1、 ENGINEERING MATERIAL SPECIFICATION Date Action Revisions Rev 03 2012 02 16 N Status No replacement named N. Benipal, NA 2005 08 09 Revised Inserted 3.0; deleted 3.1, 4 1974 04 15 Released AD1-819 Controlled document at www.MATS Copyright 2012, Ford Global Technologies, LLC Page 1 of 6 LAMINATE-VINY
2、L, PRESSURE SENSITIVE, DECORATIVE, ESB-M99J254-B REFLECTIVE & NON-REFLECTIVE, EXTERIOR NOT TO BE USED FOR NEW DESIGN 1. SCOPE The material defined by this specification is a back printed laminated vinyl non-reflective or reflective film, pressure sensitive adhesive backed, suitable for exterior or i
3、nterior usage. 2. APPLICATION This specification was released originally for material used for emblems, appliques exterior moldings, station wagon side panels and tailgates, or other decorative exterior or interior parts. Wood grain, solid colors or special patterns in smooth or embossed texture may
4、 be specified. The material is available in two types. Unless otherwise specified on engineering drawing, Type I is understood. Type I: Non-reflective Type II: Reflective 3. REQUIREMENTS 3.0 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Comp
5、anys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 MECHANICAL PROPERTIES Type I Type II 3.2.1 Tensile Strength, psi (MPa), min (ASTM D 882, Method “A“, 2,000 1,500 1 x 6 in (25 x 250 mm sample (13.8) (10.3) 2 in (50 mm) distance bench marks, jaw spaced at start 4 in (100 mm) p
6、ulling speed 2 in (50 mm)/min. Test both machine & cross-machine directions.) 3.2.1.1 Elongation, % min 120 120 3.2.2 Tear Strength, lb/in (N/mm) 30 (5.3) 30 (5.3) Thickness, min (ASTM D 1938) Test both machine and cross-machine directions. ENGINEERING MATERIAL SPECIFICATION ESB-M99J254-B Copyright
7、2012, Ford Global Technologies, LLC Page 2 of 6 3.2.3 Adhesion, oz/in (N/m) width, min (ASTM D 1000, except determine adhesion to anodized aluminum, stainless steel, chromium plating, and ESB-M50J100 quality enameled steel.) Type I Type II (180 Pull) (90 Pull) 3.2.3.1 As Received 50 (547) 30 (328) 3
8、.2.3.2 Aged 80 (876) 56 (613) 3.2.3.2.1 For 30 (328) 30 (328) Stainless Steel Type II, use fixture described in FLTM BU 012-01. Test Method: Expose duplicate samples to each of the following conditions: . 72 h at 70 +/- 1 C . 400 h weatherometer, per FLTM BO 101-01. . 168 h at 38 +/- 1 C and 95 - 10
9、0% relative humidity. . 240 h water immersion per FLTM BI 104-01. . 10 cycles consisting of 4 h at 70 +/- 1 C, 4 h at 38 +/- 1 C and 95 - 100% relative humidity, and 16 h at -29 C. Samples shall be conditioned for 48 h at 23 +/- 2 C prior to exposure. Tests shall be completed within 4 h (Type I) and
10、 48 h (Type II) after removal from the conditioning environment. 3.3 FILM PROPERTIES 3.3.1 Appearance Shall match the approved Ford Motor Company Styling master. 3.3.2 Thickness (ASTM D 1000) 3.3.2.1 Total Film-Adhesive Type I: 0.004-0.006 in Thickness: (0.10-0.15 mm) Type II: 0.006-0.008 in (0.15-0
11、.20 mm) ENGINEERING MATERIAL SPECIFICATION ESB-M99J254-B Copyright 2012, Ford Global Technologies, LLC Page 3 of 6 3.3.2.2 Film Thickness: Type I 0.003-0.005 in (0.08-0.13 mm) Type II: 0.005-0.007 in (0.13-0.18 mm) 3.4 RESISTANCE PROPERTIES 3.4.1 Sample Preparation Except where otherwise noted, test
12、s shall be conducted using appropriate sized steel panels (3 x 6 in (75 x 150 mm)/min) painted with ESB-M50J100 quality enamel. The film shall be applied using assembly plant techniques and shall fully cover the face of the panel allowing a 1/8 - 1/4 in (3.2 - 6.4 mm) border around the periphery of
13、the panel. Samples shall be conditioned for 48 h at 23 +/- 2 C prior to starting the tests. 3.4.2 Heat Resistance, max 1.0% shrinkage No evidence of cracking, checking or color change after exposure for 30 min at 121 +/- 3 C. The test shall be conducted 2 h after application of a 1 x 10 in (25 x 255
14、 mm) strip of the material to a 4 x 12 in (100 x 305 mm) ESB-M50J100 quality enameled steel panel. 3.4.3 Weathering Resistance Shall show a minimum degree of fading, chalking, dulling or color change, except where noted (24 months Florida). No increase in brittleness or loss of adhesion is permitted
15、 and the material shall be completely free from evidence of cracking, checking, blistering or peeling. 3.4.3.1 Florida Exposure (5 facing south, Miami area) 12 months - minimum fading, chalking, dulling or color change. 24 months - moderate fading, chalking, dulling or color change, not to exceed th
