1、Designation: D3896 07 (Reapproved 2016)Standard Practice forRubber From Synthetic SourcesSampling1This standard is issued under the fixed designation D3896; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision.
2、 A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice, intended for referee purposes, covers auniform procedure for sampling lots of solid synthetic rubbers.Raw synthetic r
3、ubber generally is marketed in bales or pack-ages of various sizes.1.2 A procedure for determining the acceptability of lots ofsynthetic rubber is given. This procedure is based on avariables sampling plan.1.3 The sample size is based on the assumption of a visuallyhomogeneous material. If obvious h
4、eterogeneity exists, thenumber of samples shall be increased.1.4 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.5 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is the
5、responsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ANSI Standard:Z1.9 Sampling Procedures and Tables for Inspection byVariables for Percent Defective23. S
6、ignificance and Use3.1 The sampling plan is intended for referee purposes onlyin establishing the properties or quality of a lot or shipment ofsynthetic rubber.4. Sampling4.1 Number of SamplesThe number of samples to beselected to represent the lot shall be determined by the size ofthe lot as indica
7、ted in Table 1. A sample bale or package isselected randomly from the lot for each sample required.NOTE 1The sampling plan is more efficient for large lots. The risk forthe producer and consumer decreases as the sample size increases.4.2 Removal of Test Portions:4.2.1 BalesFrom each sample bale sele
8、cted, cut one 600to 1500-g test portion of rubber, depending on the tests to bemade. Each test portion is tested separately. Cut the test portionthrough the entire bale, normal to the bale surfaces of thelargest area without the use of lubricant. Remove polyethylenefilm, paper, talc, or other extran
9、eous surface material prior totesting. Unless the test portion is to be tested immediately,place it in an airtight container of not more than twice thevolume of the test portion, or wrap it tightly in two layers ofaluminum foil until tested.4.2.2 PackagesFrom each sample package selected, re-move be
10、tween 600 and 1500 g of rubber depending on the teststo be made. The rubber should be selected randomly from thepackage and should be as free of surface material as practical.Unless the sample is to be tested immediately, place it in anairtight container.5. Lot Acceptability5.1 Each property of the
11、lot is evaluated separately. Therequirements of these tests are of two types: (1) those having asingle limit such as a minimum or maximum and (2) thosehaving double limits, that is, a minimum and a maximum. Aquality index is calculated for each property tested, and fromthis index, an estimate is mad
12、e of the percent of the lot that isdefective. If this percentage does not exceed the allowablevalues shown in Table 1, the lot is considered acceptable.5.2 Quality Index Calculations:5.2.1 For a requirement having a maximum limit, calculatethe quality index as follows:Q 5 U 2 X!/S (1)where:Q = quali
13、ty index,U = maximum value permitted by the specification,X= mean of values obtained for the test portion, andS = standard deviation of the samples.5.2.2 For a requirement having a minimum limit, calculatethe quality index as follows:Q 5 X2 L!/S (2)1This practice is under the jurisdiction of ASTM Co
14、mmittee D11 on Rubber andis the direct responsibility of Subcommittee D11.23 on Synthetic Rubbers.Current edition approved June 1, 2016. Published July 2016. Originally approvedin 1980. Last previous edition approved in 2011 as D3896 07 (2011). DOI:10.1520/D3896-07R16.2Available from the American Na
15、tional Standards Institute, 25 W. 43rd St., 4thFloor, New York, NY 10036.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1where:Q, X, and S = same as those for maximum value, andL = minimum value permitted by thespecification.5.3 Accep
16、tability:5.3.1 For a quality characteristic having a single specifica-tion limit, a lot is acceptable if the quality index equals orexceeds the minimum quality index shown in Table 1 for theapplicable lot and sample size.5.3.2 For a quality characteristic having both an upper andlower specification
17、limit, estimate the percentages of the lotabove the upper limit and below the lower limit from Table 2using the appropriate sample size and quality index valuescalculated in 5.2. A lot is acceptable if the sum of the twopercentages does not exceed the maximum allowable percentdefective shown in Tabl
18、e 1 for the lot size being evaluated.6. Precision and Bias6.1 Precision and bias statements are not directly applicableto this sampling practice, but they are pertinent to individualtest methods that will use this sampling practice.7. Keywords7.1 sampling; synthetic rubberASTM International takes no
19、 position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own respons
20、ibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed t
21、o ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the add
22、ress shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone),
23、 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Sampling PlanNOTE 1The sampling plan i
24、s based on Inspection Level III, ANSIZ1.9, and an Acceptable Quality Level of 2.5 %.Lot Size, kg (lb)Number ofSamplesQ Value,minAAllowablePercentDefective,maxB300 to 4000 (660 to 8800) 3 1.12 7.64001 to 6500 (8801 to 14 300) 4 1.17 10.96501 to 10 100 (14 301 to 24 200) 5 1.24 9.810 001 to 18 000 (24
25、 201 to 39 700) 7 1.33 8.418 001 to 30 000 (39 701 to 66 100) 10 1.41 7.330 001 to 50 000 (66 101 to 110 200) 15 1.47 6.650 001 to 80 000 (110 201 to 176 400) 20 1.51 6.2AMinimum value of Q for quality characteristics having single specification limit.BMaximum allowable percent defective for quality
26、 characteristics having bothupper and lower specification limit.TABLE 2 Estimate of Lot Percent DefectiveNumberofSamples:3 4 5 7 101520Q Value Estimated Percent of Lot Above or Below Limit0.95 19.3 18.3 17.9 17.5 17.3 17.2 17.21.00 16.7 16.7 16.4 16.1 16.0 15.9 15.91.05 13.7 15.0 14.9 14.8 14.7 14.7
27、 14.71.10 9.8 13.3 13.5 13.5 13.5 13.5 13.51.15 0.3 11.7 12.1 12.3 12.3 12.4 12.41.20 . 10.0 10.8 11.1 11.2 11.3 11.41.25 . 8.7 9.7 10.2 10.4 10.5 10.61.30 . 6.7 8.2 8.9 9.2 9.4 9.51.35 . 5.0 7.0 7.9 8.3 8.5 8.61.40 . 3.3 5.9 7.0 7.4 7.7 7.81.45 . 1.7 4.8 6.1 6.6 6.9 7.01.50 . . 3.8 5.3 5.9 6.2 6.31
28、.55 . . 2.9 4.5 5.2 5.5 5.71.60 . . 2.0 3.8 4.5 4.9 5.11.65 . . 1.3 3.2 4.0 4.4 4.51.70 . . 0.7 2.6 3.4 3.8 4.01.75 . . 0.2 2.1 2.9 3.4 3.61.80 . . . 1.7 2.5 2.9 3.11.85 . . . 1.3 2.1 2.6 2.81.90 . . . 0.9 1.8 2.2 2.41.95 . . . 0.6 1.4 1.9 2.12.00 . . . 0.4 1.2 1.6 1.82.10 . . . 0.1 0.7 1.2 1.32.20 . . . . 0.4 0.8 1.02.30 . . . . 0.2 0.5 0.72.40 . . . . 0.1 0.3 0.52.50 . . . . . 0.2 0.32.60 . . . . . 0.1 0.22.70 . . . . . 0.1 0.12.80 . . . . . . 0.12.90 . . . . . . .D3896 07 (2016)2
