1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions 2009 11 17 N-STATUS No known use. No replacement named D. DiGregorio, NA 2004 02 20 Revised Para 3.0 inserted; paras 1991 05 31 NB00I10043054098 Released R.D.Moore Printed copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC P
2、age 1 of 3 LUBRICANT, SOLID FILM, RESIN BONDED ESB-M99C107-A MOLYBDENUM DISULFIDE/PTFE, HEAT CURABLE NOT TO BE USED FOR NEW DESIGN 1. SCOPE The materials defined by this specification consists of a mixture of molybdenum disulfide and polytetrafluoroethylene in a phenolic binder, spray applied over p
3、hosphated steel. 2. APPLICATION This specification was released originally for a material used as a composite solid film lubricant, used to reduce friction on automotive door hardware components such as levers and sliding pins. 3. REQUIREMENTS 3.0 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Mater
4、ial suppliers and part producers must conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.4 BASE MATERIAL 3.4.1 Molybdenum Disulfide/Thermosetting Resin . Color Gray-black . Flash Point, C, min 23 (ASTM D 93) . Volatiles Distillation Range, C 103 - 153 (ASTM D
5、86) . Initial Boiling Point 103 . 10% Recovery 113.5 . 50% Recovery 128.5 . Final Boiling Point 153 . Non-Volatile Matter, by weight, min 35.0 (FLTM AK 105-01) . Resins, % weight, min 14.0 (See para 5.1 Test Procedure) . Molybdenum Disulfide, % by weight, 13.0 min (See para 5.1 Test Procedure) ENGIN
6、EERING MATERIAL SPECIFICATIONESB-M99C107-A Printed copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 2 of 3 3.4.2 Polytetrafluoroethylene/Thermosetting Resin 3.4.2.1 Component “A“ . Color White . Non-Volatile Matter 62.0 +/- 0.5 (PTFE), % by weight (FLTM AK 105-01) . Water,
7、 by weight 38.0 +/- 0.5 (ASTM D 1744) . Specific Gravity, 1.43 +/- 0.1 15.6/15.6 C (ASTM D 891) 3.4.2.2 Component “B“ . Color Blue . Flash Point, C, min 8 (ASTM D 93) . Volatiles Distillation Range, C 80 - 157 (ASTM D 86) . Initial Boiling Point 80 . 10% Recovery 91 . 50% Recovery 116 . 90% Recover
8、y 157 . Resins, % by weight 9.8 +/- 0.3 (FLTM AK 105-01) . Specific Gravity, 0.91 +/- 0.1 15.6/15.6 C (ASTM D 891) 3.5 COMPOSITE FILM PROPERTIES (Dry Film) . Color Gray-black . Coefficient of Friction (Static) 0.06 +/- 0.01 (FLTM BN 014-03) . Thickness 0.004 - 0.020 mm ENGINEERING MATERIAL SPECIFICA
9、TIONESB-M99C107-A Printed copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 3 of 3 5. GENERAL INFORMATION The information below is provided for clarification and assistance in meeting the requirements of this specification. 5.1 PROCEDURE FOR DETERMINATION OF RESINS, SOLIDS,
10、AND MOLYBDENUM DISULFIDE Weigh a known quantity of the material (A) into a tared centrifuge tube, and centrifuge at 2100 rpm for 30 minutes. Decant the liquid into a tared beaker, and add chloroform to the centrifuge tube. After shaking vigorously for several minutes, centrifuge at 2100 rpm for 30 m
11、inutes, and decant into the beaker; repeat. Dry the contents of the beaker and the centrifuge tube for four hours at 104 C. Determine the mass of the resins in the beaker (B) and the solids in the centrifuge tube (C). Weigh 0.1 to 0.2 g (D) of the solids remaining from the Molykote 106 extraction in
12、to a tared crucible, and place in a muffle furnace for eight hours at 1000 F. Determine the amount of molybdenum trioxide residue in the crucible (E). Calculate the amount of molybdenum disulfide as: (E) (1.112) (C) (100%) = % MoS2 - (D)(A) Calculate the amount of resins as: (B) (100%) = % resins - (A) Calculate the amount of solids as: (C) (100%) = % solids - (A)
