1、| | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | BRITISH STANDARD BS EN ISO 105-J01:2000 Th
2、e European Standard EN ISO 105-J01:1999 has the status of a British Standard ICS 59.080.01 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW Textiles Tests for colour fastness Part J01: General principles for measurement of surface colourThis British Standard, having been prepar
3、ed under the direction of the Sector Committee for Materials and Chemicals, was published under the authority of the Standards Committee and comes into effect on 15 August 2000 BSI 08-2000 ISBN 0 580 36123 3 BS EN ISO 105-J01:2000 Amendments issued since publication Amd. No. Date Comments National f
4、oreword This British Standard is the official English language version of EN ISO 105-J01:1999. It is identical with ISO 105-J01:1997. It supersedes method J01 of BS 1006:1990. The UK participation in its preparation was entrusted to Technical Committee TCI/81, Colour fastness and colour measurement,
5、 which has the responsibility to: aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate
6、 them in the UK. A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references Attention is drawn to the fact that CEN and CENELEC Standards normally include an annex which lists normative references to international publications with their corre
7、sponding European publications. The British Standards which implement these international or European publications may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Ca
8、talogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document c
9、omprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, page ii, pages 1 to 13, the annex ZA page, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued.EN ISO
10、 105-J01:1999A Referencenumbe r ISO105J01:1997(E) INTERNATIONAL STANDARD ISO 105J01 Fourthedition 19971215 TextilesTestsforcolourfastness PartJ01: Generalprinciplesformeasurementofsurface colour TextilesEssaisdesoliditdesteintures PartieJ01:Principesgnrauxdumesuragedelacouleurdesurface EN ISO 105-J0
11、1:1999ii Foreword ISO(theInternationalOrganizationforStandardization) isaworldwide federationofnationalstandardsbodies(ISOmemberbodies).Thework of preparingInternationalStandardsisnormallycarriedoutthroughISO technicalcommittees.Eachmemberbodyinterestedinasubjectfor which atechnicalcommitteehasbeene
12、stablishedhas the right to be represented onthatcommittee.Internationalorganizations,governmenta landnon governmental,inliaisonwithISO,alsotakepartinthework.ISO collaboratescloselywiththeInternationalElectrotechnicalCommission (IEC)onallmattersofelectrotechnicalstandardization. DraftInternationalSta
13、ndardsadoptedbythetechnica lcommitteesare circulatedtothememberbodiesforvoting.PublicationasanInternational Standard requires approval byatleast7 5 %ofthememberbodiescasting avote. InternationalStandardISO 105J01waspreparedby Technical Committee ISO/TC38, Textiles,SubcommitteeSC1, Testsforcolouredte
14、xtilesand colorants. Thisfourtheditioncancelsandreplaces the third edition (ISO105J01:1989),whichhasbeentechnicallyrevised. ISO 105waspreviouslypublishedinthirteen“parts”,eachdesignatedby a letter(e.g.“Par t A”),withpublicationdatesbetween1978and1985 .Each partcontainedaseriesof“sections”,eac hdesig
15、natedbytherespective partletterandbyatwodigitserialnumber(e.g.“SectionA01”).These sectionsarenowbeingrepublishedasseparatedocuments, themselves designated“parts”butretainingtheirearlieralphanumericdesignations.A completelistofthesepartsisgiveninISO105A01. AnnexAformsanintegralpartofthispartofISO 105
16、.AnnexBisfor informationonly. EN ISO 105-J01:19991 TextilesTestsforcolourfastness PartJ01: Generalprinciplesformeasurementofsurfacecolour 1 Scope ThispartofISO105isdesignedasareferencedocumenttosupportthepropermeasurementofthecolour ofspecimensbyinstrumentalmeansasrequiredinmanypartsofISO105.Thedocu
17、mentdescribes generalconceptsandproblemsassociatedwithreflectancecolourmeasurement. AnnexAspecifiestechniquesandspecimenhandlingprocedures. 2 Normativereferences Thefollowingstandardscontainprovisionswhich,throughreferenceinthistext,constituteprovisions ofthispartofISO105.Atthetimeofpublication,thee
