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GOST 31724-2012 Vodkas special vodkas and water for their production Determination of cations amines anions of non-organic and organic acids content by capillary electrophoresis me.pdf

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1、 , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 31724null2012, , , 317242012II, - 1.092 . - 1.22009 . -, . , , , 1 - ( )2 ()3 , (- 1 2012 . 51) : ( 3166) 00497 ( 3166) 00497 AM BY KG MD - RU UZ 4 29 - 2012 . 1590- 317242012 1 2013 .5 529302008 6 - , . () - . , - - , 20

2、14 -, - 317242012III1 12 13 .24 34.1 34.2 , , 34.3 .44.4 44.5 .44.6 .54.7 .54.8 .64.9 , 75 86 8 () , , , .9 () , , , 101 20130701 1 , , - - , - (, , , , , , , , ), (, ), (, -, , , , , ), (-, , , , , , , , , , ) , , , , , , , , , , . , , - 0,5 20 /3( 0,1 20 /3; 0,5 10 /3).2 : 5725-12003 ( ) -. 1. 572

3、5-62003 ( ) -. 6. / 170252009 - 8.01099 . - . 8.31597 . - . 12.1.00491 . . - 12.1.00776 . . . 12.1.01076 . . - 12.1.01893 . - . 317242012 , , , Vodkas, special vodkas and water for their production. Determination of cations, amines, anions of non-organic and organic acids content by capillary electr

4、ophoresis method 3172420122 12.1.01979 . . - 6175 . . 177074 ( 104283, 478880) . -, , , . 377372 . . 410872 . 2-. 413975 . . 414074 . 6-. 414277 . 4-. 414574 . . 417276 . 12-. 420775 . 3-. 420977 . 6-. 421276 . - 421777 . . 423377 . . 423477 . . 432877 . . 581777 . . 634175 . . 670972 . 1052178 . .

5、2030174 . . 2218076 . . 241042001* . 2448180 . 2533682 . , , 1 , - . (), (-) . , , , , .3 3.1 , .3.2 , , - 2 3, , 1 5 3 1 3 .3.3 3.2 , - .3.4 24481. 100 3. 50 3 .* 532282008 -. 1. . . 3172420123 () 3.2 3.3, - .3.5 , , , , . , 8 25 . 8 -, .3.6 , 5 10 3.3.7 4.7.4 4.1 , , - .4.2 , , 30 30 , , 150 50 ,

6、 () - ( ). 24104 210 0,1 . 25336. , .3 ( ). 1 5 3. 0,1 1 3. 0,005 0,05 3. - , 0,45 . 20, 50, 100, 1000 3. 2 3. 1(2)-25 (50, 100, 1000)-2 1770. , . ., 61. , . ., 3773. 2-, . ., 4108. , . ., 4139. 6-, . ., 4140. 4-, . ., 4142. , . ., 4145. 12-, . ., 4172. , . ., 4207. 6-, . ., 4209. , . ., 4217. , .

7、 4233. , . ., 4234. , . . ., 4328. , . ., 5817. , . ., 6341. 6709. 3172420124 ( 6709, - 20301) 18,2 . , . ., 10521. , . ., 22180. , - , . (thanolamine hydrochloride Fluka*, 02415, 98 %). (Propylamine hydrochloride Aldrich*, 242543, 99 %). , , , .4.3 , .4.3.1 (NaOH) = 1,0 /3 4,0 100 3, - 50 60 3 . 2 .4.3.2 . -, 10 .3 ( ). , .4.3.3 , .3 (- ), 30 ,

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