KS M ISO 11401-2010 Plastics-Phenolic resins-Separation by liquid chromatography《塑料 酚醛树脂 用液相色谱法分离》.pdf

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1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 11401 KS M ISO 11401 :2010 2010 7 28 http:/www.kats.go.krKS M ISO 11401:2010 : ( ) ( ) ( )SK ( ) ( ) : (http:/www.standard.go.kr) : :2005 11 30 :2010 7 28 2010-0294 : : ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M ISO 11401:2010 PlasticsPhe

2、nolic resinsSeparation by liquid chromatography 1993 ISO 11401, PlasticsPhenolic resinsSeparation by liquid chromatography , . 1 1.1 . / . . A: B: C: A( ) . () () , . B C( ) . ( B), ( C). . B , C . 1.2 . 1.3 . 2 . . ( ) . KS M ISO 11401:2010 2 KS M ISO 472, KS M ISO 10082, 3 . 3.1 / KS M ISO 472 3.2

3、 (novolaks) , , , . . KS M ISO 10082. KS M ISO 472 . 3.3 (resol) . . . . , KS M ISO 10082. KS M ISO 472 . 4 4.1 A - , . , . 4.1.1 , . 4.1.2 4.1.2.1 4.1.3 KS M ISO 11401:2010 3 4.1.3.1 , . 4.1.3.2 UV 4.1.3.3 / 4.1.3.4 4.1.3.5 2100 , 600 mm 7.7 mm 21 000 , 600 mm 7.7 mm 4.1.3.6 ( ) 4.1.4 4.1.4.1 . 4.1

4、4.2 100 mg 10 mL (4.1.2.1) . 4.1.5 : : :1 mL/min : 20 L :254 nm 280 nm UV , 4.1.6 , . . , . , (, ) (4.3.8 ). 4.1.7 1 . KS M ISO 11401:2010 4 1 4.2 B 4.1 . 4.2.1 , . . . 4.2.2 4.2.2.1 4.2.2.2 4.2.3 4.2.3.1 KS M ISO 11401:2010 5 , . 4.2.3.2 UV 4.2.3.3 / 4.2.3.4 4.2.3.5 5 m 125 mm 4 mm . 4.2.3.6 ( ) 4

5、2.4 4.2.4.1 . 4.2.4.2 100 mg 10 mL (4.2.2.1) . 4.2.5 : : () THF(%) (%) 0 25 75 10 50 50 40 100 0 44 100 0 47 25 75 55 25 75 :0.5 mL/min :20 L :254 nm 280 nm UV 4.2.6 . , (, ) (4.3.8 ). 4.2.7 2 . KS M ISO 11401:2010 6 2 4.3 C ( ) 4.1 . 4.3.1 , . . 4.3.2 4.3.2.1 4.3.2.2 4.3.2.3 4.3.3 KS M ISO 11401:2

6、010 7 4.3.3.1 , . 4.3.3.2 UV 4.3.3.3 / 4.3.3.4 4.3.3.5 5 m RP 18 125 mm 4 mm . 4.3.3.6 ( ) 4.3.4 4.3.4.1 . 4.3.4.2 , . a) (phenate) . b) . 4.3.4.3 100 mg 10 mL (4.3.2.3) . 4.3.5 : : () (%) (%) 0 10 90 7 30 70 15 45 55 35 95 5 38 95 5 48 10 90 60 10 90 :0.5 mL/min :20 L :254 nm 280 nm UV 4.3.6 . , KS

7、 M ISO 11401:2010 8 . (4.3.8 ) . 4.3.7 3 3 4.3.8 . . , . f . C S C S A m m A f A C : A S : m C : m S : w C . 100 S S C C mA fm A w m : A C , A S , f, m S : . KS M ISO 11401:2010 9 , . 5 . a) b) c) ( A, B C) d) e) f) g) h) i) j) k) 153787 1 92 3(13) (02)26240114 (02)262401489 http:/ KS M ISO 11401 :2010 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Plastics Phenolic resins Separation by liquid chromatography ICS 83.080.10 Korean Agency for Technology and Standards http:/www.kats.go.kr

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