1、Designation: D3144 00 (Reapproved 2013)1An American National StandardStandard Specification forCrosslinked Poly(Vinylidene Fluoride) Heat-ShrinkableTubing for Electrical Insulation1This standard is issued under the fixed designation D3144; the number immediately following the designation indicates t
2、he year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers semirigid, flame-retard
3、ant,crosslinked poly(vinylidene fluoride) heat-shrinkable tubingfor electrical insulation purposes. It is supplied in an expandedform and will shrink to its extruded diameter when heated.NOTE 1This standard is similar but not identical to IEC 606843228.1.2 The values stated in inch-pound units are t
4、o be regardedas the standard, except temperature which shall be stated indegrees Celsius.Values in parentheses are for information only.2. Referenced Documents2.1 ASTM Standards:2D910 Specification for Aviation GasolinesD1711 Terminology Relating to Electrical InsulationD2671 Test Methods for Heat-S
5、hrinkable Tubing for Elec-trical UseD3636 Practice for Sampling and Judging Quality of SolidElectrical Insulating MaterialsE176 Terminology of Fire Standards2.2 Military Standards:3MIL-H-5606 Hydraulic Fluid, Petroleum Base, Aircraft,Missile and OrdinanceMIL-T-5624 Turbine Fuel, Aviation, Grades JP-
6、4 and JP-5MIL-L-7808 Lubrication Oil,Aircraft, Turbine Engine, Syn-thetic BaseMIL-L-23699 Lubrication Oil, Aircraft, Turbine Engines,Synthetic BaseMIL-A-8243 Anti-Icing and DeicingDefrosting Fluid2.3 Federal Standards:SS-S-550 Sodium Chloride, Technical, for Water-SofteningUnits42.4 IEC Standards:60
7、6843228 Flexible insulating sleeving, Part 3, Sheet 228:Heat-shrinkable, semi-rigid, polyvinylidene fluoridesleeving, flame retarded, fluid resistant, shrink ratio 2:153. Terminology3.1 Definitions:3.1.1 For definitions pertaining to electrical insulation, referto Terminology D1711.3.1.2 For definit
8、ions pertaining to fire standards, refer toTerminology E176.4. Ordering Information4.1 When tubings are ordered to this specification, it is up tothe purchaser to define the size and color of the requiredtubing.5. Materials and Manufacture5.1 The compound used in the manufacture of heat-shrinkable t
9、ubing shall be modified poly(vinylidene fluoride),and the finished compound shall be free of all foreign matterother than intended formulation additives as appropriate.5.2 The tubing shall be extruded, crosslinked, and thenexpanded to the required dimensions.6. Chemical Property Requirements6.1 The
10、material shall conform to the chemical propertyrequirements specified in Table 1.6.2 Every lot of material manufactured shall be tested forflammability (when applicable). Other chemical requirementsshall be permitted to be tested less frequently or at a frequencyagreed upon between the purchaser and
11、 the seller.1This specification is under the jurisdiction of ASTM Committee D09 onElectrical and Electronic Insulating Materials and is the direct responsibility ofSubcommittee D09.07 on Flexible and Rigid Insulating Materials.Current edition approved Jan. 15, 2013. Published February 2013. Original
12、lyapproved in 1973. Last previous edition approved in 2006 as D3144 06. DOI:10.1520/D3144-00R12E01.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Doc
13、ument Summary page onthe ASTM website.3Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS.4Available from Superintendent of Documents, U.S. Government PrintingOffice, Washington, DC 20402.5Available from American National
14、 Standards Institute (ANSI), 25 W. 43rd St.,4th Floor, New York, NY 10036.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States17. Physical Property Requirements7.1 The material shall conform to the mechanical, thermal,and electrical requir
15、ements of Table 2.7.2 Every lot of material manufactured shall be tested forrestricted shrinkage, heat shock, tensile strength, and elonga-tion. Other physical requirements shall be permitted to betested less frequently or at a frequency agreed upon betweenthe purchaser and seller.8. Dimensional Req
16、uirements8.1 The material shall conform to the dimensional require-ments of Table 3.8.2 Tubing with non-standard dimensions shall be permittedto be supplied when agreed upon between purchaser and seller.Tubing with non-standard dimensions shall be considered tocomply with this specification if the r
17、equirements of Table 1and Table 2 are satisfied and the minimum recovered wallthickness equals or exceeds that of the identical or next largestnominal size. The wall for sizes greater than 1 in. shall be atleast as thick as that of the 1 in. size.9. Workmanship9.1 The tubing shall be homogeneous and
18、 essentially free offlaws, defects, pinholes, bubbles, seams, cracks, or inclusions.9.2 Clear tubing shall be transparent to translucent light tanor in a color as agreed between purchaser and seller.10. Sampling10.1 A lot shall consist of all material which is processed atthe same time and under the
19、 same conditions and submitted forinspection at one time.10.2 Properties shall be permitted to be tested at any stage inprocessing when they are unaffected by subsequent processing.10.3 Select a quantity of the product at random from eachlot in accordance with Practice D3636 and Table 5.10.4 Statist
20、ical process control measurements shall be per-mitted to be used to demonstrate conformance in lieu of thesampling plan noted herein when the demonstrated processcapability is greater than the specified AQL.11. Number of Tests and Retests11.1 The methods of test define the number of specimensand len