16、at shown on standard 24 month panel on file in BEPE Materials Engineering Department. 3.4.3.2 Accelerated Weathering 2,000 h (FLTM BO 101-01) 3.4.3.3 High Intensity Ultraviolet 5 cycles (FLTM BO 015-03) 3.4.4 Resistance to Water and Soap Spotting (FLTM BI 113-01, except the use of the colorimeter is
17、 omitted). No more dulling or color change than the approved master sample on file in the BEPE Materials Engineering Section. ENGINEERING MATERIAL SPECIFICATION ESB-M99J254-B Copyright 2012, Ford Global Technologies, LLC Page 4 of 6 3.4.5 Resistance to Acid Spotting (FLTM BI 113-02, except use of th
18、e colorimeter is omitted.) No more dulling or color change than the approved master sample on file in the BEPE Materials Engineering Section. 3.4.6 Water Resistance, min 240 h (FLTM BI 104-01) No film degradation, blistering or loss of adhesion. Evaluation shall be made upon removal from the water b
19、ath. No other visual defects, such as blushing, shall be evident after the sample is allowed to recover for 8 h at 23 +/- 2 C. 3.4.7 Salt Spray, Resistance, min 24 h (FLTM BI 103-01) No film degradation, blistering or loss of adhesion. Evaluation shall be made upon removal from the salt spray chambe
20、r. No other visual defects, such as blushing shall be evident after the sample is allowed to recover for 8 h at 23 +/- 2 C. 3.4.8 Gasoline Resistance The vinyl film shall show no dulling, color change or loss of adhesion, and only slight softening. Test Method: Immerse panel to which film has been a
21、pplied in 40% aromatic reference fuel (40% para-xylene, 60% iso-octane) for 15 min at 21 C at minimum. Wipe the film with a soft cloth and examine for film damage, dulling or color change. 3.4.9 Reflectance (Type II Only) The reflectance intensity values of the film shall not be less than the approv
22、ed styling master. (Test per Federal Specification L-S-300 (1-7-70), Section 3.5.5, Table II.) 3.5 FINISHED PARTS 3.5.1 Quality That obtainable with the best commercial practice. 3.5.1.1 Cleanliness All substrates to be covered by the film shall be clean in keeping with good commercial practice. Oil
23、, grease, dust and other foreign materials which would affect the adhesion of the film shall be removed prior to material application. ENGINEERING MATERIAL SPECIFICATION ESB-M99J254-B Copyright 2012, Ford Global Technologies, LLC Page 5 of 6 3.5.1.2 Appearance Shall match master samples approved by
24、Styling for: . Color match and uniformity. . Smoothness (absence of blisters). . Absence of scratches and tool marks. . Grain Pattern: Wood grain patterns must match adjacent assembled parts for grain characteristics and plank lines along a horizontal line, or as otherwise specified. 3.5.2 Adhesion,
25、 oz/in (N/m), min width Type I Type II (180 Pull) (90 Pull) 3.5.2.1 As Received 50 (547) 30 (328) 3.5.2.2 Aged 80 (876) 56 (613) Type II, use fixture described in FLTM BU 012-01. Test Method: Expose samples of the part to each of the following conditions: . 72 h at 70 +/- 1 C . 96 h at 38 +/- 1 C an
26、d 95 - 100% relative humidity. Samples shall be conditioned a minimum of 4 h at 23 +/- 2 C prior to starting the tests. Test shall be completed within 4 h (Type I) and 24 h (Type II) after removal from the conditioning environment in accordance with ASTM D 1000. Adhesion tests are not required if th
27、e size and/or shape of the part does not permit testing in accordance with the specified method. When this condition exists, the part shall be exposed to the specified test conditions and no blistering, lifting, peeling or loss of adhesion shall be permitted. 3.5.3 Heat Resistance Shall withstand a
28、simulated paint repair bake (30 min at 121 +/- 3 C) without evidence of blistering, checking, cracking or loss of adhesion. ENGINEERING MATERIAL SPECIFICATION ESB-M99J254-B Copyright 2012, Ford Global Technologies, LLC Page 6 of 6 5. GENERAL INFORMATION The information given below is provided for cl
29、arification and assistance in meeting the requirements of this specification. 5.1 MATERIAL REFERENCE FOR TEST PANELS 5.1.1 Anodized Aluminum: ESB-M2A34, anodized coating per ESB-M4P6-A. 5.1.2 Stainless Steel: ESB-M1A67. 5.1.3 Chromium Plating: SAE 903 or SAE 925 zinc die casting chromium plated per ESB-M1P23. 5.1.4 Enameled Steel: ESB-M50J100 quality, prepared per FLTM BI 103-02, Method “C“.
