1、Designation: D6984 12bD6984 13Standard Test Method forEvaluation of Automotive Engine Oils in the Sequence IIIF,Spark-Ignition Engine1This standard is issued under the fixed designation D6984; the number immediately following the designation indicates the year oforiginal adoption or, in the case of
2、revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.INTRODUCTIONThis test method described can be used by any properly equipped laboratory; it does not require
3、theassistance of anyone outside that laboratory. However, the ASTM Test Monitoring Center (TMC)2provides reference oils and an assessment of the test results obtained on those oils by the laboratory(see Annex A1). By these means, the laboratory will know whether their use of the test method givesres
4、ults statistically similar to those obtained by other laboratories. Furthermore, various agenciesrequire that a laboratory utilize the TMC services in seeking qualification of oils against specifications.For example, the U.S. Army imposes such a requirement in connection with several Army enginelubr
5、icating oil specifications.Accordingly, this test method is written for use by laboratories that utilize the TMC services.Laboratories that choose not to use those services may simply ignore those portions of the test methodthat refer to the TMC.This test method may be modified by means of Informati
6、on Letters issued by the TMC. In addition,the TMC may issue supplementary memoranda related to the test method (see A1.8).1. Scope*1.1 This test method covers an engine test procedure for evaluating automotive engine oils for certain high-temperatureperformance characteristics, including oil thicken
7、ing, varnish deposition, oil consumption, as well as engine wear. Such oilsinclude both single viscosity grade and multiviscosity grade oils that are used in both spark-ignition, gasoline-fueled engines, aswell as in diesel engines.NOTE 1Companion test methods used to evaluate engine oil performance
8、 for specification requirements are discussed in SAE J304.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 ExceptionsThe values stated in inches for ring gap measurements are to be regarded as standard, and where ther
9、e is nodirect SI equivalent such as screw threads, National Pipe Threads/diameters, tubing size, or single source supply equipmentspecifications.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibilityof the user of this stan
10、dard to establish appropriate safety and health practices and determine the applicability of regulatoryrequirements prior to use.1.4 This test method is arranged as follows:Subject SectionScope 1Referenced Documents 2Terminology 3Summary of Test Method 4Significance and Use 5Apparatus 61 This test m
11、ethod is under the jurisdiction of ASTM Committee D02 on Petroleum Products Products, Liquid Fuels, and Lubricants and is the direct responsibility ofSubcommittee D02.B0.01 on Passenger Car Engine Oils.Current edition approved Dec. 1, 2012Oct. 1, 2013. Published March 2013October 2013. Originally ap
12、proved in 2003. Last previous edition approved in 2012 asD6984D6984 12b.12a. DOI: 10.1520/D6984-12B.10.1520/D6984-13.2 Until the next revision of this test method, the ASTM Test Monitoring Center will update changes in the test method by means of information letters. Information lettersmay be obtain
13、ed from the ASTM Test Monitoring Center, 6555 Penn Avenue, Pittsburgh, PA 15206-4489. Attention: Administrator. www.astmtmc.cmu.edu. This editionincorporates revisions contained in all information letters through 12-1.132.This document is not an ASTM standard and is intended only to provide the user
14、 of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as
15、published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1Subject SectionLaboratory 6.1Drawings 6.2Specified Equipment
16、6.3Test Engine 6.4Engine Parts 6.4.1Engine Speed and Load Control 6.5Sequence IIIF Fluid Conditioning Module 6.6Engine Cooling System 6.6.1Flushing Tank 6.7Coolant Mixing Tank 6.8Condenser Cooling Systems 6.9Engine Oil-Cooling System 6.10Fuel System 6.11Induction Air Supply Humidity, Temperature, an
17、d Pressure 6.12Temperature Measurement 6.13Thermocouple Location 6.13.1Air-to-Fuel Ratio Determination 6.14Injector Flow Testing 6.14.1Exhaust and Exhaust Back Pressure Systems 6.15Blowby Flow Rate Measurement 6.16Pressure Measurement and Sensor Location 6.17Reagents and Materials 7Test Fuel 7.1Engi
