1、 ENGINEERING MATERIAL SPECIFICATION Date Action Revisions Rev 02 2011 08 02 Revised Revised 3.16; table editorial C. Richardson - FNA 2011 05 26 Revised Revised: 2, 3.2.2,3.3, 3.4, 3.6, 3.8, 3.12, 3.14,3.16, 3.16.1, 3.16.2; 3.18; table, ASTM methods format; inserted 3.5.5, 3.11.3, 3.20 C. Richardson
2、 - FNA 2006 05 22 Activated C. Richardson Controlled document at www.MATS Copyright 2011, Ford Global Technologies, LLC Page 1 of 4 FUEL, DIESEL, INITIAL FILL, ULTRA LOW SULFUR (ULSD) WSS-M4C130-A 1. SCOPE The material defined by this specification is a well-refined middle distillate petroleum produ
3、ct containing normal commercial additives. 2. APPLICATION This specification was released originally for material used as initial fill fuel for diesel engines in passenger cars and trucks designed to operate on15 ppm max sulfur fuel with cold flow properties controlled year round. 3. REQUIREMENTS Ma
4、terial specification requirements are to be used for initial qualification of materials. This material must meet the requirements of ASTM D975 Standard Specification for Diesel Fuel Oils plus the following: 3.1 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must
5、 conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 CETANE RATING 3.2.1 Cetane Number 48.0 min (ASTM D613/ASTM D6890/ISO 5165) 3.2.2 Cetane Index 40.0 min (ASTM D976/D4737A/ASTM D4737B/ISO 4264) 3.3 SULFUR 15 max (ASTM D5453/ISO 14596) 3.4 ASH 0.01% mass max
6、 (ASTM D482/ISO 6245) 3.5 COMPOSITION 3.5.1 Water 200 mg/kg max (ASTM D1744/ISO DIS 12937) 3.5.2 Total contamination 24 mg/kg max (EN 12662) ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyright 2011, Ford Global Technologies, LLC Page 2 of 4 3.5.3 Hydrocarbon typ
7、es Report (ASTM D1319/ISO 12662) 3.5.4 Polycyclic Aromatic Hydrocarbons 11% mass (IP 391:1995) 3.5.5 Fame Content 0.1% volume max (EN 14078/ASTM D7371) 3.6 DISTILLATION (ASTM D86/ISO 3837) Temperature, C Initial boiling point Report 10% vol recovery Report 50% vol recovery Report 90% vol recovery Re
8、port Final boiling point Report 3.7 DENSITY Report (ASTM D1298/ISO 3675, 15 C) 3.8 KINEMATIC VISCOSITY 1.3 - 3.5 mm2/S (ASTM D445/ISO 3104, 40 C) 3.9 OXIDATION STABILITY, total insolubles 2.5 mg/100 mL max (ASTM D2274/ISO 12205) 3.10 CALORIFIC VALUE, gross Report (ASTM D240) 3.11 CORROSION 3.11.1 Co
9、pper Tarnish 1 b max (ASTM D130/ISO 2160) 3.11.2 Rust Prevention Moderate rusting max (ASTM D665/ISO DP 7120, Procedure B, 30 minutes) 3.11.3 Silver Corrosion 1 max (ASTM D130 modified) 3.12 FLASHPOINT 50 C min (ASTM D93/ISO 2719) 3.13 LUBRICITY at 60 C 400 micron wear (ASTM D6079/ISO DIS 12156-HFRR
10、) scar diameter max 3.14 CARBON RESIDUE 0.20% max (ASTM D524/ISO 6615, 10% distillation residue) 3.15 WATER REACTION, fuel layer only 1, slight haze max (ASTM D1094/ISO 6250) ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyright 2011, Ford Global Technologies, LLC
11、 Page 3 of 4 3.16 COLD FLOW PROPERTIES, TEMPERATURE 3.16.1 Cloud Point -30 C max (ASTM D2500/ISO 3015) 3.16.2 Cold Filter Plugging Point Report (ASTM D6371/EN 116/IP 309) 3.17 ODOR The material shall have the usual characteristic odor of diesel fuel. There shall be no obvious foreign odors. 3.18 ADD
12、ITIVES The material shall contain normal commercial additives. The use of cold flow improver additives may be used with approval of Fuels and Lubricants Engineering. 3.19 COLOR The material shall be dyed in accordance with Customs and Excise requirements. 3.20 CONDUCTIVITY Report (ASTM D2624/ASTM D4
13、308) 4. GENERAL INFORMATION The information given below is provided for clarification and assistance in meeting the requirements of this specification. 4.1 FLAMMABILITY This material represents a potential fire hazard. The Manufacturing Engineering Department or other responsible activity shall noti
14、fy both the Security and Safety Units of its presence to assure that proper fire precautions are provided. The location in which it is used or stored shall be included in the notifications. 4.2 SAMPLING AND SUBMISSION OF SAMPLES (ASTM D4057/D 4177) 4.3 Quality Control records must be made available
15、to Fuels and Lubricants Engineering upon request. ENGINEERING MATERIAL SPECIFICATION WSS-M4C130-A Controlled document at www.MATS Copyright 2011, Ford Global Technologies, LLC Page 4 of 4 Manufacturing ISO/DIS ASTM Typical Limits Cetane Number 5165 D613 _ _ Cetane Index 4264 D4737A _ _ 4264 D4737B _
16、 _ Sulfur, % wt. 14596 D5453 _ _ Ash, % wt. 6245 D482 _ _ Water, mg/kg 12937 D1744 _ _ Total contamination, mg EN 12662 _ _ Aromatics, % vol 3837 D1319 _ _ Polycyclic Aromatic, % wt. IP 391:1995 _ _ Distillation 3405 D86 Initial boiling point _ _ 10% vol recovery _ _ 50% vol recovery _ _ 90% vol rec
17、overy _ _ Final boiling point _ _ Density15 C, kg/L 3675 D1298 _ _ Kinematic Viscosity, mm2/S 3104 D445 _ _ Oxidation Stability, mg/100 mL 12205 D2274 _ _ Copper Tarnish 2160 D130 _ _ Rust Prevention, Procedure B 7120 D665 _ _ Flashpoint, C 2719 D93 _ _ Lubricity at 60 C, microns 12156 D6079 _ _ Carbon residue, 10% 6615 D524 _ _ Water Reaction 6250 D1094 _ _ Cloud Point, C 3015 D2500 _ _ Cold Filter Plugging Point, C EN 116 D6371 _ _ Conductivity, pS/m D2624 _ _
