1、Designation: F1097 17 An American National StandardStandard Specification forMortar, Refractory (High-Temperature, Air-Setting)1This standard is issued under the fixed designation F1097; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revisi
2、on, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers dry air-setting refractory mor-tar for use in laying and bonding refractory
3、brick in ship boilerfurnaces and wet air-setting refractory mortar for use in layingrefractory brick in stationary boiler furnaces, bright annealingfurnaces, controlled atmosphere furnaces, and furnaces heatedby electric elements.1.2 The values stated in inch-pound units are to be regardedas standar
4、d. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this stand
5、ard to establish appro-priate safety, health, and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on
6、 Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2C24 Test Method for Pyrometric Cone Equivalent (PCE) ofFireclay and High Alumina Refract
7、ory MaterialsC27 Classification of Fireclay and High-Alumina RefractoryBrickC92 Test Methods for Sieve Analysis and Water Content ofRefractory MaterialsC133 Test Methods for Cold Crushing Strength and Modu-lus of Rupture of RefractoriesC198 Test Method for Cold Bonding Strength of RefractoryMortarC1
8、99 Test Method for Pier Test for Refractory Mortars2.2 Federal Specifications3The following documents shallapply only when one or more of the requirements of Supple-mentary Requirement S1 are specified in the contract orpurchase order (see 4.1.3):UU-S-48 Sacks, Shipping, PaperPPP-B-704 Pails: Shippi
9、ng, Steel (1 through 12 gallon)2.3 Military Standards3The following documents shallapply only when one or more of the requirements of Supple-mentary Requirement S1 are specified in the contract orpurchase order (see 4.1.3):MIL-STD-129 Marking for Shipment and StorageMIL-STD-147 Palletized Unit Loads
10、2.4 ANSI/ASQ Standards:4Z1.4 Sampling Procedures and Tables for Inspection byAttributes3. Classification3.1 The refractory mortar shall be of the following types:3.1.1 Type 1Dry.3.1.2 Type 2Wet.4. Ordering Information4.1 Orders for material under this specification shall includethe following informa
11、tion, as necessary to adequately describethe material:4.1.1 ASTM designation and year of issue,4.1.2 Type required (see 3.1), and4.1.3 Optional requirements, if any (see SupplementaryRequirement S1).5. Material5.1 The mortar shall be composed of finely ground heat-resistant clays, minerals, or a mix
12、ture of clays and minerals ineither a dry or wet condition.1This specification is under the jurisdiction of ASTM Committee F25 on Shipsand Marine Technology and is the direct responsibility of Subcommittee F25.07 onGeneral Requirements.Current edition approved Dec. 1, 2017. Published January 2018. O
13、riginallyapproved in 1991. Last previous edition approved in 2012 as F1097 91 (2012).DOI: 10.1520/F1097-17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the stand
14、ards Document Summary page onthe ASTM website.3Available from DLA Document Services, Building 4/D, 700 Robbins Ave.,Philadelphia, PA 19111-5094, http:/quicksearch.dla.mil.4Available from American National Standards Institute (ANSI), 25 W. 43rd St.,4th Floor, New York, NY 10036, http:/www.ansi.org.Co
15、pyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of Interna
16、tional Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.15.1.1 Type 1, DryMortar shall be furnished dry and shallbe ready for use as soon as mixed with water. Mortar, afterbeing mixed with water and then dried, shall be capable
17、ofbeing remixed with water.5.1.2 Type 2, WetMortar shall be furnished ready for useat a trowelling consistency and shall be easily mixed withwater to a dipping consistency.6. Performance Requirements6.1 Resistance to Heat SoakingMortar shall not soften norshow any evidence of fusion, and the shrinka
18、ge shall not begreater than hairline cracks when tested as specified in 11.2.6.2 Bonding StrengthThe average modulus of rupture atthe brick joint when tested as specified in 11.3 shall be not lessthan shown in Table 1.6.3 Pyrometric Cone Equivalent (PCE)The PCE shall benot less than cone 32 (see 11.
