1、BSI Standards PublicationBS EN 16709:2015Automotive fuels HighFAME diesel fuel (B20 andB30) Requirements and testmethodsBS EN 16709:2015 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 16709:2015.The UK participation in its preparation was entrusted to Technical
2、Committee PTI/2, Liquid Fuels.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. The British Standards Institution 2
3、015.Published by BSI Standards Limited 2015ISBN 978 0 580 85146 9ICS 75.160.20Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Committee on 31 October 2015.Amendments/corrigenda
4、 issued since publicationDate T e x t a f f e c t e dBS EN 16709:2015EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16709 October 2015 ICS 75.160.20 English Version Automotive fuels - High FAME diesel fuel (B20 and B30) - Requirements and test methods Carburants pour automobiles - Carburant di
5、esel haute teneur en EMAG (B20 et B30) - Exigences et mthodes dessai Kraftstoffe fr Kraftfahrzeuge - Dieselkraftstoffmischungen mit hohem FAME-Anteil (B20 und B30) - Anforderungen und Prfverfahren This European Standard was approved by CEN on 29 August 2015. CEN members are bound to comply with the
6、CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management
7、Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as
8、 the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Net
9、herlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2015 CEN All r
10、ights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16709:2015 EBS EN 16709:2015EN 16709:2015 (E) 2 Contents Page Foreword 3 1 Scope 4 2 Normative references 4 3 Captive fleet application . 5 4 Sampling . 6 5 Pump marking 6 6 Requirements and t
11、est methods 6 6.1 Dyes and markers . 6 6.2 Additives . 6 6.2.1 General 6 6.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT) . 6 6.3 Fatty acid methyl ester (FAME) 7 6.4 Other (bio-) components 7 6.5 Generally applicable requirements and related test methods . 7 6.6 Climate dependent requiremen
12、ts and related test methods 9 6.7 Precision and dispute . 10 Annex A (informative) A-deviations . 12 Bibliography . 13 BS EN 16709:2015EN 16709:2015 (E) 3 European foreword This document (EN 16709:2015) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and rela
13、ted products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2016, and conflicting national standards
14、 shall be withdrawn at the latest by April 2016. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document is related to the Europ
15、ean Fuels Directive 98/70/EC including amendments 2003/17/EC, 2009/30/EC and 2011/63/EU 1, 2, 3 and 4 and the requirements therein are connected to requirements in this standard. This document describes two fuel grades in the range of (14 20) % (V/V) and (24 30) % (V/V) of fatty acid methyl ester (F
16、AME) in diesel fuel to be used in captive fleet application for designated vehicles1), as it is not suitable for all vehicles. Information on the development of this fuel specification can be found in CEN/TR 16557 5. According to the CEN-CENELEC Internal Regulations, the national standards organizat
17、ions of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malt
18、a, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. 1) In the sense that they are compatible with the product. BS EN 16709:2015EN 16709:2015 (E) 4 1 Scope This European Standard specifies requirements and test methods for
19、marketed and delivered high FAME (B20 and B30) diesel fuel for use in diesel engine vehicles designed or subsequently adapted to run on high FAME (B20 and B30) fuel. High FAME (B20 and B30) diesel fuel is a mixture of up to 20 % (V/V) in total and up to 30 % (V/V) in total respectively fatty acid me
20、thyl esters (commonly known as FAME) complying to EN 14214 and automotive diesel fuel complying to EN 590. For maintenance and control reasons high FAME (B20 and B30) diesel fuel is to be used in captive fleets that are intended to have an appropriate fuel management (see Clause 3). NOTE 1 For the p
21、urposes of this European Standard, the terms “% (m/m)” and “% (V/V)” are used to represent respectively the mass fraction and the volume fraction. NOTE 2 In this European Standard, A-deviations apply (see Annex A). 2 Normative references The following documents, in whole or in part, are normatively
22、referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 116:2015, Diesel and domestic heating fuels Determination of cold
23、filter plugging point Stepwise cooling bath method EN 12916:20062, Petroleum products Determination of aromatic hydrocarbon types in middle distillates High performance liquid chromatography method with refractive index detection EN 12662:2014, Liquid petroleum products Determination of total contam
24、ination in middle distillates, diesel fuels and fatty acid methyl esters EN 14078:2014, Liquid petroleum products Determination of fatty acid methyl ester (FAME) content in middle distillates Infrared spectrometry method EN 14214:2012+A1:2014, Liquid petroleum products Fatty acid methyl esters (FAME
25、) for use in diesel engines and heating applications Requirements and test methods EN 15195:2014, Liquid petroleum products Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels by combustion in a constant volume chamber EN 15751:2014, Automotive fuels Fatty acid
26、 methyl ester (FAME) fuel and blends with diesel fuel Determination of oxidation stability by accelerated oxidation method EN 16144:2012, Liquid petroleum products Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels Fixed range injection period, constant volume
27、 combustion chamber method EN 16329:2013, Diesel and domestic heating fuels Determination of cold filter plugging point Linear cooling bath method EN 16576:2014, Automotive fuels Determination of manganese and iron content in diesel Inductively coupled plasma optical emission spectrometry (ICP OES)
28、method 2) Under revision. BS EN 16709:2015EN 16709:2015 (E) 5 EN 23015:1994, Petroleum products Determination of cloud point (ISO 3015:1992) EN ISO 2719:20022), Determination of flash point Pensky-Martens closed cup method (ISO 2719:2002) EN ISO 3104:1996, Petroleum products Transparent and opaque l
29、iquids Determination of kinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994) EN ISO 3170:2004, Petroleum liquids Manual sampling (ISO 3170:2004) EN ISO 3171:1999, Petroleum liquids Automatic pipeline sampling (ISO 3171:1988) EN ISO 3405:2011, Petroleum products Determination of d
