1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS B ISO 10426 1 1： KS B ISO 10426 1： 2007 (2012 ) 2007 11 30 http:/www.kats.go.krKS B ISO 10426 1： 2007 : ( ) ( ) ( ) : (http:/www.standard.go.kr) ： ：2007 11 30 ：2012 12 20 20120737 ： ： ( 02-509-7274) (http:/www.kats.go.kr). 10 5 , . KS B ISO 10426 1： 2007
2、 (2012 ) 1： Petroleum and natural gas industries Cements and materials for well cementing Part 1： Specification 2005 2 ISO 10426 1, Petroleum and natural gas industries Cements and materials for well cementing Part 1： Specification , . 1 8 , . , 6 (A, B, C, D, E, F) . . (set-modifying) D, E F . G H
3、 2 . . ( ) . KS L 5120, KS L ISO 679, ISO 3310 1： 1982, Test sieves Technical requirements and testing Part 1： Test sieves of metal wire cloth ISO 13500： 1998, Petroleum and natural gas industries Drilling fluid materials Specifications and tests ASTM C109/C 109M, Standard Test Method for Compressi
4、ve Strength of Hydraulic Cement Mortars (Using 2-in or 50 mm Cube Specimens) ASTM C114, Standard Test Methods for Chemical Analysis of Hydraulic Cement ASTM C115, Standard Test Methods for Fineness of Portland Cement by the Turbidimeter ASTM C183, Standard Practice for Sampling and the Amount of Tes
5、ting of Hydraulic Cement KS B ISO 10426 1： 2007 2 ASTM C204, Standard Test Method for Fineness of Hydraulic Cement by Air Permeability Apparatus ASTM C465, Standard Specification for Processing Additions for Use in the Manufacture of Hydraulic Cements ASTM E220, Standard Test Method for Calibration
6、of Thermocouples by Comparison Techniques ASTM E1404, Standard Specification for Laboratory Class Conical Flasks DIN 12385： 1988, Laboratory glassware, conical flasks, wide neck EN 196 2： 2005, Methods of testing cement Part 2： Chemical analysis of cement EN 196 6： 1989, Methods of testing cement Pa
7、rt 6： Determination of fineness EN 196 7： 1989, Methods of testing cement Part 7： Methods of taking and preparing samples of cement 3 . 3.1 , , . 3.2 (Bearden) (consistency) (Bc) (consistency) 3.3 (乾 ) 3.4 ( ) . 3.5 (class) ISO 3.6 (grade) ISO 3.7 (乾 ) (乾 ) 3.8 (爐 ) KS B ISO 10426 1： 2007 3 3.9 3.10
8、 (consistometer) 3.11 3.12 / 3.13 (純 ) 3.14 3.15 3.16 Bc . 4 4.1 , 4.1.1 (A, B, C, D, E, F, G H) (O, MSR HSR) . a) A . ASTM C 465 , , A . (ASTM C150, I ) . KS B ISO 10426 1： 2007 4 b) B . ASTM C 465 , , B . , (MSR) (HSR) (ASTM C 150, II ). c) C . ASTM C 465 , , C . , , MSR HSR (ASTM C 150, III ) . d
9、) D . ASTM C 465 , , D . / , (MSR) (HSR) . e) E . ASTM C 465 , , E , . / , (MSR) (HSR) . f) F . ASTM C 465 , , F . / , (MSR) (HSR) . g) G . G / . , 2003/53/EC 2009 12 31 . , (MSR) (HSR) . h) H . H / . , 2003/53/EC 2009 12 31 . , (MSR) (HSR) . . . 4.1.2 1 . ASTM C 114( EN196 2) . KS B ISO 10426 1： 20
10、07 5 4.1.3 2 6 10 . 1 A B C D, E, F G H (O) (MgO), , % 6.0 NA 6.0 NA NA NA (SO3), , % 3.5 NA 4.5 NA NA NA , , % 3.0 NA 3.0 NA NA NA , , % 0.75 NA 0.75 NA NA NA (C3A), , % NR NA 15 NA NA NA (MSR) (MgO), , % NA 6.0 6.0 6.0 6.0 6.0 (SO3), , % NA 3.0 3.5 3.5 3.0 3.0 , , % NA 3.0 3.0 3.0 3.0 3.0 , , % NA
