GOST 31644-2012 Juice products Determination of 5-Hydroxymethylfurfural (HMF) by High Performance Liquid Chromatography (HPLC) method《5-羟甲基糠醛(HMF)的高效液相色谱测定法(HPLC)》.pdf

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GOST 31644-2012 Juice products Determination of 5-Hydroxymethylfurfural (HMF) by High Performance Liquid Chromatography (HPLC) method《5-羟甲基糠醛(HMF)的高效液相色谱测定法(HPLC)》.pdf_第1页
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GOST 31644-2012 Juice products Determination of 5-Hydroxymethylfurfural (HMF) by High Performance Liquid Chromatography (HPLC) method《5-羟甲基糠醛(HMF)的高效液相色谱测定法(HPLC)》.pdf_第4页
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1、 , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)316442012 5- , - 1.092 . - 1.22009 . , . -, , , 1 () ( ), ( )2 3 , (- 50 20 2012 .) : ( 3166) 00497 ( 3166) 00497 AZAMBYKZKGRUTJ 4 26 - 2012 . 438- 316442012 1 2013 .5 5369420096 ( ) - ., . , 2012 -, II 3164420121 .12 13 24

2、 , , , , .25 36 .37 .68 79 .810 .9 () 5- - 1011III 316442012 5- Juice products.Determination of 5-Hydroxymethylfurfural (HMF) by High Performance Liquid Chromatography (HPLC) method 201307011 , - , , , , ( - ) () 5- (5-). ( ) 5- 1 /3(1). ( )50 /3(1).2 : 5725-12003()-. 1. 5725-22003()-. 2. - 12.1.005

3、88 . - 12.1.00776 . . 12.1.01076 .- 12.1.01893 . - . 12.1.01979 . . - 177074 ( 104283, 478880) . -, , , . 670972 . 1202676 . 1827072 . 2296790 ( 248680, 339981) - . 241042001 . 1 316442012 2533682 . , 2631384., 2667185 , . 2916991 ( 64877) . 2922791 ( 835-181) . . 1. - , 1 , , , , . (), () . , , , ,

4、 .3 - - (). 5- - 284 .4 , , , 4.1 ( 200 600 ) - - Millenium 2000.4.2 : 200800 ; c1770,2 ; c1770,08 (c108= 656 ); c1770,002 .1) 0,3 . c1770,003 . 1 .; c177 0,0008 . 1 .; 2) - c177 0,0001 . 0 ., c108= 500 c177 0,0006 . 1 ., c108= 500 ; 1,0 % (c108= 200 ) 0,05 % (c108= 220 340 ).4.3 250 4,6 , -, 5 .4.4

5、 25, 100 250 .4.5 24104 - c1770,1 .4.6 - ( ).4.7 (g-) 8001000.4.8 0,20 0,45 .4.9 1-2-1, 1-2-5, 1-2-10 2- 29169.4.10 1-2-25 29227 25 3 - c1771%.1). .2) .2 3164420124.11 25, 50, 100, 500, 1000 3 1770.4.12 1000 3 1770.4.13 25336: 1000 3; ; 50, 100, 250, 500, 1000 3.4.14 () 26 3.4.15 10 .4.16 .4.17 1202

6、6.4.18 6709.4.19 1.4.20 .4.21 18270.4.22 5- 97 % 5- 99 %.4.23 5 3 22967.4.24 -24/10 (30c18050).4.25 . , - - , .5 26313, 26671.6 6.1 1770 1000 3 840 3- 6709, 150 3 4.20 10 3 - 18270, 4.16 . 4.16- 15 0,45 . 5 . 15 0,20 .6.2 6.2.1 5- , , - . 5- ( - ) : 1:3 1:10, - 1:25 1:50. 5- - , , 4.7 990 g 15 . 12 3 4.23 , 0,45 0,20 4.14.6.2.2 5- - 10,0 % ( , ,3 316442012, .) , , 990g15. 10,0 % ( , , .) 1:5 -. 1770 50 3 1770 - 10 3 . 990 g - 15 . - 990 g 15 . 12 3 , - 0,45 0,20 .6.2.3 5- - - 1:5. 24104 50 3 4.24 57 , - 2535 . - (), ., ,- , - 6.2.2. 12 3 , - 0,45 0,20 .6.2.4 5- - 6.2.1, 6.2.2, 5-

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