1、Designation: C910 16Standard Test Method forBond and Cohesion of One-Part Elastomeric SolventRelease-Type Sealants1This standard is issued under the fixed designation C910; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year o
2、f last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method determines the bond and cohesion ofone-part, elastomeric, solvent release-type sealants after high-
3、and low-temperature aging.1.2 The subcommittee with jurisdiction is not aware of anysimilar ISO standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and
4、 health practices and determine the applica-bility of regulatory limitations prior to use.NOTE 1Currently there is no ISO standard similar to this test method.2. Referenced Documents2.1 ASTM Standards:2C717 Terminology of Building Seals and SealantsD1191 Test Method for Concrete Joint Sealers (Withd
5、rawn1996)3E145 Specification for Gravity-Convection and Forced-Ventilation Ovens3. Terminology3.1 DefinitionsRefer to Terminology C717 for definitionsof the following terms used in this test method: elastomer,elastomeric, sealant, standard conditions, solvent-release seal-ant.4. Apparatus4.1 Extensi
6、on Machine, as shown in Fig. 1, so designed thatthe test specimen can be automatically extended at a constantrate of 3.18 mm (18 in.)/h from a joint width of 12.7 mm (12in.) to 14.29 mm (916 in.) at 23 6 3C (10 6 5F).4.2 Oven, forced-draft type, having temperature controlledat 70 6 2C (158 6 3.6F).
7、See Specification E145.4.3 Oven, convection type, having temperature controlled at50 6 1C (122 6 2F).4.4 Freezer Chest or Cold Box, having temperature con-trolled at 23 6 3C (10 6 5F).4.5 Mortar Blocks, six, prepared as described in Test Meth-ods D1191, except that the blocks shall be approximately
8、25.4mm (1 in.) wide by 76.2 mm (3 in.) long by 25.4 mm (1 in.)thick and surfaced by wet grinding on an iron lap with No. 60silicon carbide or aluminum oxide grain.4.6 Plates, six, of water-white polished float or plate glassapproximately 25.4 mm (1 in.) wide by 76.2 mm (3 in.) long by6.35 mm (14 in.
9、) thick.4.7 Aluminum Alloy Plates, six, 6063-T5 or 6061-T6 clearanodized a minimum of 20 min over a scale-free finish,approximately 25.4 mm (1 in.) wide by 76.2 mm (3 in.) long by6.35 mm (14 in.) thick.4.8 Polyethylene Spacer Bars, nine, approximately 12.7 mm(12 in.) by 12.7 mm (12 in.) by 50.8 mm (
10、2 in.), 18 bars 12.7mm (12 in.) by 12.7 mm (12 in.) by 25.4 mm (1 in.) and 18 bars14.29 mm (916 in.) by 6.35 mm (14 in.) by 25.4 mm (1 in.).5. Reagents5.1 Acetone or Methyl Ethyl Ketone Solvents.5.2 Detergent Solution.4,55.3 Distilled Water.6. Sampling6.1 Take all test specimens from a previously un
11、openedcontainer.1This test method is under the jurisdiction ofASTM Committee C24 on BuildingSeals and Sealants and is the direct responsibility of Subcommittee C24.30 onAdhesion.Current edition approved Jan. 15, 2016. Published March 2016. Originallyapproved in 1979. Last previous edition approved i
12、n 2011 as C91006(2011). DOI:10.1520/C0910-16.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3The last approv
13、ed version of this historical standard is referenced onwww.astm.org.4Neodol 25-35, a registered trademark of Shell Oil Co., One Shell Plaza,Houston, TX 77002, has been found suitable.5Dawn, a registered trademark of Proctor and Gamble Co., P.O. Box 579,Cincinnati, OH 54201, or Palmolive Green, a reg
14、istered trademark of ColgatePalmolive Co., 300 T. ParkAve., NewYork, NewYork, have been found suitable forthis purpose.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States17. Procedure7.1 Clean the glass and aluminum plate first with solve
15、nt,with detergent solution, followed by a final rinse with distilledwater. Allow plates to air dry. Prepare the six mortar blocks asdescribed in 4.5.7.2 Precondition the unopened containers of sealant atstandard conditions for a minimum of 24 h.7.3 Prepare three test specimens for each substrate to
16、betested, as follows: Using the polyethylene spacer bars tocontrol the joint dimensions, form a bead of sealant 12.7 mm(12 in.) wide by 12.7 mm (12 in.) thick by 50.8 mm (2 in.) longbetween the parallel 25.4 mm (1 in.) by 76.2 mm (3 in.) longfaces of two similar blocks or plates.7.4 Condition these
17、specimens by allowing them to set for24 h at standard conditions, then drying them in a convectionoven for 7 days at 50 6 1C (122 6 2F).7.5 Place the specimens in freezer for 24 h at 23 6 3C(10 6 5F). Dislodge spacer bars from sealant, but do notremove spacer bars from assembled specimens.7.6 Remove
18、 specimens from the freezer and condition themfor1hatstandard conditions.7.7 Place the specimens in a forced-draft oven for 7 days at70 6 2C (158 6 3.6F).7.8 Remove the specimens from the oven. Place them in afreezer for 24 h at 23 6 3C (10 6 5F).7.9 Place the specimens, while frozen, in the grips o
19、f theextension machine and extend the joint width from the original12.7 mm (12 in.) to 14.29 mm (916 in.) at 23 6 3C (10 65F) at the rate of 3.18 mm (18 in.)/h. After extension iscompleted, record any initial failure. Then apply appropriatespacers to maintain 14.29 mm (916 in.) thickness, removespec
20、imens with spacers in place from machine and allow towarm for3hat236 2C (73.4 6 3.6F).At this time examinespecimens for adhesive or cohesive failure.8. Report8.1 Measure and record the loss in adhesive or cohesivefailure, or both, in square centimetres (or square inches) foreach individual test spec
21、imen of mortar, glass, and aluminum.NOTE 1Three-dimensional view of compression-extension machine with automatic control units shows four specimens ready for compression-extension cycling.FIG. 1 Compression-Extension MachineC910 1629. Precision and Bias69.1 The precision and bias calculations for th
22、is test methodare based on the results of four laboratories testing threematerials using five specimens. The results are given in Table1.10. Keywords10.1 bend; cohesion; elastomeric; solvent-release sealantASTM International takes no position respecting the validity of any patent rights asserted in
23、connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the res
24、ponsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive caref
25、ul consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International
26、, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the AS
27、TM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ data have been filed at ASTM International Headquarters and maybe obtained by requesting Research Report RR
28、:C24-1023.TABLE 1 Precision and BiasC910 Bond Cohesion Adhesion LossAMaterial AverageEstimatedStandardDeviationWithinLaboratoryEstimatedStandardDeviationBetweenLaboratoriesRepeat-abilityInternalReproduci-bilityG1 0.056 0.114 0.120 0.32 0.34G2 0.001 0.000 0.000 0.00 0.00G3 0.065 0.144 0.158 0.41 0.45
29、C910 Bond Cohesion Cohesion LossBMaterial AverageEstimatedStandardDeviationWithinLaboratoryEstimatedStandardDeviationBetweenLaboratoriesRepeat-abilityInternalReproduci-bilityG1 0.001 0.000 0.000 0.000 0.000G2 0.001 0.000 0.000 0.000 0.020G3 0.015 0.035 0.036 0.099 0.102AAt 95 % confidence a variation of as much as 0.41 in.2can be expected withina laboratory and 0.45 in.2between laboratories.BAt 95 % confidence a variation of as much as 0.10 in.2can be expected withina laboratory and 0.10 in.2between laboratories.C910 163
