1、C 52 GBZ GBZ/T 160.53 2004 Methods for determination of phenyl ethers in the air of workplace 2004 5 21 2004 12 1 GBZ/T 160.53 2004 GBZ 1 GBZ 2 Anisidine Diphenyl- ether 2004121 GB/T 16055-1995 1995 GBZ/T 160.53 2004 1 2 GBZ 159 3 3.1 3.2 3.2.1 200mg/100mg 3.2.2 0500ml/min 03L/min 3.2.3 5ml 3.2.4 3.
2、2.5 10l 3.2.6 1 30m 0.53mm FFAP 2 2m 4mm OV-17 Shimalite W = 10 100 120 250 250 20ml/min 1 30ml/min 2 3.3 3.3.1 3.3.2 OV 17FFAP 3.3.3 Shimalite W 80100 3.3.4 10ml 40.0mg/ml 3.4 GBZ 159 3.4.1 500ml/min 15min 3.4.2 50ml/min 1 4h 3.4.3 50ml/min 1 4h 7d 3.5 3.5.1 3.5.2 0.50ml 30min 3.5.3 0.01.010.040.0m
3、g/ml 2.0l 3 (mg/ml) 3.5.4 (mg/ml) 3.6 3.6.1 1 293 P V o = V 1 273 + t 101.3 Vo L V L t P kPa 3.6.2 2 c 1 c 2 v C = 1000 2 V o D C mg/m 3 c 1 c 2 mg/ml v ml Vo L D % 3.6.3 GBZ 159 3.7 3.7.1 50g/ml 3.3 mg/m 3 7.5L 504000g/ml 5.07.7% 3.7.2 100mg 10.2mg87 3.7.3 - - 4 4.1 , 4.2 4.2.1 100mg/50mg 4.2.2 0 5
4、00ml/min 4.2.3 5ml 4.2.4 10l 4.2.5 2m 4mm FFAP:Chromosorb WAW = 10:100 210 270 270 45ml/min 4.3 4.3.1 4.3.2 FFAP 4.3.3 Chromosorb WAW 6080 4.3.4 10ml 0.50mg/ml 4.4 GBZ 159 4.4.1 200ml/min 15min 4.4.2 50ml/min 2 8h 4.4.3 50ml/min 2 8h 5d 4.5 4.5.1 4.5.2 1.0ml 30min 4.5.3 0.010.020.030.0 g/ml 1.0l 3 ( g/ml) 4.5.4 ( g/ml) 4.6 4.6.1 1 4.6.2 3 c vC = 3 Vo D C mg/ m 3 c g/ml v ml Vo L D % 4.6.3 GBZ-159 4.7 4.7.1 1.0 g/ml 0.33mg/ m 3 3L 1.030g/ml 3.56.3 4.7.2 100mg 12.6mg92.4 4.7.3 4.7.4