KS M 1009-2008 Antimony standard solution《锑标准液》.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 1009 KS M 1009:2008 2008 12 19 http:/www.kats.go.krKS M 1009:2008 : ( ) ( ) ()MPT ( ) : (http:/www.standard.go.kr) : : 1988 11 30 : 2008 12 19 2008-0927 : : ( 025097301) (http:/www.kats.go.kr). 10 5 , . KS M 1009:2008 Antimony standard solution 1 . 2 .

2、 ( ) . KS M 0001, KS M 0011, pH KS M 0016, KS M 0076, KS M 0126, ( ) KS M 8356, KS M ISO 6353 2, 2: 1 KS M ISO 6353 3, 3: 2 3 KS M 0001 . 4 KS M 0126 . 4.1 4.2 . 4.3 1 99.9 % (III) KS M 1009:2008 2 . 4.4 2 99.9 % (III) 7. a) 1 . 5 1 . 1 ( ) mg Sb/L Sb 1 000 980 1 020 Sb 100 98 102 Sb 10 9.0 11.0 8.

3、 . 6 . a) (III) 99.9 % . b) KS M 8356 . c) KS M 0076 3.( ) A 2 . 217.6 nm . AB101 A : 15 mL 5 mL 2 (10 mg Sb/L) 40 L B : 15 mL 5 mL 7 . a) 6. a) (III) 2.5 3.0 mol/L . b) 8. 1 . 8 8.1 KS M 0001 2 KS M 1009:2008 3 . 8.2 (Sb 1 000) a) . 1) 6. c) . 2) (1: 2) KS M ISO 6353 2(R 3) 28.0 30.0 % 50 mL 100 mL

4、 . 3) ( ) ( ) 4 ( ) 20 g 100 mL . 4) KS M ISO 6353 2(R 29) 3 10 g 100 mL . 5) KS M ISO 6353 3(R 89) . 6) 1)KS M ISO 6353 2(R 25) 40 g 100 mL . 7) (1: 5) 6. b) 10 mL 50 mL . 8) 5 mmol/L KS M ISO 6353 3(R 68) 13 g 100 mL (1: 5) 1 mL 1 000 mL . 100 mL 1 000 mL . 9) 2 (1 000 mg Sb/L) b) . 1) 1 mV ( 1012

5、) . 2) 3) - 4) pH KS M 0011 II . c) . 1) (Sb 1 000) 10 mL 300 mL . 2) ( ) 20 mL . 3) 10 mL 50 mL . 4) (1: 2) pH 5.5 7 g . 5) 5 mmol/L . 6) 2 (1 000 mg Sb/L) 10 mL 300 mL . 7) 2) 5) . 8) . 9) 1) 8) 3 . 10) 3 2 (1 000 mg Sb/L) 5 mmol/L . 3 0.5 % . 0.5 % 6) 8) 3 . 11) d) 1) (Sb 1 000) . 12) (Sb 1 000)

6、3 0.5 . 0.5 % . 1) . KS M 1009:2008 4 d) . 1) (Sb 1 000) . 120ttcc = c : (Sb 1 000) (mg Sb/L) c0: 2 (1 000 mg Sb/L) (mg Sb/L) t1: 2 (1 000 mg Sb/L) 5 mmol/L (mL) t2: (Sb 1 000) 5 mmol/L (mL) 2) 1) 3 1 . 8.3 (Sb 100) a) . 1) 6. c) . 2) (1: 2) 8.2 a) 2) . 3) ( ) 8.2 a) 3) . 4) 8.2 a) 4) . 5) 8.2 a) 5)

7、 . 6) 1)8.2 a) 6) . 7) (1: 5) 8.2 a) 7) . 8) 1 mmol/L KS M ISO 6353 3(R 68) 2.6 g 100 mL (1: 5) 1 mL 1 000 mL . 100 mL 1 000 mL . 9) 2 (100 mg Sb/L) b) . 1) 8.2 b) 1) . 2) 8.2 b) 2) . 3) 8.2 b) 3) . 4) pH 8.2 b) 4) . c) . 1) (Sb 100) 15 mL 300 mL . 2) ( ) 20mL . 3) 10 mL 15 mL . 4) (1: 2) pH 5.5 7 g

8、 . 5) 1 mmol/L . 6) 2 (100 mg Sb/L) 15 mL 300 mL . 7) 2) 5) . 8) . 9) 1) 8) 3 . 10) 3 2 (100 mg Sb/L) 1 mmol/L . 3 0.5 % . KS M 1009:2008 5 0.5 % 6) 8) 3 . 11) d) 1) (Sb 100) . 12) (Sb 100) 3 0.5 % . 0.5 % . d) . 1) (Sb 100) . 120ttcc = c : (Sb 100) (mg Sb/L) c0: 2 (100 mg Sb/L) (mg Sb/L) t1: 2 (100

9、 mg Sb/L) 1 mmol/L (mL) t2: (Sb 100) 1 mmol/L (mL) 2) 1) 3 1 . 8.4 (Sb 10) a) . 1) 6. c) . 2) (2.8 mol/L) 6. b) 230 mL 1 000 mL . 3) 2 (11 mg Sb/L) 4) 2 (10 mg Sb/L) 5) 2 (9 mg Sb/L) b) . 1) (Sb 10) 5 1 % . c) . 1) KS M 0016 7.( ) 217.6 nm (2.8 mol/L) 2 (10 mg Sb/L) . 2) (2.8 mol/L) (Sb 10) . 3) (2.

10、8 mol/L) (Sb 10) 2 (11 mg Sb/L) (9 mg Sb/L) . 4) (2.8 mol/L) (Sb 10) 2 . 5) d) 1) (Sb 10) . 6) 1) 4) 3 (Sb 10) 3 1 % . 1 % . d) . 1) (Sb 10) . KS M 1009:2008 6 112112)()(cEEEEccc += c : (Sb 10) (mg Sb/L) c1: 2 (10 mg Sb/L) (mg Sb/L) c2: 2 (11 mg Sb/L) (9 mg Sb/L) (mg Sb/L) E : (Sb 10) E1: 2 (10 mg S

11、b/L) E2: 2 (11 mg Sb/L) (9 mg Sb/L) 2) 1) 3 1 . 9 . 10 2) . 11 . d), h) , i) . a) b) (20 ) c) (III) (0.75 mol/L) d) (mL) e) ( , ) f) g) h) i) 1) 25 . . 2) . 3) . 2) , . 135513 7017 (02)60094114 (02)600948878 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M 1009:2008KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Antimony standard solution ICS 71.040.30

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