1、Designation: D5616 04 (Reapproved 2010)Standard Specification forReclaimed Trichloroethylene1This standard is issued under the fixed designation D5616; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A nu
2、mber in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the grades of trichloroethyl-ene2typically needed in various industries for noncriticalapplications such as in
3、metal cleaning formulations. It may beused as a reference document by purchasers or personsestablishing in-house trichloroethylene recovery programs.2. Referenced Documents2.1 ASTM Standards:3D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acidsand Other Related Products4D2108 Test Method for Co
4、lor of Halogenated OrganicSolvents and Their Admixtures (Platinum-Cobalt Scale)D2109 Test Methods for Nonvolatile Matter in HalogenatedOrganic Solvents and Their AdmixturesD2111 Test Methods for Specific Gravity and Density ofHalogenated Organic Solvents and Their AdmixturesD2942 Test Method for Tot
5、al Acid Acceptance of Haloge-nated Organic Solvents (Nonreflux Methods)D2989 Test Method for Acidity-Alkalinity of HalogenatedOrganic Solvents and Their AdmixturesD3401 Test Methods for Water in Halogenated OrganicSolvents and Their AdmixturesD3741 Test Methods for Appearance of Admixtures Con-taini
6、ng Halogenated Organic SolventsD6806 Practice for Analysis of Halogenated Organic Sol-vents and Their Admixtures by Gas Chromatography2.2 Code of Federal Regulations:529 CFR 1910.1200 Department of Labor, OSHA Regula-tions, Hazard Communication49 CFR Parts 100 to 199 Department of TransportationHaza
7、rdous Materials Regulations3. Classification3.1 Type IGenerally recognized for use in precision ap-plications.3.2 Type IIUse for less-demanding precision applications.3.3 Type IIIMay not be suitable for all applications.4. Properties4.1 Type I reclaimed trichloroethylene shall meet the re-quirements
8、 of Table 1.4.2 Type II reclaimed trichloroethylene shall meet the re-quirements of Table 1.4.3 Type III reclaimed trichloroethylene shall meet therequirements of Table 1.5. Packaging5.1 Industrial or commercial quantities shall be packagedand labeled in accordance with DOT regulations as found in 4
9、9CFR 100 to 199, in accordance with state and local regulations,and in accordance with OSHA regulations found in 29 CFR1919.1200.6. Keywords6.1 halogenated solvent; reclaimed; TCE; tri;trichloroethyleneTypes I, II, and III1This specification is under the jurisdiction of ASTM Committee D26 onHalogena
10、ted Organic Solvents and Fire Extinguishing Agents and is the directresponsibility of Subcommittee D26.02 on Vapor Degreasing.Current edition approved Feb. 1, 2010. Published March 2010. Originallyapproved in 1994. Last previous edition approved in 2004 as D5616 04. DOI:10.1520/D5616-04R10.2Trichlor
11、oethylene: CAS No. 79-01-6.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4Withdrawn. The last approved vers
12、ion of this historical standard is referencedon www.astm.org.5Available from the Superintendent of Documents, U. S. Government PrintingOffice, Washington, DC 20402.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.ASTM International ta
13、kes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own r
14、esponsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addre
15、ssed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at t
16、he address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (p
17、hone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).TABLE 1 PropertiesProperty Specification Test MethodType I Type II Type IIISpecific gravi
18、ty, 25/25 1.45 to 1.46 1.44 to 1.47 1.43 to 1.48 D2111Nonvolatile residue, ppm, max 50 50 50 D2109Water, ppm, max 100 100 150 D3401 orD1064Assay, wt % 99.5 99.0 97.0 D68061,1,1 trichloroethane content, wt %, max 0.02 0.05 0.5 D6806Color, Pt-Co, max 20 20 35 D2108Appearance clear and freefrom suspendedmatterclear and freefrom suspendedmatterclear and freefrom suspendedmatterD3741Acid acceptance, as NaOH, wt %, min 0.16 0.16 0.20 D2942Acidity, as HCl, ppm, max 1.0 1.0 1.0 D2989D5616 04 (2010)2
