1、 (). (ISO 15302:2007, MOD) , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)321232013(ISO 15302:2007), - 1.092 . 1.22009 . -, . , , 1 - ( ) -(-)2 (-)3 , ( 7 2013 . 43) : ( 3166) 00497 ( 3166) 00497 BYKZKGRUTJUZ 4 27 2013 . 224- 321232013 (ISO 15302:2007) 1 2014 .5 ISO 1530
2、2:2007 Animal and vegetable fats and oils Determination of benzoapyrene Reverse-phasehigh performance liquid chromatography method ( . (). ). , , . (MOD). 539552010 ( 15302:2007)6 -, - . () . , - - , 2014 , - - II 3212320131 .12 13 24 25 .26 27 38 .39 .310 .411 .512 5 () 6 () .7 () - , 8III 32123201
3、3 (). Animal and vegetable fats and oils. Determination of benzoapyrene.Reverse-phase high performance liquid chromatography method1 a - - () 0,1 / 50 /.2 : 661:2003 . - 3696:1987 . - 5555:2001 . 5725-22003 ( ) - . 2. - 177074 ( 104283, 478880) ., , , . 2916991 ( 64877) . 2533682 . , - - , 1 , - . -
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5、4).6.2 4 , 10 3 (5.1) 90 (5.8). , - . . 15 24 . .6.3 , 0,5 /3, 0,1 , 12,5 1770 25 3. (5.6) . 4 C 6 .2 3212320136.4 , 0,5 /3, 0,2 /3 0,01 /3, - .6.5 b - , , , 10 /. 10 - 1 /. b, 99,0 % , .7 , , :7.1 , 300 15 , ().7.2 ,(35 c177 2) C(65 c177 2) C.7.3 , 40 C. . - .7.4 , , 50,- . , - .7.5 7.5.1 , , (, 7
6、5 4,6 , Lichrosorb RP-18 ( 5 ).7.5.2 , 250 4,6 ( ), () (,Chromspher 5 PAH Vydac 201 TP5).7.6 , 460 ( 10 ) 384 ( 10 ). - .7.7 ( 1 ), - .7.8 , .7.9 .7.10 1770,25 3.7.12 29169, 1 5 3, .7.13 , .8 5555. , .9 661.3 32123201310 10.1 10.1.1 , 0,001,0,400 - 25336 2 3 (5.2).20 - (5.10) . 50 / . , 50 - (5.10). 125 / .10.1.2 (7.1) - (5.2). 22 (5.8) 25336 50 3 , .10.1.3 (5.7) 30 .10.1.4 .10.1.5 20 3.10.1.6 (10.1.1) . (5.2), - .10.1.7 - 1 /, 20 3 60 3 100 3.10.1.8 , 65 C, 0,5 3 1,0 3, (7.7), 0,1 .10.1.9 (5.1), - 35 C ( 25 3/) . - 1 , . , . 10.1.9 - .10.1.10 35 C .10.1.11 0,1 .
