1、 , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)317342012, 1.092 . 1.22009 . , - . , , -, 1 - - (), - 160 , 42 3 , (- 1 2012 . 51-) : ( 3166) 00497 ( 3166) 00497 AZAMBYKGMDRUTJ -4 ASTM D 1796-11 Standard test method for water andsediment in fuel oils by the centrifuge me
2、thod (laboratory procedure) ( ). D02.02 - ASTM D02 API - (ASTM). ASTM, - , ASTM, , - . - 1.52001 ( 3.6). ASTM . (en). (IDT)5 15 2012 . 893- 317342012 - 1 2014 .6 -, - . () . , - - , 2013 -, II 3173420121 12 13 24 25 .36 57 .68 69 .810 .811 8 .1 () 10III 317342012 Fuel oils. Method for determination
3、of water and sediment by centrifuge method 201407011 1.1 0 % 30 % ( ) . 1 , - , , - . ASTM D 95 (API MPMS, - 10.5) ASTM D 473 (API MPMS, 10.1). 2 API MPMS, 10.6 (ASTM D 1796) API MPMS, 10.3(ASTM D 4007) API 2548.1.2 , , . , , .1.3 , -. , -. 6.1.2 . -().2.1 ASTM1):ASTM D 446-07 Test method for water
4、in petroleum products and bituminous materials by distillation()ASTM D 473-07 Test method for sediment in crude oils and fuel oils by the extraction method ( )ASTM D 4007-11 Test method for water and sediment in crude oil by the centrifuge method (laboratoryprocedure) (- )ASTM D 4057-06 (2011) Pract
5、ice for manual sampling of petroleum and petroleum products (- )ASTM D 4177-95 (2010) Practice for automatic sampling of petroleum and petroleum products (- )1) ASTM ASTM website, www.astm.org ASTM serviceastro.org, ASTM(Website standsrds Document Summary).1 317342012 ASTM D 5854-96 (2010) Practice
6、for mixing and handling of liquid samples of petroleum and petroleumproducts()ASTM D 6304-07 Test method for determination of water in petroleum products, lubricating oils, andadditives by coulometric Karl Fischer titration ( , - )ASTM 542-01 (2007) Practice for calibration of laboratory volumetric
7、apparatus ( )2.2 API2):API MPMS Chapter 8.1 (R2006) Practice for manual sampling of petroleum and petroleum products(ASTM D 4057) ( )API MPMS Chapter 8.2 (R2010) Practice for automatic sampling of petroleum and petroleum products(ASTM D 4177) ( )API MPMS Chapter 8.3 (R2010) Practice for mixing and h
8、andling of liquid samples of petroleum andpetroleum products (ASTM D 5854) ( )API MPMS Chapter 10.1 (2007) Test method for sediment in crude oils by the extraction method(ASTM D 473) ( )API MPMS Chapter 10.3 (2008) Test method for water and sediment in crude oil by the centrifuge method(laboratory p
9、rocedure) (ASTM D 4007) ( )API MPMS Chapter 10.5 (R 2010) Test method for water in petroleum products and bituminous materialsby distillation (ASTM D 95) 2.3 IP3):Methods Book, appendix B. Specification for methylbenzenes (toluenes) , - . ()2.4 ISO4):ISO 5272:1979 Toluene for industrial use Specific
10、ations ( . )3 3.1 . .4 4.1 , . - , , , -.4.2 , . , , , - ASTM D 6304.2 3173420122) . , 1220 L.St., N.W., Washington, DC 20005.3) , 61 New Cavendish St., London, WIG 7AR, U.K.4) (ANSI), 25 W.43rdSt., 4thFloor, New York, NY10036, http:/www.ansi.org.5 5.1 5.1.1 , ( ) - 203 (8 ), (rcf) 500 800 (5.1.6).5
11、.1.2 , , -, , - , . . -() .5.1.3 - . - (60 c177 1) (140,0 c177 1,8) F . - .5.1.4 . 3 - , , , .5.1.5 , (r/min), r/min = 1335 rcf d, (1) rcf ;d , , , ; r/min = 265 rcf d, (2) rcf ;d , , , .5.1.6 , - (r/min), rcf = drmin13352c230c232c231c246c248c247 ,(3) d , , , ; rcf = drmin2652c230c232c231c246c248c24
12、7 ,(4) d , , , .5.2 5.2.1 , , 1. , 1, . - , 3 317342012 . 1 , , 20 (68 F) .4 3173420121 ; 2 ; 3 10 ; 4 1;5 1 203 (8 ) 1 203 (8 -), , , 0 0,1 0,05 c1770,02 0 0,3 0,05 c1770,03 0 0,5 0,05 c1770,05 0 1,0 0,10 c1770,05 1,0 2,0 0,10 c1770,10 2,0 3,0 0,20 c1770,10 3,0 5,0 0,50 c1770,20 5,0 10 1,00 c1770,50 10 25 5,00 c1771,00 25 100 25,00 c1771,005.2.2 ASTM 542, , (NIST)5) -. 0,5 ; 1, 1,5, 2, 50 100 . , - 1, .5.3 , -
