1、Designation: D 2917 07Standard Specification forMethyl Isoamyl Ketone1This standard is issued under the fixed designation D 2917; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses in
2、dicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope*1.1 This specification covers methyl isoamyl ketone (98 %grade) for use in paint
3、, varnish, lacquer, and related products.1.2 The following applies to all specified limits in thisstandard: for purposes of determining conformance with thisstandard, an observed value or a calculated value shall berounded off “to the nearest unit” in the last right-hand digitused in expressing the
4、specification limit, in accordance withthe rounding-off method of Practice E29.1.3 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.4 For specific hazard information and guidance, see thesuppliers Material Safety Data Sheet.2.
5、Referenced Documents2.1 ASTM Standards:2D 268 Guide for Sampling and Testing Volatile Solventsand Chemical Intermediates for Use in Paint and RelatedCoatings and MaterialD 1078 Test Method for Distillation Range of VolatileOrganic LiquidsD 1209 Test Method for Color of Clear Liquids (Platinum-Cobalt
6、 Scale)D 1364 Test Method for Water in Volatile Solvents (KarlFischer Reagent Titration Method)D 1476 Test Method for Heptane Miscibility of LacquerSolventsD 1613 Test Method for Acidity in Volatile Solvents andChemical Intermediates Used in Paint, Varnish, Lacquer,and Related ProductsD 3893 Test Me
7、thod for Purity of Methyl Amyl Ketone andMethyl Isoamyl Ketone by Gas ChromatographyD 4052 Test Method for Density and Relative Density ofLiquids by Digital Density MeterD 5386 Test Method for Color of Liquids Using TristimulusColorimetryE29 Practice for Using Significant Digits in Test Data toDeter
8、mine Conformance with SpecificationsE 300 Practice for Sampling Industrial Chemicals2.2 U.S. Federal Specification:PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packagingof33. Properties3.1 Methyl isoamyl ketone shall conform to the followingrequirements:Apparent specific gravity:20/20C 0.812 to 0.8
9、15or25/25C 0.809 to 0.812Color, Pt-Co scale, max (Note 1)15Distillation, CInitial boiling point, min 140Dry point, max 148Water, wt %, max 0.1Acidity as acetic acid, wt %, max 0.02Purity, wt %, min 98_NOTE 1Instrumental Pt-Co color determined by Test Method D 5386has been shown to have no statistica
10、lly significant difference from Pt-Cocolor determined by Test Method D 1209. However, it is not knownwhether methyl isoamyl ketone was part of the sample set included in theinterlaboratory study.4. Sampling4.1 The material shall be sampled in accordance withPractice E 300.1This specification is unde
11、r the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.Current edition approved June 1, 2007. Published July 2007. Originally approvedin 1970. Last
12、 previous edition approved in 2002 as D 2917 02.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Available fr
13、om Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/www.dodssp.daps.mil.1*A Summary of Changes section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 1942
14、8-2959, United States.5. Test Methods5.1 The properties enumerated in this specification shall bedetermined in accordance with the following ASTM testmethods:5.1.1 Apparent Specific GravityDetermine the apparentspecific gravity by any convenient method that is accurate tothe third decimal place, the
15、 temperature of both specimen andwater being 20C or 25C. See Guide D 268 or Test MethodD 4052.5.1.2 ColorTest Method D 1209 (see Note 1).5.1.3 Distillation RangeTest Method D 1078, using atemperature measuring device having a range of 98 to 152Cand a resolution of 0.1C.5.1.4 WaterTest Method D 1364.
16、45.1.5 AcidityTest Method D 1613.5.1.6 PurityTest Method D 3893.6. Packaging and Package Marking6.1 Package size shall be agreed upon by the purchaser andthe supplier.6.2 Packaging shall conform to applicable carrier rules andregulations or when specified shall conform to Fed. Spec.PPP-C-2020.7. Key
17、words7.1 ketone; methyl isoamyl ketone; MIAK; solventsSUMMARY OF CHANGESCommittee D01.35 has identified the location of selected changes to this standard since the last issue(D 2917 - 02) that may impact the use of this standard. (Approved June 1, 2007.)(1) Changed specs limits for apparent specific
18、 gravity in 3.1.(2) Added new Note 1 to 3.1.(3) Added Test Method D 5386 to list of Referenced Docu-ments.(4) Referenced new Note 1 in 5.1.2.(5) Revised 5.1.3.(6) Deleted Practice E 1 from 2.1.ASTM International takes no position respecting the validity of any patent rights asserted in connection wi
19、th any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible tech
20、nical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful considerat
21、ion at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Ha
22、rbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).4In some cases Test Method D 1476 may serve as a useful alternative method todetermine the presence of water. Because it is a qualitative test, its use would requireagreement between buyer and seller.D2917072