18、ne and Condenser Coolant 7.2Coolant Additive 7.3Coolant Preparation 7.4Pre-Test Cleaning Materials 7.5Sealing and Anti-seize Compounds 7.6Test Oil Sample Requirements 8Preparation of Apparatus 9Condenser Cleaning 9.1Intake Manifold Cleaning 9.3Cleaning of Engine Parts (other than the block and heads
19、) 9.4Engine Block Cleaning 9.5Cylinder Head Cleaning 9.6Engine Build-up Procedure 9.7General Information 9.7.1Special Parts 9.7.2Hardware Information 9.7.3Fastener Torque Specifications and TorquingProcedures9.7.4Parts Replacement 9.8Engine Block Preparation 9.9Piston Fitting and Numbering 9.10Pisto
20、n Ring Fitting 9.10.1Pre-Test Camshaft and Lifter Measurements 9.11Camshaft Bearing Installation 9.12Camshaft Installation 9.13Main Bearings 9.14Crankshaft Installation 9.14.1Main Bearing Cap Installation 9.14.2Crankshaft Sprocket 9.15Camshaft Sprocket and Timing Chain 9.16Crankshaft End Play 9.17Pi
21、ston Pin Installation 9.18Piston Installation 9.18.1Harmonic Balancer 9.19Connecting Rod Bearings 9.20Engine Front Cover 9.21Coolant Inlet Adapter 9.22Oil Dipstick Hole 9.23Oil Pan 9.24Cylinder Head Assembly 9.25Adjustment of Valve Spring Loads 9.26Cylinder Head Installation 9.27Hydraulic Valve Lift
22、ers 9.28Pushrods 9.29Valve Train Loading 9.30Intake Manifold 9.31Rocker Covers 9.32Water Inlet Adapter 9.33Condenser 9.34Coolant Outlet Adapter 9.35External Oil Cooling System 9.36Oil Sample Valve 9.37Ignition System 9.38Throttle Body 9.39D6984 132Subject SectionAccessory Drive Units 9.40Exhaust Man
23、ifolds, Water-Cooled 9.41Engine Flywheel 9.42Pressure Checking of Engine Coolant System 9.43Lifting of Assembled Engines 9.44Mounting the Engine on the Test Stand 9.45External Cooling System Cleaning 9.46Engine Coolant Jacket Cleaning (Flushing) 9.47Coolant Charging 9.48Test Oil Charging 9.49Engine
24、Oil Pump Priming 9.50Calibration 10Laboratory and Engine Test Stand Calibration 10.1Testing of Reference Oils 10.2Reference Oil Test Frequency 10.3Reporting of Reference Oil Test Results 10.4Evaluation of Reference Oil Test Results 10.5Status of Non-Reference Oil Tests Relative to ReferenceOil Test1
25、0.6Status of Test Stands Used for Non-Standard Tests 10.7Data Acquisition and Control 10.8Sample Rate 10.8.1Measurement Accuracy 10.8.2Temperature 10.8.3Pressure 10.8.4Flow 10.8.5Speed 10.8.6Load 10.8.7Measurement Resolution 10.8.8System Time Response 10.8.9Quality Index 10.8.10Engine Operating Proc
26、edure 11Dipstick and Hole Plug 11.1Dipstick Hole O-ring 11.2Engine Start-up and Shutdown Procedures 11.3Start-up 11.4Scheduled Shutdown 11.5Non-Scheduled Shutdowns 11.6Oil Sampling 11.7Oil Leveling 11.8Air-to-Fuel-Ratio Measurement and Control 11.9Air-to-Fuel Ratio Verification 11.10Blowby Flow Rate
27、 Measurement 11.11NOx Determinations 11.12Data Recording 11.13Initial Run (10 min) 11.14Engine Oil Quality Testing (80 h) 11.15Test Termination 11.16Determination of Test Results 12Engine Disassembly 12.2Preparation of Parts for Rating of Sticking, Deposits,and Plugging12.3Piston Deposit Rating 12.4
28、Post-Test Camshaft and Lifter Wear Measurements 12.5End-of Test Used Oil Sample Testing 12.6Viscosity Test 12.7Testing Oil Samples for Wear Metals 12.8Blowby Flow Rate Measurements 12.9Oil Consumption Computation 12.10Photographs of Test Parts 12.11Retention of Representative Test Parts 12.12Severit
29、y Adjustments 12.13Determination of Operational Validity 12.14Report 13Report Forms 13.1Precision of Reported Units 13.2Deviations from Test Operational Limits 13.3Precision and Bias 14Keywords 15AnnexesD6984 133Subject SectionThe Role of the ASTM Test Monitoring Center (TMC) andthe Calibration Prog
30、ramAnnex A1Sequence IIIF Test Parts Replacement Guidelines Annex A2Sequence IIIF Determination Volume of Engine Oil in Pan Annex A3Sequence IIIF Test Fuel Analysis Annex A4Sequence IIIF Test Reporting Annex A5Sequence IIIF Test Air-to-Fuel Ratio Control Flow Chart Annex A6Sequence IIIF Test Set Poin
31、ts and Control States Annex A7Sequence IIIF Quality Index Upper and Lower Values Annex A8Sequence IIIF Engine Oil Level Worksheet Annex A9Engine Build Worksheets Annex A10Blowby Flow Rate Determination Annex A11Safety Precautions Annex A12Sequence IIIF Blueprint Listing Annex A13Fluid Conditioning M
32、odule Components Annex A14Engine Oil Cooling System Schematic Annex A15Guidelines For Hardware Subject To First In First OutCriteriaAnnex A16AppendixesSequence IIIFHD Test Procedure Appendix X1Sequence IIIFVIS Test Procedure Appendix X22. Referenced Documents2.1 ASTM Standards:3D86 Test Method for D
33、istillation of Petroleum Products at Atmospheric PressureD130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip TestD235 Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)D240 Test Method for Heat of Combustion of Liquid Hydrocarbon
