod of corrosion-resistant steel: diameter 3 250 Figure 2 Simulated manifold and heating element ENISO20823:2003IS:32802 O3002(E) 4 I SO 3002 All irhgts seredevr6 Samples and sampling 6.1 Unless othe
