1、Designation: D5100/D5100M 95a (Reapproved 2018)Standard Test Method forAdhesion of Mineral Aggregate to Hot Bitumen1This standard is issued under the fixed designation D5100/D5100M; the number immediately following the designation indicates theyear of original adoption or, in the case of revision, t
2、he year of last revision. A number in parentheses indicates the year of lastreapproval. A superscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method determines the adhesion of mineralaggregate when applied over a pour coat of hot bitumen o
3、n aroof membrane.1.2 The values stated in either SI units or inch-pound unitsare to be regarded separately as standard. The values stated ineach system may not be exact equivalents; therefore, eachsystem shall be used independently of the other. Combiningvalues from the two systems may result in non
4、-conformancewith the standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety, health, and environmental practices and deter-mine the applicability of regul
5、atory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Or
6、ganization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2D226/D226M Specification for Asphalt-Saturated OrganicFelt Used in Roofing and WaterproofingD312/D312M Specification for Asphalt Used in RoofingD450/D450M Specification for Coal-Tar Pitch Used inRoofing,
7、 Dampproofing, and WaterproofingD1079 Terminology Relating to Roofing and Waterproofing3. Terminology3.1 DefinitionsFor definitions of terms used in this testmethod, see Terminology D1079.4. Summary of Test Method4.1 Asmall section of roof surface is fabricated with roofingfelt or membrane using mea
8、sured amounts of a bituminouspour coat and mineral aggregate surfacing. The assembly isallowed to cool, the loose aggregate is removed and weighed,and the mass of adhered aggregate is calculated and reported.5. Significance and Use5.1 The quantities of mineral aggregate adhered to thesurface of a ro
9、of vary with the characteristics and total amountof the aggregate. Mineral aggregate shields bituminous mem-branes from solar radiation. Unadhered mineral aggregate canbe displaced by wind, water, and traffic, exposing the bitumen.5.2 This test method provides a laboratory means of deter-mining and
10、recording the mass of aggregate that adheres to abituminous pour coat.6. Apparatus6.1 Steel Tray, measuring 143 mm 558 in. 6 1 % square by13 mm 0.5 in. 6 10 % in height.6.2 Scales, for weighing bitumen and mineral aggregate,balance 1.00-kg 2.2-lb capacity, sensitive to 0.01 % of thecapacity.6.3 Cont
11、ainers, for hot bitumen and mineral aggregate (1-L1-qt capacity).7. Procedure7.1 Cut a piece of saturated felt to just cover the bottom ofthe steel tray; the saturated felt shall be Type 1 complying withSpecification D226/D226M.7.2 Attach the saturated felt to the inside of the tray with athin film
12、of a release agent such as silicone stopcock grease orpetroleum jelly. Lightly grease the insides of the sides of thetray with the same material.7.3 Weigh out 400 g 0.88 lb of gravel, chert, or trap rock,or 300 g 0.66 lb of slag mineral aggregate surfacing 61%.Record this mass as A. This is equivale
13、nt to 19.5 kg/m2400lb/100 ft2 and 14.6 kg/m2300 lb/100 ft2, respectively.7.4 Apply top pour coat of bitumen uniformly according toquantities and temperatures listed in Table 1.1This test method is under the jurisdiction ofASTM Committee D08 on Roofingand Waterproofing and is the direct responsibilit
14、y of Subcommittee D08.03 onSurfacing and Bituminous Materials for Membrane Waterproofing and Built-upRoofing.Current edition approved May 1, 2018. Published June 2018. Originallyapproved in 1990. Last previous edition approved in 2010 as D5100/D5100M 95a(2010)1. DOI: 10.1520/D5100_D5100M-95AR18.2For
15、 referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700,
16、 West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the Worl
17、d Trade Organization Technical Barriers to Trade (TBT) Committee.17.5 Immediately apply mineral aggregate into hot bitumenand spread uniformly over entire surface within the tray.Allowthe assembly to cool for 30 min minimum.7.6 Turn sample upside down and collect loose aggregate.Weigh the loose aggr
18、egate and record this mass as B.7.7 Repeat the procedure three more times, recording eachindividual mass determination.8. Calculation8.1 Calculate the mass of the adhered aggregate for each testas:C 5 A 2 B (1)where:C = mass of the adhered aggregate in pounds per square foot(4.88 (A B) gives the mas
19、s of the adhered aggregate inkg/m2).8.2 Calculate the mean mass of the adhered aggregate Cmbydividing the sum of the four determinations by four.8.3 Calculate an estimate of the standard deviation s by:s 54(C22 (C!212(2)8.4 Calculate the standard error of the mean S by:S 5s2(3)9. Report9.1 Report th
20、e following information:9.1.1 The type of aggregate, including screen grading, andthe type of bitumen used.9.1.2 The mass of the adhered aggregate for any singledetermination as Cm6 3.18 s (95 % level of confidence).9.1.3 The mean mass of adhered aggregate as Cm63.18 S.10. Precision and Bias10.1 Pre
21、cisionThe precision of this test method dependson the characteristics of the mineral aggregate. The precision ofany single test series can be estimated from the statisticsrequired by the test method. Differences between laboratoriescan be tested with standard statistical techniques such as thenull h
22、ypothesis.10.2 BiasThe procedure of this test method for the adhe-sion of mineral aggregate to hot bitumen has no bias becausethe quantity of aggregate adhered in the laboratory is definedby this test method.11. Keywords11.1 adhered mineral aggregate; hot bitumen; roof mem-braneASTM International ta
23、kes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own r
24、esponsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addre
25、ssed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at t
26、he address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (p
27、hone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Bitumen Application Rates and TemperaturesASTM Standard TypeApplicationTemperatureC FApplication RateSpecification D312/D312MIIIIIIIV177143502520414400252181442525232144502560 g/tray or 2.9 kg/m260 lb/100 ft2Specification D450/D450MIIII1821436025191143752575 g/tray or 3.7 kg/m275 lb/100 ft2D5100/D5100M 95a (2018)2