18、ditionsindicatedwerevalid.Allstandardsare subjecttorevision,andpartiestoagreementbasedonthispartofISO105areencouragedtoinvestigate thepossibilityofapplyingthemostrecenteditionsofthestandardsindicatedbelow.MembersofIECand ISOmaintainregistersofcurrentlyvalidInternationalStandards. ISO139:1973, Textil
19、esStandardatmospheresforconditioningandtesting. CIEPublicationNo.15.2, Colorimetry,2nded.(1986) 1) . 3 Definitions ForthepurposesofthispartofISO105,thefollowingdefinitionsapply. 3.1 colourmeasurement: Anumericalrepresentationofthecolourofaspecimenobtainedbyuseof acolourmeasuringinstrument;asinglemea
20、surementmayrepresentanaverageofmultiplereadingsofa specimen. _ 1)AvailablefromtheInternationalCommissiononIlluminationCentralBureau,Kegelgasse27,A1030Vienna, Austria. EN ISO 105-J01:19992 3.2 colourmeasuringinstrument: Anydevice(suchasacolorimeterorspectrophotometer)usedto measuretherelativeamountof
21、radiationreflectedfromaspecimeninthevisibleregionofthespectrum (comprisingthewavelengthsfrom360nmto780nm,andincludingasaminimumtheregionfrom 400nmto700nm). 3.3 geometry (ofacolourmeasuringinstrument ):Oneofthefollowingillumination/viewing conditions. d/0 0/d 0/45 45/0 whichdescribestheangleormanneri
22、nwhichacolourmeasuringinstrument 1)illuminatesthespecimen: d0045 2)viewstheresultingreflectedlight: 0(0 10 ) d450 d=diffuse;0=normal(0 to10 );45(452)=tolerablerangeoftheanglebetweenthedirectionof illuminationorviewingandthenormaltothespecimen. NOTEInstrumentsofdifferentgeometriesmayproducedifferentc
23、olorimetricresultsonmosttextile materials. 3.4 areaofviewopticalaperture (ofacolourmeasuringinstrument ):Thedimensions(sizeand shape)ofthesurfaceareathatacolourmeasuringinstrumentiscapableofcoveringinasinglecolour measurement. 3.5 fluorescence:Aphenomenoninwhichradiantfluxofcertainwavelengthsisabsor
24、bedand reemittedatother,usuallylonger,wavelengths. 3.6 reflectance:Theratioofthereflectedradiantorluminousflux(light)totheincidentfluxinthe givenconditions. 3.7 reflectancefactor: Theratioofthefluxreflectedfromthespecimentothefluxreflectedfromthe perfectreflectingdiffuserunderthesamegeometricandspec
25、tralconditionsofmeasurement. 3.8 specularreflection: Thereflectionwithoutdiffusion,inaccordancewiththelawsofoptical reflection,asinamirror. 3.9 standardization(ofcolourmeasuringinstrument ):Theactofmeasuringoneormorecalibrated materialswithacolourmeasuringinstrumentforthepurposeofcalculatingasetofco
26、rrectionfactorsto beappliedtosubsequentmeasurements. EN ISO 105-J01:19993 NOTECalibrationistypicallyperformedbyaninstrumentmanufacturertoensurethattheinstrumentmeets thecriteriaasestablishedbynationalstandardizinglaboratories. 3.10 verificationstandard: Incolourmeasurement,anystablematerialwhichisus
27、edforthepurpose ofconfirming(orverifying)thevalidityofaninstrumentstandardization.Colourmeasurements,which aremadeimmediatelyfollowingastandardization,arecomparedtooriginalmeasurementsofthestandard todetectimproperstandardization. 4 Principle Materialsofanopaqueornearlyopaquenature(butnottranslucent
28、)aremeasuredbyreflectancemethods inordertoobtainanumericalrepresentationofthecolourofthespecimen. NOTES 1Properequipmentsetup,standardizationofthecolourmeasuringinstrumentandproperpresentationofthetest specimenstotheinstrumentarerequiredtoachieveconsistent,reliableandmeaningfulreflectancemeasurement
29、 results. 2Ingeneral,instrumentalcolourmeasurementproceduresaredictatedbythetypeofspecimentobemeasured andtheinstrumentwithwhichitwillbemeasured.Manytypesofcolourmeasuringinstrumentationareavailable, differinginsuchfeaturesasareaofview,illuminationmethod,andgeometry.Theuseriscautionedthat conflictin
30、gresultsmaybeobtainedoncomparisonsofdataacquiredoninstrumentsofdifferentdesigns. 5 Apparatus 5.1 Reflectancecolourmeasuringinstrumen t,forilluminatingaspecimenandmeasuringthe amountoflightwhichisreflectedfromthesurfaceofthespecimen.Illuminationisusuallypolychromatic (whitelight);howevermonochromatic
31、modeisacceptablefornonfluorescentspecimens.Reflectance colourmeasuringinstrumentsmaybebroadlydividedintotwogroups: a)Spectrophotometers(typicallydiffuse/0,usingpolychromaticillumination)separateandmeasure thespectrumoflightreflectedfromthespecimenrelativetoareferencewhiteatregularintervals (waveleng
