EN 1348-2007 2341 Adhesives for tiles - Determination of tensile adhesion strength for cementitious adhesives《瓷砖胶粘剂 混凝土胶粘剂粘接强度的测定》.pdf

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1、Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIg49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58s

2、trength for cementitious adhesivesThe European Standard EN 1348:2007 has the status of a British StandardICS 83.180; 91.100.10Adhesives for tiles Determination of tensile adhesion BRITISH STANDARDBS EN 1348:2007BS EN 1348:2007Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, U

3、ncontrolled Copy, (c) BSIThis British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 December 2007 BSI 2007ISBN 978 0 580 57398 9Amendments issued since publicationAmd. No. Date Commentscontract. Users are responsible for its correct application.Compl

4、iance with a British Standard cannot confer immunity from legal obligations.National forewordThis British Standard is the UK implementation of EN 1348:2007. It supersedes BS EN 1348:1999 which is withdrawn.The UK participation in its preparation was entrusted to Technical Committee B/539, Ceramic ti

5、les and other rigid tiling.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 1348August 2007ICS 83.180; 91.100.10 Supersede

6、s EN 1348:1997 English VersionAdhesives for tiles - Determination of tensile adhesion strengthfor cementitious adhesivesColles carrelage - Dtermination de ladhrence partraction des mortiers-collesMrtel und Klebstoffe fr Fliesen und Platten - Bestimmungder Haftfestigkeit zementhaltiger Mrtel fr innen

7、 undauenThis European Standard was approved by CEN on 21 January 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographic

8、al references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN me

9、mber into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, L

10、atvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brusse

11、ls 2007 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 1348:2007: ELicensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative r

12、eferences 4 3 Sampling.4 4 Test conditions 4 5 Test materials.4 5.1 General4 5.2 Ceramic tiles.5 5.3 Concrete slab .5 6 Apparatus .5 6.1 Weight .5 6.2 Pull-head plates .5 6.3 Tensile testing machine 5 6.4 Air-circulating oven .5 6.5 Notched trowel.5 7 Mixing of the adhesive 5 8 Procedure .6 8.1 Prep

13、aration of test units .6 8.2 Initial adhesion strength .6 8.3 Tensile adhesion strength after water immersion6 8.4 Tensile adhesion strength after heat ageing 7 8.5 Tension adhesion strength after freeze-thaw cycle.7 9 Evaluation and expression of results7 10 Test report 8 Licensed Copy: Wang Bin, I

14、SO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 3 Foreword This document (EN 1348:2007) has been prepared by Technical Committee CEN/TC 67 “Ceramic tiles”, the secretariat of which is held by UNI. This European Standard shall be given the status of a nationa

15、l standard, either by publication of an identical text or by endorsement, at the latest by February 2008, and conflicting national standards shall be withdrawn at the latest by February 2008. This document supersedes EN 1348:1997. According to the CEN/CENELEC Internal Regulations, the national stand

16、ards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Po

17、rtugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 4 1 Scope This European Standard specifies a method for the determination of the tensile adhesion st

18、rength of cementitious ceramic tile adhesives. This European Standard is applicable to all cementitious adhesives and cementitious adhesives with separate components for internal and external ceramic tile installations on walls and floors. This European Standard does not contain performance requirem

19、ents or recommendations for the design and installation of ceramic tiles. NOTE Ceramic tile adhesives can be used also for other kinds of tiles (natural and agglomerated stones etc.), if they do not adversely affect the stones. 2 Normative references The following referenced documents are indispensa

20、ble for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 196-1:2005, Methods of testing cement Part 1: Determination of strength EN 1067, Adhesives Exam

21、ination and preparation of samples for testing EN 1323, Adhesives for tiles Concrete slabs for tests EN 12004, Adhesives for tiles Requirements, evaluation of conformity, classification and designation EN 14411, Ceramic tiles Definitions, classification, characteristics and marking EN ISO 15605, Adh

22、esives Sampling (ISO 15605:2000) 3 Sampling Take, at least, 2 kg test sample of the adhesive in accordance with EN ISO 15605 and EN 1067. 4 Test conditions Standard conditions shall be (23 2) C and (50 5) % relative humidity and a speed of air in the testing area of less than 0,2 m/s. 5 Test materia

23、ls 5.1 General Condition all test materials (adhesive etc.) to be tested for at least 24 h under standard conditions. The adhesive to be tested shall be within its shelf life, where this is specified. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSI

24、EN 1348:2007 (E) 5 5.2 Ceramic tiles The tiles shall be checked prior to conditioning to ensure that they are new, clean, dry and of the following type of tile: type V1: dry pressed ceramic tile in accordance with EN 14411, group BIa , with a water absorption 0,5 % by mass, unglazed and with a plain

25、, matt, adhering surface, with facial dimensions of (50 1) mm (50 1) mm. 5.3 Concrete slab The concrete slab shall comply with EN 1323. 6 Apparatus 6.1 Weight A mass capable of exerting a force of (20 0,05) N, with a cross sectional area of less than 50 mm 50 mm. 6.2 Pull-head plates Square metallic

26、 plates, with dimensions of (50 1) mm (50 1) mm and a minimum thickness of 10 mm, with a suitable fitting for connection to the test machine. 6.3 Tensile testing machine A test machine for direct pull tensile force test and with suitable capacity and sensitivity for the test. The machine shall be ca

27、pable of applying the load to the pull-head plate at the rate of (250 50) N/s through a suitable fitting that does not exert any bending force. 6.4 Air-circulating oven An air-circulating oven capable of controlling the temperature to within 3 C. 6.5 Notched trowel A notched trowel having 6 mm 6 mm

