1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions 2010 01 08 N-STATUS No replacement named J. Crist, NA 2005 10 19 Revised Inserted 3.0; Deleted 3.1, 3.2, 3.3, 3.8, 3.9 & 4 1991 04 18 Released DFI0EC0107002028 L. Rumao J. B. Huebner Printed copies are uncontrolled Copyright 2010, Ford Global
2、Technologies, LLC Page 1 of 4 THERMOPLASTIC POLYURETHANE + POLYCARBONATE WSF-M4D650-A2 (TPUR+PC) BLEND MOLDING COMPOUND NOT TO BE USED FOR NEW DESIGN 1. SCOPE The material defined by this specification is a blend molding compound based on thermoplastic polyurethane (TPUR) and polycarbonate (PC). 2.
3、APPLICATION This specification was released originally for material used for audio control bezels. 3. REQUIREMENTS Material specification requirements are to be used for initial qualification of materials. 3.0 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must
4、conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.4 MOLDING COMPOUND 3.4.1 Melt Flow Rate 4 - 13 g/ (ISO 1133/ASTM D 1238, 10 minutes 230 C, 2.16 kg) 3.5 MOLDED TEST SPECIMEN 3.5.1 Preparation of Test Specimens Unless otherwise specified all tests shall be ca
5、rried out on injection molded one-end gated test specimens. The following dimensions are required: A. 150 min x 10 x 4.0 +/- 0.2 mm (Tensile Bar, ISO 3167) B. 120 x 10 x 4.0 +/- 0.2 mm Specimens with shorter dimensions shall be cut from the center portion of the test specimen A and/or B. The specime
6、ns shall be prepared according to ISO 294. No annealing allowed. 3.5.2 Density 1.18 - 1.22 g/cm (ISO 1183, Method A/ASTM D 792, Method A1) ENGINEERING MATERIAL SPECIFICATIONWSF-M4D650-A2 Printed copies are uncontrolled Copyright 2010, Ford Global Technologies, LLC Page 2 of 4 3.5.3 Tensile Strength
7、at Max Load, min 34 MPa (ISO R 527/ASTM D 638M, 150 min x 10 x 4.0 +/- 0.2 mm specimen, 50 mm/min test speed) 3.5.3.1 Elongation at Max Load, min 97% (Test Method according to para 3.5.3) 3.5.4 Flexural Modulus, min 980 MPa (ISO 178/ASTM D 790M, Method I, Procedure A, 80 x 10 x 4.0 +/- 0.2 mm specim
8、en, 64 mm support span) 3.5.5 Shear Modulus at 23 C 330 - 550 MPa (ASTM D 4065, forced constant amplitude, fixed frequency of 1 Hz +/- 15%, strain level below 1%. Specimen approx. 60 x 10 x 4.0 +/- 0.2 mm cut from the center of specimen A. Specimen length between clamps 35-40 mm. Soak time at each t
9、emperature interval - 3 minutes minimum) Additionally, a Shear Modulus vs. Temperature curve shall be plotted for -50 to +160 C temperature range, at 5 C minimum intervals. The plotted curve must be within tolerance range shown on page 4. 3.5.6 Impact Strength, Izod, min (ISO 180, Method A/ASTM D 25
10、6, Method A, 80 x 10 x 4.0 +/-0.2 mm specimen, 10 specimens for each test) 3.5.6.1 At 23 +/- 2 C 65 kJ/m 3.5.6.2 At -23 +/- 2 C 4 kJ/m 3.5.6.3 At -40 +/- 2 kJ/m The test specimens must be conditioned for minimum of 6 h at the above specified temperature prior to impact test. Low temperature testing
11、shall be done within the cold box, if not possible, test can be conducted outside, but within 5 s. 3.5.7 Heat Deflection Temperature, min (ISO 75/ASTM D 648, 120 x 10 x 4.0 +/- 0.2 mm specimen) 3.5.7.1 At 1.82 MPa 69 C 3.5.7.2 At 0.45 MPa 107 C 3.5.8 Heat Aging Performance (ISO 188/ASTM D 573, 150 +
12、/- 50 air changes/h, 1000 h at 100 +/- 2 C. Unaged property values shall be determined at the time of the aged properties determination) ENGINEERING MATERIAL SPECIFICATIONWSF-M4D650-A2 Printed copies are uncontrolled Copyright 2010, Ford Global Technologies, LLC Page 3 of 4 3.5.8.1 Tensile Strength
13、at Max Load +/- 25% Change (Test Method per para 3.5.3) 3.5.8.2 Impact Strength, Izod Change +/- 25% (Test Method per para 3.5.6.1, specimens to be notched before heat aging) 3.6 FLAMMABILITY (ISO 3795) Burn Rate, max 100 mm/minute The specimen size required for material approval is 355 x 100 x 2.5
14、/- 0.1 mm with a smooth surface. 3.7 FOGGING (SAE J1756, 3 h at 100 C heating, 21 C cooling plate, post test conditioning 1 h and 16 h) Fog Number, min 60 Formation of clear film, droplets or crystals is cause for rejection. 5. GENERAL INFORMATION The information given below is provided for clarifi
15、cation and assistance in meeting the requirements of this specification. 5.1 COEFFICIENT OF LINEAR THERMAL EXPANSION 9.1-5/ C (ASTM D 696) 5.2 MOLD SHRINKAGE (ISO 2577, approx. 150 x 100 x 3.2 +/- 0.2 mm injection molded specimen) 5.2.1 Molding Shrinkage After 48 h at 23 +/- 2 C 0.5 - 0.7% 5.2.2 Pos
16、t Shrinkage (Separate specimens required for each test) After 48 h at 80 C 0.6 - 0.8% After 30 min at 120 C 0.6 - 0.8% 5.3 HARDNESS, DUROMETER D 65 - 75 (ISO 868/ASTM D 2240, 15 s dwell) ENGINEERING MATERIAL SPECIFICATIONWSF-M4D650-A2 Printed copies are uncontrolled Copyright 2010, Ford Global Technologies, LLC Page 4 of 4
