1、 , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)321682013, - 1.092 . 1.22009 . -, . , , 1 - - ( -) 2 3 , ( 19 2013 . 56-) : ( 3166) 00497 ( 3166) 00497 BYKZKGMDRUTJUZ -4 17 - 2013 . 1071- 321682013 1 2014 .5 5387820106 -, - . () . , - - , 2013 -, II 3216820131 .12 13 24
2、.25 26 36.1 36.2 .36.3 36.4 36.5 .36.6 , , 36.7 66.8 .76.9 , , , -.76.10 7 8III 321682013 Honey. Method for the determination of honeydew honey1 .2 : 12.1.00491 . . 12.1.00776 . . - 12.1.01979 . . - 12.4.00983 . . . 102767 . (II) 3-. 177074 ( 104283, 478880) ., , , . 3310-12002.1. - . 670972 . 86777
3、6 . . 1491983 , . - 197922001 . 241042001 . 2533682 . , 2562983 . 2849890 . . 2922791 ( 835-181) . . 1. 317662012 . 317682012 . 1 321682013 20140101 317692012 . 317702012 . 317742012 . - , 1 , - . - (), () . , , , , .3 19792, 25629, 31769 - :3.1 (honeydew elements): , ,- .3.2 (structural elements of
4、 honey): - .4 4.1 12.1.019.4.2 12.1.004 12.4.009.4.3 12.1.007.4.4 , - , - .5 , - - , 1, 2, 3. 1 -, , , : , , 2 (/): , , 11332 321682013 3 - * , %, , %, *, /, , %, 45,015,00,80,60* -, .* , , , , . 19792.6 6.1 19792.6.2 6.2.1 , - 1600 , 220 , - 20 C 100 C, 14919 40 C, 3310-1 20 .6.2.2 ( ) , - .6.2.3 .
5、 .3, .6.3 19792 31766.6.4 ()()31769, (/) 2.6.5 31770.6.6 , , 6.6.1 , 19792.6.6.2 : , , , () .6.6.2.1 , , , :- 0,1 5,0 3/;- ;- ;- ;- .3 321682013 250 (150 ) 4,6 . Phenomenex C18(ODS) 4 c180 3 . 0,010 0,050 3 ( ). 24104 - c1770,003 . Millipore Simplicity . . 1(2)-100-2() 1770. 2-2-25 29227. 3-50(100)
6、1770. -1-100 25336. -1(2,3)-250-29/32(34) 25336. 1- 0,0100,100 3,0,1001,0 3, 1,05,0 31- . 0,45 c215 106. 20 C 100 C. 15 20 . . . 99,0 %. 99,0 %. 99,0 %. 99,0 %. 1 1. -, . .6.6.2.2 ) 250 3 25336 80 3 20 3 1. . 4 C 30 .) (2,000 c177 0,001) , (1,500 c177 0,001) , (0,250 c177 0,001) , (0,150 c177 0,001)
7、 100 3 1770. 25 3 . , . 0,45 c215 106. 4 C 30 18 C 180 .) 50 3 (5,000 c177 0,001) , 6.2. 1020 3 6709, 100 3. , - , , - 2/3 . 25 3. , . - 0,45 c215 106. 4 C 30 18 C 180 .6.6.2.3 :- Eclipse XDB-C18, 5 , 150 c180 4,6 (. 6.6.2.1);- Phenomenex 18 (ODS) 4 c180 3 (. 6.6.2.1);4 321682013- (30 c177 1) C;- 1,3 3/;- 6.6.2.2,);- 20 . : (5,2 c177 0,3) ; (6,0 c177 0,3) ; (8,5 c177 0,3) ; (18,0 c177 0,3) . , 6.6.2.2,), , 6.6.2.2,), .