1、 ENGINEERING MATERIAL SPECIFICATION Date Action Revisions Rev. 03 2016 03 03 Revised Revised Flashpoint from 50 to 38 C C. Richardson - FNA 2011 08 02 Revised Revised 3.16; table editorial C. Richardson - FNA 2006 05 22 Activated C. Richardson Controlled document at www.MATS Copyright 2016, Ford Glo
2、bal Technologies, LLC Page 1 of 5 FUEL, DIESEL, INITIAL FILL, ULTRA LOW SULFUR (ULSD) WSS-M4C130-A 1. SCOPE The material defined by this specification is a well-refined middle distillate petroleum product containing normal commercial additives. 2. APPLICATION This specification was released original
3、ly for material used as initial fill fuel for diesel engines in passenger cars and trucks designed to operate on 15 ppm max sulfur fuel with cold flow properties controlled year round. 3. REQUIREMENTS Material specification requirements are to be used for initial qualification of materials. This mat
4、erial must meet the requirements of ASTM D975 Standard Specification for Diesel Fuel Oils plus the following: 3.1 APPROVED SOURCES This specification requires the use of approved sources. Only the sources identified on the Ford Approved Source List (ASL) can be used when this specification is listed
5、 on the drawing, CAD file, or other documents. The list of approved sources is located within Ford at or available externally through a Ford Materials Engineer. 3.2 CETANE RATING 3.2.1 Cetane Number 48.0 min (ASTM D613/ASTM D6890/ISO 5165) 3.2.2 Cetane Index 40.0 min (ASTM D976/D4737A/ASTM D4737B/I
6、SO 4264) 3.3 SULFUR 15 max (ASTM D5453/ISO 14596) 3.4 ASH 0.01% mass max (ASTM D482/ISO 6245) 3.5 COMPOSITION 3.5.1 Water 200 mg/kg max (ASTM D1744/ISO DIS 12937) 3.5.2 Total contamination 24 mg/kg max (EN 12662) ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyrig
7、ht 2016, Ford Global Technologies, LLC Page 2 of 5 3.5.3 Hydrocarbon types Report (ASTM D1319/ISO 12662) 3.5.4 Polycyclic Aromatic Hydrocarbons 11% mass (IP 391:1995) 3.5.5 Fame Content 0.1% volume max (EN 14078/ASTM D7371) 3.6 DISTILLATION (ASTM D86/ISO 3837) Temperature, C Initial boiling point Re
8、port 10% vol recovery Report 50% vol recovery Report 90% vol recovery Report Final boiling point Report 3.7 DENSITY Report (ASTM D1298/ISO 3675, 15 C) 3.8 KINEMATIC VISCOSITY 1.3 - 3.5 mm2/S (ASTM D445/ISO 3104, 40 C) 3.9 OXIDATION STABILITY, total insolubles 2.5 mg/100 mL max (ASTM D2274/ISO 12205)
9、 3.10 CALORIFIC VALUE, gross Report (ASTM D240) 3.11 CORROSION 3.11.1 Copper Tarnish 1 b max (ASTM D130/ISO 2160) 3.11.2 Rust Prevention Moderate rusting max (ASTM D665/ISO DP 7120, Procedure B, 30 minutes) 3.11.3 Silver Corrosion 1 max (ASTM D130 modified) 3.12 FLASHPOINT 38 C min (ASTM D93/ISO 271
10、9) 3.13 LUBRICITY at 60 C 400 micron wear (ASTM D6079/ISO DIS 12156-HFRR) scar diameter max 3.14 CARBON RESIDUE 0.20% max (ASTM D524/ISO 6615, 10% distillation residue) 3.15 WATER REACTION, fuel layer only 1, slight haze max (ASTM D1094/ISO 6250) ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Contr
11、olled document at www.MATS Copyright 2016, Ford Global Technologies, LLC Page 3 of 5 3.16 COLD FLOW PROPERTIES, TEMPERATURE 3.16.1 Cloud Point -30 C max (ASTM D2500/ISO 3015) 3.16.2 Cold Filter Plugging Point Report (ASTM D6371/EN 116/IP 309) 3.17 ODOR The material shall have the usual characteristi
12、c odor of diesel fuel. There shall be no obvious foreign odors. 3.18 ADDITIVES The material shall contain normal commercial additives. The use of cold flow improver additives may be used with approval of Fuels and Lubricants Engineering. 3.19 COLOR The material shall be dyed in accordance with Custo
13、ms and Excise requirements. 3.20 CONDUCTIVITY Report (ASTM D2624/ASTM D4308) 4. GENERAL INFORMATION The information given below is provided for clarification and assistance in meeting the requirements of this specification. Contact for questions concerning Engineering Material Specifications. 4.1 F