19、4).7. Requirements7.1 FinenessMortar shall be ground to such fineness thatnot more than 5 % shall be retained on a No. 40 ASTM sieve,and not more than 0.5 % shall be held on a No. 30ASTM sieve(see 11.1).7.2 Shelf Life, Type 1Mortar shall show no deteriorationafter 1 years storage.7.3 Shelf Life, Typ
20、e 2At any time within one year ofshipment from the supplier, the mortar in a previously un-opened container shall not have stiffened to such an extent asto interfere with its easy removal and mixing.7.4 ConsistencyMortar, when tempered with water, shallbe of such consistency that it will be suitable
21、 for spreadingeasily with a trowel or for dipping and for laying refractorybrick and bonding them together upon drying and uponsubsequent heating at furnace temperatures. Mortar shall retainthis degree of workability for 2 h.7.4.1 The mixed mortar shall have sufficient water retentionto permit a116-
22、in. (2-mm) joint to be made with a trowellingconsistency, but not allow the newly laid brick to float out ofposition.8. Workmanship8.1 Workmanship shall be first class in every respect. Thereshall be no foreign material or caked aggregate lumps in themortar. Wet mortar shall be easily removed from t
23、he containerand shall mix easily to a uniform trowelling consistency.9. Sampling9.1 An inspection lot for tests and inspections shall consistof all material manufactured at essentially the same time and ofthe same type offered for delivery at one time.9.2 For the tests specified in 11.1 through 11.4
24、, the sampleunit shall be 15 lb (7 kg) of mortar. No fewer than three sampleunits shall be randomly selected throughout the lot. No morethan one sample shall be drawn from any one container.9.2.1 The test sample shall be a 45-lb (20-kg) composite ofthe randomly selected sample units. Two or more det
25、ermina-tions as applicable (see Table 2) shall be performed on thecomposite. There shall be no evidence of failure to meet thespecified unit or average requirements.9.3 The PCE shall be determined on two cones of differentsamples from each lot. If both cones fail, this shall be cause forrejection wi
26、thout retest. If either cone fails, three additionalcones shall be made, each from a different sample. If any oneof the three retest cones fails, this shall be cause for rejection.10. Specimen Preparation10.1 The entire mortar sample for testing shall be thor-oughly mixed to ensure uniformity before
27、 any portion is takenfor tests. The selected portion of Type 1 (dry) mortar shall bemixed with water to a trowelling consistency for the tests of11.2 and 11.3. Storage time after water mixing shall be 20 to30minutes.10.2 For the test specified in 11.3, brick-mortar joints shallbe prepared in accorda
28、nce with Test Method C198, except thatrefractory bricks, conforming to Classification C27,60%High-Alumina, shall be used and shall be cut in half. The twohalves of each brick shall be placed in a device suitable forbringing, with a straight motion, the molded ends together withthe faces parallel at
29、all times to form a bond.10.2.1 Asmall quantity of mortar shall be spread by a trowelon the upper face forming the bond to ensure intimate contact.Sufficient mortar to give a18-in. (3-mm) thick layer shall bespread evenly on the lower bond forming face and the upperhalf shall be lowered until it is1
30、16 in. (2 mm) from the lowerhalf. The excess mortar shall be cut from the joint, flush withthe sides of the brick. The unit thus formed shall be removedat once from the bond-forming machine. The bond specimensshall be allowed to air-dry for 20 to 24 hours.11. Test Methods11.1 FinenessThe fineness te
31、st shall be made in accor-dance with Test Methods C92.11.2 Heat Soak:11.2.1 A pier of refractory brick, conforming to Classifica-tion C27, super-duty, laid up with the test mortar shall beprepared and heated at 2910F (1588C) for 5 hours inaccordance with Test Method C199.11.2.2 The cooled pier shall
32、 be examined for evidence ofshrinkage, softening, or fusion of the mortar. One or moremortar joints shall be broken and the freshly broken mortarsurface shall be viewed from various angles. Any shininess orlight flash at the mortar surface shall be considered anindication of excessive fusion.11.3 Bo
33、nding Strength:11.3.1 Five bond specimens (see 10.2) shall be placed in anoven operating at 230F (110C) for at least 16 hours; fivebond specimens shall be held at each of the other testTABLE 1 Bonding Strength of MortarTemperatures, F (C)Average Modulus of Rupture,psi (kPa), min230 (110) 200 (1400)1
34、000 (538) 100 (700)2000 (1093) 100 (700)F1097 172temperatures (1000F, 2000F (538C, 1093C) for 5 hoursand then allowed to cool in the closed furnace for 12 to 18hours. The time required to reach test temperatures shall be 3hours. The bond shall not be broken until the specimens havereached approximat