28、notches at 12 mm centres. 7 Mixing of the adhesive The amount of water and/or liquid admix, required for preparing the adhesive, shall be as stated by the manufacturer in parts by mass (e.g. the amount of liquid, in kilos and the amount of powder, in kilos, to be mixed, shall be declared). If a rang

29、e of values is given, the average shall be used. A minimum quantity of 2 kg of the adhesive shall be prepared in a mixer of the type described in 4.4 of EN 196-1:2005, using the slow speed settings (140 5) r/min and (62 5) r/min planetary movement. Carry out the following procedure: pour the liquid

30、into the pan; scatter the dry powder over the liquid; mix for 30 s; Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 6 take out the mixing paddle; scrape down the paddle and pan within 1 min; replace the paddle and mix for 1 min. Let

31、 the adhesive mature in accordance with the adhesive manufacturers instructions, followed by further mixing for 15 s. 8 Procedure 8.1 Preparation of test units Apply a thin layer of the adhesive, mixed in accordance with Clause 7, to the concrete slab with a straight edge trowel. Then apply a thicke

32、r layer and comb with a notched trowel (6.5). The trowel shall be held at an angle of approximately 60 to the substrate at a right angle to one edge of the slab and drawn across the slab parallel to that edge (in a straight line). After 5 min place ten type V1 tiles on the adhesive at a distance apa

33、rt of 50 mm and load each tile with (20 0,05) N for 30 s. 8.2 Initial adhesion strength Prepare the test units in accordance with 8.1. After 27 days storage under standard conditions bond the pull-head plates (see 6.2) to the tiles with a suitably high strength adhesive (e.g. epoxide). After a furth

34、er 24 h storage under standard conditions determine the tensile adhesion strength of the adhesive by applying a force at a constant rate of (250 + 50) N/s. If fast-setting properties of adhesives are to be tested, also determine the tensile adhesion strength 6 h after bonding, under standard conditi

35、ons (see Clause 4). Report the results in Newtons. 8.3 Tensile adhesion strength after water immersion Prepare the test units in accordance with 8.1. Condition the test units under standard conditions for 7 days, and immerse in water at the standard temperature. After 20 days remove the test units f

36、rom the water, wipe with a cloth and bond the pull-head plates (6.2) to the tiles. After a further 7 h immerse the test units in water at the standard temperature. The following day remove the test units from water and immediately carry out the tensile adhesion test in accordance with 8.2. Report th

37、e results in Newtons. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 7 8.4 Tensile adhesion strength after heat ageing Prepare the test units in accordance with 8.1. Condition the test units under standard conditions for 14 days an

38、d then place the units in an air-circulating oven at (70 3) C for a further 14 days. Remove from the oven and bond the pull-head plates (6.2) to the tiles with a suitable high strength adhesive (e.g. epoxide). Condition the test units for a further 24 h under standard conditions. Determine the tensi

39、le adhesion strength in accordance with 8.2. Report the results in Newtons. 8.5 Tension adhesion strength after freeze-thaw cycle Prepare the test units in accordance with 8.1. In addition a layer of the adhesive approximately 1 mm thick shall be applied with a straight edged trowel to the back face

40、 of the type V1 tile before placing. Condition the test units for 7 days under standard conditions and immerse in water for 21 days before carrying out 25 freeze-thaw cycles. For each freeze-thaw cycle: 1) remove the test units from the water and and place in a cold chamber to achieve a steady cabin

41、et temperature of (-15 3) C within 2 h 20 min; 2) maintain the test units at (-15 3) C for 2 h 20 min; 3) immerse the test units in water at (20 3) C and raise the temperature to (15 3) C; 4) maintain the test units at (15 3) C for a minimum 2 h before commencing the next freeze-thaw cycle. Repeat t

42、he cycle 25 times. After the last cycle remove the test units from water, wipe with a cloth and bond the pull-head plates (6.2) to the tiles. Condition the test units for a further 24 h under standard conditions and determine the tensile adhesion strength in accordance with 8.2. Report the results i

43、n Newtons. 9 Evaluation and expression of results The individual tensile adhesion strength shall be determined to an accuracy of 0,1 N/mm2using the following equation: As= L / A where Asis the individual tensile adhesion strength in Newtons per square millimetre; L is the total load in Newtons; A is

44、 the bonding area in square millimetres (2 500 mm2). The tensile adhesion strength for each set of conditions shall be determined as follows: Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIEN 1348:2007 (E) 8 determine the mean of the ten values; di

45、scard the values falling outside the range of 20 % from the mean value; if five or more than five values remain, determine the new mean value; if less than five values remain, repeat the test; determine the mode of failure of the test units according to EN 12004 as the predominant mode. 10 Test repo

46、rt The test report shall provide the following information: a) number and year of issue of this European Standard, i.e. EN 1348:2007; b) place, date and time of sampling; c) type of adhesive, commercial designation and manufacturer; d) identification of test sample; e) handling and storage of sample

47、s before testing; f) test conditions; g) date of test; h) amount of water or liquid used for preparing the adhesive; i) test results (individual and mean values and the mode of failure); j) tensile adhesion strength for each condition in Newtons per square millimetre; k) any other factor that could

48、have influenced the result. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIblankLicensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02/2008 06:39, Uncontrolled Copy, (c) BSIBS EN BSILicensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 28/02

49、/2008 06:39, Uncontrolled Copy, (c) BSI389 Chiswick High RoadLondonW4 4AL1348:2007BSI British Standards InstitutionBSI is the independent national body responsible for preparing British Standards. It presents the UK view on standards in Europe and at the international level. It is incorporated by Royal Charter.RevisionsBritish Standards are updated by amendment or revision. Users of British Standards should make sure that they possess the latest amendments or editions.It is

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