1、July 2009DEUTSCHE NORM English price group 6No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 75.140; 91.100.50!$XO9“153
2、4422www.din.deDDIN EN 13304Bitumen and bituminous binders Framework for specification of oxidised bitumensEnglish version of DIN EN 13304:2009-07Bitumen und bitumenhaltige Bindemittel Spezifikationsrahmen fr oxidiertes BitumenEnglische Fassung DIN EN 13304:2009-07SupersedesDIN EN 13304:2003-07www.be
3、uth.deDocument comprises 7 pagesDIN EN 13304:2009-07 2 National foreword This standard has been prepared by Technical Committee CEN/TC 336 “Bituminous binders” (Secretariat: AFNOR, France). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Test
4、ing Standards Committee), Joint Technical Committee NA 062-03-32 GA Bitumen; Prfverfahren und Anforderungen fr die Bindemittel. Amendments This standard differs from DIN EN 13304:2003-07 as follows: a) EN ISO 3838 has been deleted from clause 2 “Normative references” and EN 15326 has been added. b)
5、Table 1 in clause 3 has been revised. Previous editions DIN EN 13304: 2003-07 EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 13304March 2009ICS 75.140; 91.100.50 Supersedes EN 13304:2003 English VersionBitumen and bituminous binders - Framework for specification ofoxidised bitumensBitumes et lian
6、ts bitumineux - Cadre de spcifications desbitumes oxydsBitumen und bitumenhaltige Bindemittel -Spezifikationsrahmen fr oxidiertes BitumenThis European Standard was approved by CEN on 10 February 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the condit
7、ions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three of
8、ficial versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria,
9、 Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE F
10、OR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13304:2009: EEN 13304:2009 (E) 2 Contents Page Fo
11、reword 31 Scope 42 Normative references 43 Properties and test methods 44 Typical grades 5DIN EN 13304:2009-07 EN 13304:2009 (E) 3 Foreword This document (EN 13304:2009) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European
12、 Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2009, and conflicting national standards shall be withdrawn at the latest by September 2009. Attention is drawn to the possibility that some of the ele
13、ments of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 13304:2003. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
14、 countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia
15、, Spain, Sweden, Switzerland and the United Kingdom. DIN EN 13304:2009-07 EN 13304:2009 (E) 4 1 Scope This European Standard provides a framework for the specification of oxidised bitumens used mainly in roofing, waterproofing, adhesives and thermal and phonic insulations. Within Europe several type
16、s of oxidised bitumens are used and, dependent on climatic conditions, type of building construction and traditional practices, different grades may be used for the same purpose. The framework given in this European standard provides a basis for quality agreements to be established between supplier
17、and client. The oxidised bitumen products are graded by a combination of the values of ring and ball softening point, and penetration at 25 C, expressed as multiples of 5. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated refe
18、rences, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1426, Bitumen and bituminous binders Determination of needle penetration EN 1427, Bitumen and bituminous binders Determination of the softening point R
19、ing and Ball method EN 12592, Bitumen and bituminous binders Determination of solubility EN 12593, Bitumen and bituminous binders Determination of the Fraass breaking point EN 13301, Bitumen and bituminous binders Determination of staining tendency of bitumen EN 13302, Bitumen and bituminous binders
20、 Determination of viscosity of bitumen using a rotating spindle apparatus EN 13303, Bitumen and bituminous binders Determination of the loss in mass after heating of industrial bitumen EN 15326, Bitumen and bituminous binders Measurement of density and specific gravity Capillary-stoppered pyknometer
21、 method EN ISO 2592, Determination of flash and fire points - Cleveland open cup method (ISO 2592:2000) 3 Properties and test methods The specification of oxidised bitumens shall be made according to the rules given in Table 1: DIN EN 13304:2009-07 EN 13304:2009 (E) 5 Table 1 Properties and test met
22、hods Property Test methods Unit Limits and tolerance Ring and ball softening point aEN 1427 C 5 of mid-point valuee Penetration at 25 CEN 1426 0,1 mm 5 of mid-point valuee Solubility in toluene b EN 12592 % 99,0 Loss in mass after heating EN 13303 % 0,5 Flash point EN ISO 2592 C 250 Fraass breaking
23、point EN 12593C NR cStaining properties EN 13301 mm NR cDynamic viscositydEN 13302 Pas NR cDensity EN 15326kg/m3NR caRing and ball softening point testing for oxidised bitumens are carried out in glycerol, as the values typically are above 80 C. bIf other solvents are used, it shall be stated in the
24、 test report. cNR: No requirements. Values can be agreed between the client and the supplier dThe type of instrument used to determine viscosity should be agreed between supplier and client. eMid-point value: value which defines the ring and ball softening point class or the penetration class.4 Typi
25、cal grades Typical grades for oxidised bitumens are: 85/25; 85/40; 95/25; 95/35; 100/40; 105/35; 110/30; 115/15. EXAMPLE 85/25 means that the ring and ball softening point of the product is between 80 C and 90 C and penetration between 20 x 0,1 mm and 30 x 0,1 mm. NOTE This list does not imply that all grades are available in all countries, neither is it intended to be comprehensive or limiting. Other grades may be supplied in accordance with the local practices and by agreement between client and supplier. DIN EN 13304:2009-07