21、gth required for each test.11.2 If the results of any test, except for attributes listed inTable 3, do not conform to the requirements prescribed in thisspecification, perform two additional tests on different speci-mens from the same lot. Nonconformance to Table 3 require-ments on first inspection
22、shall be cause for rejection.11.3 If either of the two additional tests result innonconformance, the purchaser has the option of rejecting thelot of material. Notice of nonconformances observed by thepurchaser based on tests made according to this specificationshall be reported to the manufacturer w
23、ithin 60 days fromreceipt of the material.11.4 Tubing that has been rejected shall be permitted to bereplaced or reworked to correct the nonconformances andresubmitted for inspection. Before resubmitting, full particularsconcerning previous rejection and action taken to correct thenonconformances sh
24、all be furnished to the inspector.12. Test Methods12.1 Use the test methods described in Test Methods D2671unless stated otherwise in Table 1 or Table 2.12.2 Use a time of 3 min and a temperature of 200 6 2C392 6 4 F to recover (shrink) tubings in this specification.13. Inspection13.1 The manufactur
25、er or purchaser or both shall haveavailable all the facilities to enable the complete testing to thisspecification.TABLE 1 Chemical Property RequirementsProperty RequirementFluid resistance, 24 h at 233C736FJP-4 fuel, MIL-T-5624Lubricating oil, MIL-L-7808Lubricating oil, MIL-L-23699Hydraulic fluid,
26、MIL-H-56065% NaCl, SS-S-550Aviation gasoline, Grade 100, min octane 130,Specification D910Deicing fluid, MIL-A-8243Followed by tests for:Dielectric strength, min, V/mil kV/mm 500 19.7Tensile strength, min, psi MPa at2 in. 50 mm/min5000 34.5Flammability, Procedure A, max, s 15Water absorption, 24 h a
27、t 233C736F,max% 0.5TABLE 2 Physical Property RequirementsProperty RequirementRestricted shrinkage, Procedure A,175 3 C347 6 F 2000 Vno cracking, no dielectricbreakdownDielectric strength, min, V/mil kV/mm 600 23.6Heat shock, 3004C572 7 F no cracking, flowing, ordrippingLow-temperature flexibility, 5
28、5 2 C67 4 F (see Table 4 formandrels)no crackingUse Procedure A of Methods D2671for sizes364through12Use Procedure C of Methods D2671for sizes34through 1Tensile strength, min, psi MPa, using1-in. 25-mmbench marks and 1-in. 25-mm jawseparation at 2in. 50 mm/min5000 34.5Elongation, min %, using 1-in.
29、25-mmbench marksand 1-in. 25-mm jaw separation at 2in.50mm/min150Heat resistance, 168 h at 2503C482 6 FElongation, min, %50Volume resistivity, min, -cm 1013Secant modulus, min, psi MPa 105690Specific gravity, max 1.8D3144 00 (2013)1214. Certification14.1 When specified in the purchase order or contr
30、act, themanufacturers or suppliers certification shall be furnished tothe purchaser stating that samples representing each lot havebeen manufactured, tested, and inspected in accordance withthis specification and the requirements have been met. Whenspecified in the purchase order or contract, a repo
31、rt of the testresults shall be furnished.15. Packaging, Marking, and Shipping15.1 The tubing shall be supplied in lengths of 48 + 1, 0 in.1219 + 25, 0 mm unless otherwise specified.15.2 The tubing shall be packaged in conformance withstandard commercial practice unless otherwise specified. Indi-vidu
32、al sizes shall be neatly bundled or boxed. The exteriorshipping container shall be acceptable by parcel post orcommon carrier.15.3 Each bundle or container of tubing shall be distinctlyidentified by a tag or label. The name of the manufacturer,the expanded and recovered dimension of the tubing, thel
33、ength, quantity, and other appropriate information shall beshown thereon.16. Keywords16.1 crosslinked poly(vinylidene fluoride) heat-shrinkabletubing; electrical insulation; heat-shrinkable tubing; poly(vi-nylidene fluoride)ASTM International takes no position respecting the validity of any patent r
34、ights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at a
35、ny time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments
36、will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by
37、ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail);
38、 or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).TABLE 3 Dimensional RequirementsAs Supplied After Heat ShrinkingLongitudinalChange, %Nominal Size, in.Inside Diameter,min. in. mmEccentricity,ma
39、x, %Inside Diameter,max, in. mmWall Thickness, in. mm364 0.046 1.16 40 0.023 0.59 0.010 0.002 0.25 0.05 10116 0.063 1.60 40 0.031 0.76 0.010 0.002 0.25 0.05 10332 0.093 2.34 40 0.046 1.16 0.010 0.002 0.25 0.05 1018 0.125 3.18 40 0.062 1.60 0.010 0.002 0.25 0.05 10316 0.187 4.75 40 0.093 2.34 0.010 0
40、.002 0.25 0.05 1014 0.250 6.35 40 0.125 3.18 0.012 0.003 0.31 0.08 1038 0.375 9.50 40 0.187 4.75 0.012 0.003 0.31 0.08 1012 0.500 12.7 40 0.250 6.35 0.012 0.003 0.31 0.08 1034 0.750 19.1 40 0.375 9.50 0.017 0.003 0.43 0.08 101 1.000 25.4 40 0.500 12.7 0.019 0.003 0.48 0.09 10TABLE 4 Mandrel SizesHea
41、t-Shrinkable Tubing InsideDiameter As Supplied, in.Mandrel Diameter, in. mm364 to14 0.312 7.9438 to12 0.375 9.5334 to 1 0.438 11.1TABLE 5 Sampling Table for Lot Acceptance TestsPropertyRequire-mentInspec-tionLevelAQLSampling Unit,ft mInside diameter assuppliedTable 3 S-3 1.0 4 1.2Inside diameter after unre- Table 3 S-3 1.0 4 1.2stricted shrinkageWall thickness aftershrinkageTable 3 S-3 1.0 4 1.2Longitudinal change Table 3 S-2 1.0 4 1.2Straight length size, min 15.1hereinS-3 1.0 single straightlengthWorkmanship 9.1hereinI 2.5 4 1.2D3144 00 (2013)13