34、 Fuels by Bomb CalorimeterD323 Test Method for Vapor Pressure of Petroleum Products (Reid Method)D381 Test Method for Gum Content in Fuels by Jet EvaporationD445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)D525 Test Method for Oxidation
35、 Stability of Gasoline (Induction Period Method)D1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator AdsorptionD2699 Test Method for Research Octane Number of Spark-Ignition Engine FuelD2700 Test Method for Motor Octane Number of Spark-Ignition Engine FuelD32
36、31 Test Method for Phosphorus in GasolineD3237 Test Method for Lead in Gasoline by Atomic Absorption SpectroscopyD3338 Test Method for Estimation of Net Heat of Combustion of Aviation FuelsD3343 Test Method for Estimation of Hydrogen Content of Aviation FuelsD4052 Test Method for Density, Relative D
37、ensity, and API Gravity of Liquids by Digital Density MeterD4175 Terminology Relating to Petroleum, Petroleum Products, and LubricantsD4485 Specification for Performance of Active API Service Category Engine OilsD4684 Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oil
38、s at Low TemperatureD4815 Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C1 to C4 Alcohols inGasoline by Gas ChromatographyD5185 Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by InductivelyCoupled Plasma Atomic Emissi
39、on Spectrometry (ICP-AES)D5191 Test Method for Vapor Pressure of Petroleum Products (Mini Method)D5293 Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between 5 and 35C Using Cold-CrankingSimulatorD5452 Test Method for Particulate Contamination in Aviation Fuels by Laboratory Filtr
40、ationD5453 Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel,and Engine Oil by Ultraviolet FluorescenceD5862 Test Method for Evaluation of Engine Oils inTwo-Stroke CycleTurbo-Supercharged 6V92TADiesel Engine (Withdrawn2009)4D6557 Test
41、 Method for Evaluation of Rust Preventive Characteristics of Automotive Engine OilsD6593 Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in a Spark-Ignition InternalCombustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditio
42、ns3 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.4 The last approved version of this historical standard is
43、referenced on www.astm.org.D6984 134D6750 Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine1K Procedure (0.4 % FuelSulfur) and 1N Procedure (0.04 % Fuel Sulfur)D7320 Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engi
44、neD7422 Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel EngineE29 Practice for Using Significant Digits in Test Data to Determine Conformance with SpecificationsE191 Specification forApparatus For Microdetermination of Carbon and Hydrogen in Organic and Orga
45、no-Metallic CompoundsE608/E608M Specification for Mineral-Insulated, Metal-Sheathed Base Metal ThermocouplesE1119 Specification for Industrial Grade Ethylene GlycolG40 Terminology Relating to Wear and ErosionIEEE/ASTM SI-10 Standard for Use of the International System of Units (SI): The Modern Metri
46、c System2.2 Military Specification:5MIL-PRF-2104 Lubricating Oil, Internal Combustion Engine, Tactical Service2.3 SAE Standards:6J183 Engine Oil Performance and Engine Service Classification (Other Than “Energy-Conserving”)J300 Engine Oil Viscosity Classification *HS-23/00*J304 Engine Oil Tests2.4 O
47、ther ASTM Document:7CRC ASTM Deposit Rating Manual 20 Rating Techniques and Breakdown Methods(Formerly CRC Manual 20)3. Terminology3.1 Definitions:3.1.1 blowby, nin internal combustion engines, that portion of the combustion products and unburned air/fuel mixture thatleaks past piston rings into the
48、 engine crankcase during operation.3.1.2 BTDC (before top dead center), nused with the degree symbol to indicate the angular position of the crankshaft relativeto its position at the point of uppermost travel of the piston in the cylinder.3.1.3 calibrate, vto determine the indication or output of a
49、device (e.g., thermometer, manometer, engine) with respect to thatof a standard.3.1.4 clogging, nthe restriction of a flow path due to the accumulation of material along the flow path boundaries. D41753.1.5 cold-stuck piston ring, nin internal combustion engines, a piston ring that is stuck when the piston and ring are at roomtemperature, but inspection shows that it was free during engine operation.3.1.5.1 DiscussionA cold-stuck piston ring cannot be moved with moderate finger pressure. It is characterized by a polished face over its entirecircumference, indic
