1、 , , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)316912012, - 1.092 . - 1.22009 . , . -, , , 1 (-) - 335 2 3 , (- 15 2012 . 42) : ( 3166) 00497 ( 3166) 00497 AZBYKGRUTJ 4 29 2012 . 1423- 316912012 - 1 2013 .5 5309320086 ( ) - . , - . - , 2013 -, II 3169120121 .12 13 .24
2、 , , , , .25 .36 37 .68 79 .710 7 8III 316912012 , Grain and products of its treatment, mixed feeds.Determination of zearalenone content using high-performance liquid chromatography1 - (: 2) (, , ) , - (, ). 0,1 10 /.2 : 177074 ( 104283, 478880) ., , , . 416676 . . 420477 . . 432877 . . 655280 . . 6
3、70972 . 929374 . 13586.383 . 13496.080 , . 2001588 . 241042001 . 2533682 . . - 26312.184 . 2766888 . 2922791 ( 835-181) . . 1. - , 1 , , . (), (-) . , , , , .1 316912012 201307013 , - - .4 , , , , () , - (270 c177 20) - 450 470 () , (270 c177 20) . 0,1 /3. . - , 40000 , 18 150 2,1 ., - . - 200 24104
4、 0,01 . 2 1, 5, 10 3 29227. 2 100, 200, 500 3 1770. 2 50, 100, 250 3 1770. 100 /3 c177 5,0 /3. -12 . , 25336, - 2,5 10 . , 120 1. , 1 . , 200 C. . 1 . 1 10 - c 1 14 c177 0,1. 100 250 3 25336. 25336. 100, 1000 3 25336. 10 50 3 25336. . 6709 1 . 4166, . . , 200 0,025 , 0,03%. 20015, . 4328, . . 6552,
5、 . 4204, . . . 9293. , , , .2 3169120125 13586.3, 13496.0, 26312.1, 27668. 100 , , 1 . . . .6 6.1 ( - ), - . - . 3 .6.2 6.2.1 ( - 50:50) . . . . 1.6.2.2 40 /3 500 3 200 300 3 , 20 , . . 2 .6.2.3 3,5 % 200 3 100 3 , 7 3- , , , . .6.3 6 C , .6.3.1 1 /3 1 3 100 /3, 100 3 . (0,/3) 0=VV. c.oc215,(1) c.
6、/3;Vc. , (1 3);V (100 3). 6 .6.3.2 6.3.1 . 1. -3 316912012 40 C 45 C. - 6.2.1 1. 24 . 1 6.3.1, 3 , 3 , /315 1 5,02 1 1 1,03 1 5 0,2 (,/3) =VV00c215,(2) 0 6.3.1,/3;V0 , , 3;V , 3.6.4 () . (. 4). - , - .6.5 -6.3.2. , - , . 5 %. - . :- 0,99;- - c177 10 %. - , 5 %.6.6 . , - 6.3.2. , . - , - , . (3) (4) ttt12c45c163 0,05,(3)4 316912012t1t2 ,;t t1 t2,.CCC12c45c163 0,07,(4) 1 2 ,