35、ely room temperature.11.3.2 The modulus of rupture of the test specimens shall bedetermined in accordance with Test Methods C133, except thatthe load shall be applied at the rate of 1000 lb/min (450kg/min).11.3.2.1 In conducting this test, bring the upper bearingedge to bear on the joint itself.11.4
36、 Pyrometric Cone EquivalentThe PCE shall be deter-mined in accordance with Test Method C24.12. Inspection12.1 Unless otherwise specified in the contract or purchaseorder, the supplier is responsible for the performance of allinspection requirements as specified herein. Except as other-wise specified
37、, the supplier may use his own facilities or anycommercial laboratory acceptable to the purchaser. The pur-chaser reserves the right to perform any of the inspections setforth in the specification where such inspections are deemednecessary to ensure supplies and services conform to pre-scribed requi
38、rements.13. Packaging13.1 Packing of the mortar shall be sufficient to affordadequate protection against deterioration and physical damageduring shipment from the supply source to the first receivingactivity for immediate use and may conform to the supplierscommercial practice.14. Keywords14.1 bondi
39、ng strength; mortar; refractory mortarSUPPLEMENTARY REQUIREMENTSThe following supplementary requirements shall apply only when specified in the contract orpurchase order (see 4.1.3).S1. Special Government RequirementsS1.1 Quality Conformance Inspection:S1.1.1 Sampling for quality conformance inspect
40、ion shall beperformed in accordance with the provisions set forth inANSI/ASQ Z1.4, except where otherwise indicated.S1.1.2 Examination of the end item shall be made inaccordance with the classification of defects, inspection levels,and quality levels specified in S1.1.2.1 through S1.1.2.3. Thelot si
41、ze, for the purpose of determining the sample size inaccordance with ANSI/ASQ Z1.4, shall be expressed in unitsof filled containers for the examinations in S1.1.2.1 andS1.1.2.2.S1.1.2.1 Examination of the end item container for defects inappearance, workmanship, closures, and marking (see TableS1.1)
42、. The sample unit for this examination shall be one filledcontainer.S1.1.2.2 Examination of end item container for defects in netcontents. The sample unit for this examination shall be onefilled primary container. The average net contents shall be notless than the specified or indicated quantity.S1.
43、1.2.3 Inspection levels for examinations. The inspectionlevels for determining the sample size shall be as specified inTable S1.2.TABLE 2 Testing RequirementsCharacteristicSpecificationReferenceNumber of Determinations per CompositeResults Reported asRequirement TestMethodPass orFailANumerically toN
44、earestBType 1 and Type 2, as applicableFinenessRetained on No. 40 ASTM sieve 7.1 11.1 2 . 0.1%Retained on No. 30 ASTM sieve 7.1 11.1 2 . 0.1%Resistance to heat soakingMelting 6.1 11.2 2 X .Shrinkage 6.1 11.2 2 X .Bonding strength 6.2After heating at230F (110C) 11.3 avg of 5 . . . psi1000F (538C) 11.
45、3 avg of 5 . . . psi2000F (1098C) 11.3 avg of 5 . . . psiPyrometric cone:CType 1 6.3 11.4 2 . . . cone numberAIf failure is indicated, report description of failure or numerical point of failure as applicable.BTest report shall include all values on which results are based.CSee 9.3.F1097 173S1.1.2.4
46、 Examination for workmanship. For the examinationfor conformance to Section 8, the sample unit shall be one bagof dry mortar or one drum of wet mortar, as applicable. Theexamination may be made during selection of samples fortesting or other examinations. For each lot, select a sample sizein accorda
47、nce with Table S1.2. Reject the lot on one failure.See Note S1.1.NOTE S1.1Optional Requirements of 4.1.3 when included in contractor purchase order can state when Acceptance Quality Limits (AQL) of 1(Reject: 2) can be used for lot sizes of 501 to 35 000, orAQL of 2 (Reject:3) can be used for lot siz
48、es of 35 001 to 500 000 or AQL of 3 (Reject: 4)can be used for lot sizes over 500 000 for examinations of S1.1.2. OptionalRequirements of 4.1.3 should also state when AQL of 1 (Reject: 2) can beused for lot sizes of more than 35 000 for examinations of S1.1.2.2.S1.2 Tests:S1.2.1 For the tests specif
49、ied in 11.1 through 11.4, theinspection level for determining sample size shall be S1 inaccordance with ANSI/ASQ Z1.4.S1.2.2 First Article Testing (FAT)Unless otherwise speci-fied in the purchase order or contract First Article Testing(FAT) shall be done in accordance with conformance require-ments of 6.1 through 6.3 and 7.1 to determine if mortar meetsphysical, mechanical and fineness requirements of the specifi-cation; see Note S1.2. Complete FAT reports must be submittedfor government review and approval, or government informa-tion depen