30、istillation characteristics at atmospheric pressure (ISO 3405:2011) EN ISO 3675:1998, Crude petroleum and liquid petroleum products Laboratory determination of density - Hydrometer method (ISO 3675:1998) EN ISO 3924:20102), Petroleum products Determination of boiling range distribution Gas chromatog
31、raphy method (ISO 3924:2010) EN ISO 4259:20062), Petroleum products Determination and application of precision data in relation to methods of test (ISO 4259:2006) EN ISO 5165:19982), Petroleum products Determination of the ignition quality of diesel fuels Cetane engine method (ISO 5165:1998) EN ISO
32、6245:2002, Petroleum products Determination of ash (ISO 6245:2001) EN ISO 12185:1996, Crude petroleum and petroleum products Determination of density Oscillating U-tube method (ISO 12185:1996) EN ISO 12937:2000, Petroleum products Determination of water Coulometric Karl Fischer titration method (ISO
33、 12937:2000) EN ISO 13032:2012, Petroleum products Determination of low concentration of sulfur in automotive fuels Energy-dispersive X-ray fluorescence spectrometric method (ISO 13032:2012) EN ISO 20846:2011, Petroleum products Determination of sulfur content of automotive fuels Ultraviolet fluores
34、cence method (ISO 20846:2011) EN ISO 20884:2011, Petroleum products Determination of sulfur content of automotive fuels Wavelength-dispersive X-ray fluorescence spectrometry (ISO 20884:2011) 3 Captive fleet application This European Standard is intended to cover fuels for use in captive fleet applic
35、ation for designated vehicles. Captive fleet is defined as a group of vehicles that use dedicated facilities and logistics for supply and storage of their fuel only accessible for them. The vehicles shall receive adequate maintenance as part of an organization or group agreement with the vehicle sup
36、plier(s). NOTE 1 The fleet is usually operated by a single organization, but might also be operated by a consortium of professional vehicle owners. NOTE 2 The fact that they are dedicated implies that fuel facilities are clearly identified as differing from public fuel facilities, by separate placem
37、ent, and to which accessibility is limited to only captive fleet users. BS EN 16709:2015EN 16709:2015 (E) 6 4 Sampling Samples shall be taken as described in EN ISO 3170 or EN ISO 3171 and/or in accordance with the requirements of national standards or regulations for the sampling of automotive dies
38、el fuel. The national requirements shall be set out in detail or shall be referred to by reference in a National Annex to this European Standard. In view of the sensitivity of some of the test methods referred to in this European Standard, particular attention shall be paid to compliance with any gu
39、idance on sampling containers which is included in the test method standard. 5 Pump marking Information to be marked on dispensing pumps used for delivering high FAME (B20 and B30) diesel fuel, and the dimensions of the mark shall be in accordance with the requirements of national standards or regul
40、ations for the marking of pumps for automotive fuel. Such requirements shall be set out in detail or shall be referred to by reference in a National Annex to this European Standard. Labelling shall be clearly visible, easily legible and displayed at any point where high FAME (B20 and B30) diesel fue
41、l with metallic additives is made available to consumers. The label shall contain: “Contains metallic additives” in the national language(s) and shall be laid down in the National Annex to this document. Should pump marking for high FAME (B20 and B30) diesel fuel be necessary for distinction to avoi
42、d misfuelling, it is recommended to use easily recognized visual symbols that a) identify that the diesel fuel has a fatty acid methyl ester (FAME) content greater than and including 14 % (V/V) and less than and including 20 % (V/V), in this case the recommended symbol is “B20”, or b) identify that
43、the diesel fuel has a fatty acid methyl ester (FAME) content greater than and including 24 % (V/V), and less than and including 30 %(V/V), in this case the recommended symbol is “B30”. 6 Requirements and test methods 6.1 Dyes and markers The use of dyes or markers is allowed. 6.2 Additives 6.2.1 Gen
44、eral In order to improve the performance quality, the use of additives is allowed. Suitable fuel additives without known harmful side-effects are recommended, in the appropriate amount, to help to avoid deterioration of driveability and emissions control durability. Other technical means with equiva
45、lent effect may also be used. NOTE Deposit forming tendency test methods suitable for routine control purposes have not yet been identified and developed. 6.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT) When methylcyclopentadienyl manganese tricarbonyl (MMT) is used, a specific labelling is
46、 required (see also Clause 5). MMT is a metallic additive that can be used in automotive fuels, but whose presence is limited since 1 January 20114. BS EN 16709:2015EN 16709:2015 (E) 7 6.3 Fatty acid methyl ester (FAME) High FAME (B20 and B30) fuel may contain from 14,0 %(V/V) up to 20,0 %(V/V) or f
47、rom 24,0 %(V/V) up to 30,0 % (V/V) of FAME complying with EN 14214, in which case the climate-dependent requirements set out in EN 14214:2012+A1:2014, 5.4.2 do not apply. Climate dependent requirements for FAME as a blending component for use in high FAME (B20 and B30) fuel according to this documen
48、t are set out in EN 14214:2012+A1:2014, 5.4.3. The specific grades shall be specified on a national basis according to local climatic conditions and the FAME volume in the diesel fuel. The finished blend of high FAME (B20 and B30) fuel shall also comply with the climate dependent requirements set ou
49、t in 6.6. Cold flow additives, when used in FAME, should be specifically matched to the base diesel fuel and FAME quality to ensure correct performance consistent with the requirements set out in this European Standard. The choice could result in incompatibility between the cold flow additives used in the FAME and the diesel fuel. The choice of cold flow additive technology should be a contractual matter between the fuel blender and the FAME supplier taking into account the climat