32、thintervalsof5nm,10nmand20nmaremostcommon).Thesedatamaybeusedto calculatethedesiredtristimulusvalues (X,Y,Z)foranygivenilluminantandobserver.Some spectrophotometers(typically0/diffuse)illuminatethesamplewithmonochromaticlightandmeasure theamountoflightreflectedfromthesurfaceasthesampleisilluminateda
33、tregularwavelength intervals. b)Colorimetersmeasurethetristimulusvalues (X,Y,Z)directlythroughbroadbandfilterswhichare designedtoproducecolorimetricvaluesforoneilluminantandobserver(typicallyC/2).Measurement ofreflectancefactorsatspecificwavelengthsisnotpossiblewithacolorimeter. Withinthesetwocatego
34、ries,theinstrumentsarefurtherdefinedbytheirgeometryasdefinedin3.3. EN ISO 105-J01:19994 Diffuse/0(sphere)instrumentsilluminatethespecimenindirectlywhenthespecimenisplacedagainsta portopeningintoadiffuselyilluminatedsphereandviewthespecimenatananglebetween 0 and10 fromtheperpendicular.Thisarrangement
35、isdesignedtocapturealllightreflectedfromthespecimen. Somesphereinstrumentswithaviewinganglegreaterthan 0 includeaspecularportwhichpermitsthe inclusionorexclusionofthespecularreflectance. 0/diffuse(sphere)instrumentsaresimilar,butthepathofilluminationandviewingarereversed.This methodilluminatesthesam
36、pleatananglebetween 0 and10 andmeasurestheamountoflightreflected fromthesurfaceintothesphere. Instrumentswith45/0(or0/45)geometryilluminatethespecimenatthefirstangleandviewthespecimen atthesecond.Thesetwogeometriescanbeeithercircumferential(viewingorilluminatingat45tothe specimeninacompletecircle)or
37、directional.Formosttextilesamples,either45/0or0/45yield equivalentresults. 5.2 Whitecalibratedstandard ,withwhichtostandardizetheinstrument.Thecolorimetricvaluesfor thiscalibrationstandardarestoredintheinstrumentorthesoftwareandrequireonlythataspecific standardbeusedtostandardizetheinstrument.Thecor
38、rectwhitestandardisusuallyidentifiedwitha serialnumber. 5.3 Blackstandard ,requiredforsomeinstruments.Itmaybeofzeroreflectance(alighttrap)orit maybecalibrated,inwhichcasethecommentsin5.2apply. 6 Procedure 6.1 General a)Collectandpreparespecimen,notinganyspecialsamplingand/orconditioningprocedurestha
39、tmay berequiredasdescribedin6.3(seealsoannexA). b)Standardizeinstrumentaccordingto6.2.Maintainarecordoftheprocedureandtheresultsofany verificationstandardsmeasured. c)Presentspecimentocolourmeasuringinstrumentfollowinganyspecialtechniquesrequiredforthe typeofmaterialbeingmeasuredpersection6.4(seeals
40、oannexA). d)Measurethecolourofthespecimen,obtainingtheappropriatespectralreflectancefactors(or tristimulusvaluesifacolorimeterisused). e)Calculatecolorimetricvalues,ifrequired,asdescribedinclause7. 6.2 Standardization Properstandardizationofanycolourmeasuringinstrumentisnecessaryinordertoachievemore
41、precise andaccurateresults.Whiledifferenttypesofinstrumentsrequirevaryingmethodsofstandardization, therearecommonprincipleswhichshallbeobserved. EN ISO 105-J01:19995 Ingeneral,instrumentstandardizationinvolvesmeasuringacleanwhitesurfaceofknownreflectance factorsandcalculating(throughsoftwarebuiltint
42、otheinstrumentorcomputerprogram)aseriesof correctionfactorswhichwillbeappliedtosubsequentmeasurements.Someinstrumentsalsorequirea blacktile(orlighttrap),andpossiblyagreytile.Eachofthesematerialsshallbemaintainedinitsoriginal clean,unscratchedcondition.Refertothespecificmanufacturersrecommendationsfo
43、rcleaning instructions. Thefrequencywithwhichthisstandardizationisperformeddependsonmanyfactorsincludingthetype ofinstrument,theenvironmentalconditionsinwhichtheinstrumentoperates,andtherequiredaccuracy oftheresults.Formostapplications,anintervalof2hto4hisacceptable. Oncethestandardizationstephasbee
44、nperformed,itisimportanttoverifythesuccessoftheprocedure bymeasuringsomecolouredmaterial s (verificationstandards)andcomparingtheresultingcolorimetric valuestotheoriginalvaluesforthesematerials.Ifthemeasuredvaluesdonotfallwithinanacceptable variationfromtheiroriginalvalues,thestandardizationisnotconsideredvalid.Thenumberof verification standardsandtheacceptabilitylimitsdependonuserrequirements,butaret
