ASTM D7578-2010 9375 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants《石油产品和润滑剂元素分析的校准要求的标准指南》.pdf
《ASTM D7578-2010 9375 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants《石油产品和润滑剂元素分析的校准要求的标准指南》.pdf》由会员分享,可在线阅读,更多相关《ASTM D7578-2010 9375 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants《石油产品和润滑剂元素分析的校准要求的标准指南》.pdf(12页珍藏版)》请在麦多课文档分享上搜索。
1、Designation: D7578 10Standard Guide forCalibration Requirements for Elemental Analysis ofPetroleum Products and Lubricants1This standard is issued under the fixed designation D7578; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, t
2、he year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This guide covers different ways by which the testmethods used for elemental analysis of petroleum product
3、andlubricant samples are calibrated before the sample analysis.1.2 Uniform practice for test method calibration is benefi-cial in standardizing the procedures, and obtaining consistentresults across different laboratories.1.3 This guide includes only the basic steps for generallyencountered instrume
4、nt types. Anything out of the ordinarymay require special procedures. See individual test methods forinstructions to handle such situations.1.4 This guide is not a substitute for a thorough understand-ing of the actual test method to be used, caveats it contains, andadditional instrument preparation
5、 that may be required.1.5 The user should not expand the scope of the testmethods to materials or concentrations outside the scope of thetest methods being used.1.6 This guide should also be applicable to sample prepa-ration of non-petroleum based bio-fuels for elemental analysis.Work is underway on
6、 these aspects in Subcommittee D02.03.As more information becomes available, it will be added to thisstandard.1.7 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.8 This standard does not purport to address all of thesafety con
7、cerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D129 Test Method for Sulfur in Petrole
8、um Products (Gen-eral Bomb Method)D445 Test Method for Kinematic Viscosity of Transparentand Opaque Liquids (and Calculation of Dynamic Viscos-ity)D482 Test Method for Ash from Petroleum ProductsD808 Test Method for Chlorine in New and Used PetroleumProducts (Bomb Method)D874 Test Method for Sulfate
9、d Ash from Lubricating Oilsand AdditivesD892 Test Method for Foaming Characteristics of Lubricat-ing OilsD1018 Test Method for Hydrogen In Petroleum FractionsD1091 Test Methods for Phosphorus in Lubricating Oilsand AdditivesD1266 Test Method for Sulfur in Petroleum Products(Lamp Method)D1318 Test Me
10、thod for Sodium in Residual Fuel Oil (FlamePhotometric Method)D1548 Test Method for Vanadium in Navy Special FuelOil3D1552 Test Method for Sulfur in Petroleum Products(High-Temperature Method)D1839 Test Method for Amyl Nitrate in Diesel FuelsD2622 Test Method for Sulfur in Petroleum Products byWavel
11、ength Dispersive X-ray Fluorescence SpectrometryD2784 Test Method for Sulfur in Liquefied PetroleumGases (Oxy-Hydrogen Burner or Lamp)D3120 Test Method for Trace Quantities of Sulfur in LightLiquid Petroleum Hydrocarbons by Oxidative Microcou-lometryD3228 Test Method for Total Nitrogen in Lubricatin
12、g Oilsand Fuel Oils by Modified Kjeldahl MethodD3230 Test Method for Salts in Crude Oil (ElectrometricMethod)D3231 Test Method for Phosphorus in GasolineD3237 Test Method for Lead in Gasoline by Atomic Ab-sorption Spectroscopy1This practice is under the jurisdiction of ASTM Committee D02 on Petroleu
13、mProducts and Lubricants and is the direct responsibility of Subcommittee D02.03 onElemental Analysis.Current edition approved Feb. 15, 2010. Published March 2010. DOI: 10.1520/D7578-10.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceas
14、tm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Withdrawn. The last approved version of this historical standard is referencedon www.astm.org.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshoho
15、cken, PA 19428-2959, United States.D3246 Test Method for Sulfur in Petroleum Gas by Oxida-tive MicrocoulometryD3340 Test Method for Lithium and Sodium in LubricatingGreases by Flame PhotometerD3341 Test Method for Lead in GasolineIodineMonochloride MethodD3348 Test Method for Rapid Field Test for Tr
16、ace Lead inUnleaded Gasoline (Colorimetric Method)D3605 Test Method for Trace Metals in Gas Turbine Fuelsby Atomic Absorption and Flame Emission SpectroscopyD3831 Test Method for Manganese in Gasoline By AtomicAbsorption SpectroscopyD4045 Test Method for Sulfur in Petroleum Products byHydrogenolysis
17、 and Rateometric ColorimetryD4046 Test Method for Alkyl Nitrate in Diesel Fuels bySpectrophotometryD4047 Test Method for Phosphorus in Lubricating Oils andAdditives by Quinoline Phosphomolybdate MethodD4294 Test Method for Sulfur in Petroleum and PetroleumProducts by Energy Dispersive X-ray Fluoresc
18、ence Spec-trometryD4307 Practice for Preparation of Liquid Blends for Use asAnalytical StandardsD4628 Test Method for Analysis of Barium, Calcium,Magnesium, and Zinc in Unused Lubricating Oils byAtomic Absorption SpectrometryD4629 Test Method for Trace Nitrogen in Liquid PetroleumHydrocarbons by Syr
19、inge/Inlet Oxidative Combustion andChemiluminescence DetectionD4927 Test Methods for Elemental Analysis of Lubricantand Additive ComponentsBarium, Calcium, Phospho-rus, Sulfur, and Zinc by Wavelength-Dispersive X-RayFluorescence SpectroscopyD4929 Test Methods for Determination of Organic ChlorideCon
20、tent in Crude OilD4951 Test Method for Determination of Additive Ele-ments in Lubricating Oils by Inductively Coupled PlasmaAtomic Emission SpectrometryD5056 Test Method for Trace Metals in Petroleum Coke byAtomic AbsorptionD5059 Test Methods for Lead in Gasoline by X-Ray Spec-troscopyD5184 Test Met
21、hods for Determination of Aluminum andSilicon in Fuel Oils by Ashing, Fusion, InductivelyCoupled Plasma Atomic Emission Spectrometry, andAtomic Absorption SpectrometryD5185 Test Method for Determination of Additive Ele-ments, Wear Metals, and Contaminants in Used Lubricat-ing Oils and Determination
22、of Selected Elements in BaseOils by Inductively Coupled Plasma Atomic EmissionSpectrometry (ICP-AES)D5291 Test Methods for Instrumental Determination ofCarbon, Hydrogen, and Nitrogen in Petroleum Productsand LubricantsD5384 Test Methods for Chlorine in Used Petroleum Prod-ucts (Field Test Kit Method
23、)D5453 Test Method for Determination of Total Sulfur inLight Hydrocarbons, Spark Ignition Engine Fuel, DieselEngine Fuel, and Engine Oil by Ultraviolet FluorescenceD5600 Test Method for Trace Metals in Petroleum Coke byInductively Coupled Plasma Atomic Emission Spectrom-etry (ICP-AES)D5622 Test Meth
24、ods for Determination of Total Oxygen inGasoline and Methanol Fuels by Reductive PyrolysisD5708 Test Methods for Determination of Nickel, Vana-dium, and Iron in Crude Oils and Residual Fuels byInductively Coupled Plasma (ICP)Atomic Emission Spec-trometryD5762 Test Method for Nitrogen in Petroleum an
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