14、LAMMABILITY This material represents a potential fire hazard. The Manufacturing Engineering Department or other responsible activity shall notify both the Security and Safety Units of its presence to assure that proper fire precautions are provided. The location in which it is used or stored shall b
15、e included in the notifications. 4.2 SAMPLING AND SUBMISSION OF SAMPLES (ASTM D4057/D 4177) 4.3 Quality Control records must be made available to Fuels and Lubricants Engineering upon request. 4.1 APPROVAL OF MATERIALS Suppliers desiring approval of their materials shall first obtain an expression o
16、f interest from Purchasing, Design or Product Development, and Materials Engineering. The supplier shall submit a completed copy of their laboratory test reports, signed by a qualified and authorized representative of the test facility, demonstrating full compliance with all the requirements of the
17、Material Specification. Tested material samples must be available for review upon request and kept for a minimum of one year. Upon request, the supplier will review the associated quality control documents (Process Failure Mode and Effects Analysis, Control Plans, Certification testing) with Ford. 4
18、.2 SUPPLIERS ONGOING RESPONSIBILITY All materials must be equivalent in all characteristics to the material upon which approval was originally granted. ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyright 2016, Ford Global Technologies, LLC Page 4 of 5 Prior to m
19、aking any changes to the material originally approved, whether or not such changes affect the materials ability to meet the specification requirements, the supplier shall notify the affected Supplier Technical Assistance (STA), Purchasing, and Materials Engineering activities of the proposed changes
20、 (with reasons) by submission of a completed Suppliers Request for Engineering Approval, SREA. For parts and components using Ford Engineering Material Specifications, all samples tested to the specifications for Design Verification (DV), Production Verification (PV) and Production Part Approval Pro
21、cess (PPAP) sign off must be kept until Job 1. 4.3 RESTRICTED SUBSTANCE MANAGEMENT STANDARD Substance restrictions imposed by regulations or Company direction applies to the materials addressed by this document. The restrictions are identified in the Restricted Substance Management Standard WSS-M99P
22、9999-A1 which is updated yearly. It is the suppliers responsibility to comply with this standard on a continuing basis through IMDS and or GMAP reporting. 5. SUMMARY OF REVISIONS 2016 03 03 Revised Flashpoint from 50 to 38 C 2011 08 02 Revised 3.16; table editorial 2011 05 26 Revised: 2, 3.2.2,3.3,
23、3.4, 3.6, 3.8, 3.12, 3.14,3.16, 3.16.1, 3.16.2; 3.18; table, ASTM methods format; inserted 3.5.5, 3.11.3, 3.20 C. Richardson - FNA ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyright 2016, Ford Global Technologies, LLC Page 5 of 5 Manufacturing ISO/DIS ASTM Typi
24、cal Limits Cetane Number 5165 D613 _ _ Cetane Index 4264 D4737A _ _ 4264 D4737B _ _ Sulfur, % wt. 14596 D5453 _ _ Ash, % wt. 6245 D482 _ _ Water, mg/kg 12937 D1744 _ _ Total contamination, mg EN 12662 _ _ Aromatics, % vol 3837 D1319 _ _ Polycyclic Aromatic, % wt. IP 391:1995 _ _ Distillation 3405 D8
25、6 Initial boiling point _ _ 10% vol recovery _ _ 50% vol recovery _ _ 90% vol recovery _ _ Final boiling point _ _ Density15 C, kg/L 3675 D1298 _ _ Kinematic Viscosity, mm2/S 3104 D445 _ _ Oxidation Stability, mg/100 mL 12205 D2274 _ _ Copper Tarnish 2160 D130 _ _ Rust Prevention, Procedure B 7120 D665 _ _ Flashpoint, C 2719 D93 _ _ Lubricity at 60 C, microns 12156 D6079 _ _ Carbon residue, 10% 6615 D524 _ _ Water Reaction 6250 D1094 _ _ Cloud Point, C 3015 D2500 _ _ Cold Filter Plugging Point, C EN 116 D6371 _ _ Conductivity, pS/m D2624 _ _