11、 0.75 0.75 0.75 0.75 0.75 (C3S), , % , % NA NA NR NR NR NR NR NR 58b48b58b48b (C3A), , % NA 8 8 8 8 8 (Na2O) , , % NA NR NR NR 0.75c0.75c (HSR) (MgO), , % NA 6.0 6.0 6.0 6.0 6.0 (SO3), , % NA 3.0 3.5 3.0 3.0 3.0 , , % NA 3.0 3.0 3.0 3.0 3.0 , , % NA 0.75 0.75 0.75 0.75 0.75 (C3S), , % , % NA NA NR N
12、R NR NR NR NR 65b48b65b48b (C3A), , % NA 3b3b3b3b3b2 (C3A) (C4AF), , % NA 24b24b24b24b24b (Na2O) , , % NA NR NR NR 0.75c0.75cNR . NA . a (C3A) 8 % , (SO3) 3 % . b . Al2O3 Fe2O3 0.64 , C3A “0” . Al2O3 Fe2O3 0.64 , . C3A (2.65%Al2O3) (1.69%Fe2O3), C4AF 3.04%Fe2O3C3S (4.07%CaO) (7.60%SiO2) (6.72%Al2O3)
13、 (1.43%Fe2O3) (2.85%SO3)Al2O3 Fe2O3 0.64 , C3S . C3S (4.07%CaO) (7.60%SiO2) (4.48%Al2O3) (2.86%Fe2O3) (2.85%SO3) c (Na2O ) . Na2Oequivalent (0.658%K2O) (%Na2O) KS B ISO 10426 1： 2007 6 2 A B C D E F G H , ( 5) 46 46 56 38 38 38 44 38 ( )(6. ) ( , m2/kg) ( , m2/kg) 150280160280220400NRNRNR NR NR NR N
14、RNRNRNR , (8. ) NR NR NR NR NR NR 5.9 5.9 (8h ) (9. ) , 6 MPa MPa(psi) NA 38 atm. 1.7 1.4 2.1 NR NR NR 2.1 2.1NA 60 atm. NR NR NR NR NR NR 10.3 10.36S 110 20.7 NR NR NR 3.4 NR NR NR NR8S 143 20.7 NR NR NR NR 3.4 NR NR NR9S 160 20.7 NR NR NR NR NR 3.4 NR NR (24h ) (9. ) , 6 MPa(psi) MPa(psi) NA 38 at
15、m. 12.4 10.3 13.8 NR NR NR NR NR4S 77 20.7 NR NR NR 6.9 6.9 NR NR NR6S 110 20.7 NR NR NR 13.8 NR 6.9 NR NR8S 143 20.7 NR NR NR NR 13.8 NR NR NR9S 160 20.7 NR NR NR NR NR 6.9 NR NR , (10. ) 9 13 (15 30 ) Bca ( / ) 4 30 90 90 90 90 NR NR NR NR5 30 NR NR NR NR NR NR 90 905 30 NR NR NR NR NR NR 1201206
16、30 NR NR NR 100 100 100 NR NR8 30 NR NR NR NR 154 NR NR NR9 30 NR NR NR NR NR 190 NR NRa10. 10. (Bearden) (Bc) NR . 4.2 , 4.2.1 C,D,E,F,G H 24 ( 1 ) 1 000 ( 2 ). KS B ISO 10426 1： 2007 7 A B 14 ( 1 ) 25 000 ( 2 ). , 1 2 . 4.2.2 KS B ISO 10426 , 7 . 4.2.3 3 . 5, 6, 10 11 . 3 5. ASTM C 183( EN 196 7)
17、A, B, C 6. ASTM C 115 ASTM C 204( EN 196 6) 7. 7.1 G, H 8. 8.1 A, B, C, G, H 9. 9.1 ( , 9.1.3.2 ) D, E, F 9. 9.1 10. 10.1 4.2.4 . 5 ASTM C 183( EN 196 7) . 6 6.1 ASTM C 115 ASTM C 204( EN 196 6) . 6.2 2 (m2/kg) , D, E, F, G H . KS B ISO 10426 1： 2007 8 ( ) . 7 , 7.1 7.1.1 0.1 % , 1 . 7.1.2 4 . 7.1.1
18、 . 4 g g 1 000 0.50 500 0.35 300 0.30 200 0.20 100 0.15 50 0.10 7.1.3 ISO 3310 1 20 (850 m ) . 7.1.4 1 ( 1 ) . 1 . , 10 % . . 1 KS B ISO 10426 1： 2007 9 7.2 7.2.1 ASTM C 183 . 7.2.2 60 23 1 (73 F2 F) , 60 23 1 (73 F2 F) . 7.2.3 , . , (濕潤 ) . 7.2.4 5 . 5 2 . 5 A, B (g) C (g) D, E, F, H (g) G (g) 3550
19、5 3830.5 3270.5 3490.5 7720.5 6840.5 8600.5 7920.5 7.2.5 5 , 15 4 000 rpm200 rpm(66.7 r/s3.3 r/s) . 12 000 rpm500 rpm(200 r/s8.3 r/s) . 8 ( ) 8.1 8.1.1 10.1 ( ) . . 27 1.7 (80 F3 F) 150 rpm15 rpm(2.5 r/s0.25 r/s) . ( 2 5 ). ( 2, 3 ) . KS B ISO 10426 1： 2007 10 1 7 2 8 3 9 4 10 5 11 6 12 2 KS B ISO
20、10426 1： 2007 11 1 ( 2 ) 2 3 ( 4 ) 4 ( 5 ) 3 KS B ISO 10426 1： 2007 12 ： mm(in) 1 180 2 2 3 4 KS B ISO 10426 1： 2007 13 ： mm(in) 1 ： 302 1.0 mm7.9 mm(0.04 in0.313 in) 2 ： 416 6.4 mm211.1 mm(0.25 in8.313 in) 5 8.1.2 7.1.1 . KS B ISO 10426 1： 2007 14 8.1.3 ASTM E 1404, I, 2 DIN 12385 500 mL ( 6 ). ： mm 1 ASTM ( 1, 2), 500 mL a b ( ) 6 8.2 8.2.1 ( ) 1.7 (3 F) . ASTM E 220 “ ” J . , . 1.7 (3 F) ( A ). 8.2.2 150 rpm15 rpm(2.5 r/s0.25 r/s) , , . 8.2.3 30 . 6 , . 8.3 8.3.1 7. . KS B ISO 10426 1： 2007 15 8.3.2 . 8.3.3 , , . 1 . 8.3.4 20 30 . 27 1.7 (80 F3 F) . 8.3.5 790 g5 g
